Fill in appropriate values in box colored yellow final end point is at

To Study the kinetics of reaction in Co

Step 1

Prepare different concentration of NaOH (A) and Ethyl Acetate (B) and fill in the storage tank as given

Range of concentration f
Range of concentration for Ethy

Your Chosen conc

Essentially CA0' Not equals

Step 2

Set the flow rate of NaOH (A) solution and Ethyl Acetate (B) solution from the storage tank using

Range of flow rate f

Range of flow for Ethy

Your Chosen

Step 3

Wait for CSTR and PFR to attain the ste

make sure ball valve between PFR and CSTR is open and liquid is coming out from the outlet

volum
volume
738.94736
Minimum time required for steady state in 1.5 times sp
Fill in your answer the minimum time required for ste

0 indicates stady state not achived you need to wait more for ste
1111111 indicates stady state is achived go ahead and take

you will get wrong reading if, readings are taken without waiting for ste
wait for more time for steady state if values in red
Go ahead for further teps stime if values in red box is
Step 4

Sample collection CSTR

make sure ball valve between PFR and CSTR is open and liquid is coming out from the outlet

Volume of CSTR sample

Step 5

Sample collection PFR

Close the valve ball valve between PFR and CSTR liquid is coming out from the outl
Wait for some time and collect th

Volume of PFR sample

Step 6

Prepare stander HCl for neutralize remaining NaOH at given time in above reaction
Excess of NaOH is neutralized by immediately adding this sample to conical flask with 20 ml 0
Volume of stander HCl taken in con
Normality of stander HCl taken in con

Step 7

Estimation of excess of HCl use using stander NaOH solution by titration

Remaining HCL can be estimated by titration this mixture with 0.1 N solution fro

Concentration of NaOH taken i

You are expected to get below end point to

Burette end point for PFR Sa
Burette end point for CSTR sa

If CA0=CBO reading V PFR and VCSTR are worng and equals to

 t bottom in sheet need to used for calculations
Combine flow reactor

CA0' = 0.03 N to 0.15 N

CB0' = 0.03 N to 0.15 N

NaOH CA0' = 0.1 mol/L

Ethyl Acetate CB0' = 0.09 mol/L

νA = 5 LPH to 15 LPH
νB = 5 LPH to 15 LPH

NaOH νA = 10 LPH
Ethyl acetate νB = 9 LPH

V PFR 0.69 L
V CSTR 1.91 L

t ss 800 sec

1111111
Vs CSTR 20 ml

CSTR
Sample
Vs PFR 20 ml
20 ml

V HCl 20 ml
N HCl 0.1 N

N NaOH 0.1 N

V PFR 14.0 ml
V CSTR 16.1 ml
Final Reading
to be used for
calculations
Titration using standered
0.1 N NaOH from burette
End point is V CSTR

20 ml sample from C
mixed with 20 m
stander HCl
 0

131

0 CB0'
CA0'
0

362

54

νA νB
0
 Ball
Valve
CSTR
Sample
20 ml PFR Sample 20 ml
20 ml sample from CSTR 20 ml sample from PFR
mixed with 20 ml mixed with 20 ml
stander HCl stander HCl
Titration using standered
0.1 N NaOH from burette
End point is V PFR