Studes:-nbtutood

CH:

Gnnomaldehyda
A) For Cassia ail ast)talos
CaMia oil 685ml
ANg
Facter Crinamic adihyd
Imt orsAle KoN lutin (6o4)o-06514
carramie alsutyde
-. x =685 x bo661

o452
1009 Caiia eil Cotai 45-2 94
:% Gontent iimaldahyda in Casia ail is 45-277%
rimomaldehyde
tvg =I3ml
Factor:
4md o o-5M Ale KoH doutian =
i: |13ml d os MAl 0-0661 q Cnnamic aldahyd
KoH douion
o74643
l00g irnamaldehyde
dehyde is }4-643. wlw
 25

Cxpexament NO 3
Detexminatiacn a Aldekydel and ktencs fan

Aimi Ta determins the eerant Centnt d aldahydud

and Kotena pukeat in aiuo_elential o ie

Requisaeooenta:
Appaatuk i Buxatte, Beaken, Canical laik, fipette and
uighing dpsan in Ethanal Co)
D-SM Pataiun Hydxexid1 io 60% ethsaal
Hyaanyoni hydrachlasida
Phunslud Aeltien, Taluene

Releence, i A H Beckett JB_ stenlake, "Batial phama kutial

Th deteninatiea aldehyda dapead upon the

uadian with hydraxylaioa hydahlasida cyawled
R-CHÌ t NH,OH, Hl R-CH:N-OH t Ho + Ha.
Tae dibatd HC Con be titrated withAtd altale.
The uatieahich id eAMible, qad te Campltisa i/
Hhe Hciu emeued by tthotg uith alkali.ds the
t te detet
tbatian i Gostinucd tota the al yellaw lalaute
t
the methyl ct ange indiratiak.
Hydmanylania Hydzahlaside i hydalyled in delatie
nd i acidi. to mekyl erange Ta Conaptalata fan
the ad prentdue to
 Calwlatisns:

:’obsrvatien Table. gars

BURETTE READLNGS
0ILS
Ri R
0me64md 6:85m
6-&md
(3) himsn ail
ed m u8ml:
1·4md 16 m 1:Smt
9 range ||2m ||4m |3m2
’ Callatian:

FACTOR= 1mb o 0:5 Al koH dalton:(607) =0:06641g o

Grroriic udehyde
Averaged innamon ail 6, mlin

Thauloe,
ha1 a< innamonail Contain Oi45609 - Gnnorit
alaebyde
Cantent
 the Latr ià fit neutralled ta the fll yeles
oindy Aydieylaias hydracklaida but a denall
Jn hydaxyloasise alio i praleat.
bath haseand dat m ua ith aldehudis Thud
he aid utratd duioa the
h actual aslayA danewhat
e then dhald Hhiatstial hae ben fendi
empialal acterCx 00k) ia iatadued tata
HCalelatian to allo thid ettat

’PreCedue

led toa
Sml aToua to diuau inosnen oil fallaued

igatauly shakaa aod

0:SMAlc. kOH AdtO.
ttnated
9 Th
againt
ttatien was Cantiaued uith wig aaud i dhatkihg
All the aussr lay tain yele alaur the
indicatay

I FoR LEMON 0IL ORANGE 0IL

Atapjoallauk.
in ethanal C6o.. hydanyleia hydzahleide uagat
The Contst the ak Vigeteusly dhaken oanel
tnted againat 0:SM Alc KoH Selten
cbrol 1144
95 Cantain cl range l009 i.
Thoat
1:5mt
t ail rarge Cmt
ihdAatage
)
0t633a/ Imd0:StAlc Fato
ange Far ’
w (atral) oil dmen Contet 2
545374 alentain Jamsn loog
athal O'595344 contoin ail snan l0g
Thuutoe,
atkal
ar 8m
mlm :78 ail een Cmt) Asage
0:0#633 (607) KoH Alcio5m Iml Fater:
Qil demen ’DFex
 (29)

0 Th titatiea wad Continud utth igkukdythaking

the loex autr eadian ataiAA yellaw Calaut
the indicats

Rut: giua
The aldehyde delatien Contaia isnomi aldehyde) in

Tae adehyde (cathal) Cantoia ia qiun Aemenoil i

A
5:953 wlw.
The aldehuda Cataal) Cantaia in qiua gtang
1144% wlw.
J4)9 The aldehyde Contoán Ctinnorni alcehyde)in giuaa
45.222 wlw
Cimaaldehyda Sanple
)Tha aldehyde Can tain iain gun
44-693% wlw