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14680629.2019
14680629.2019
To cite this article: G. Bharath, Manoj Shukla, M. N. Nagabushana, Satish Chandra & Amit Shaw
(2020) Laboratory and field evaluation of cement grouted bituminous mixes, Road Materials and
Pavement Design, 21:6, 1694-1712, DOI: 10.1080/14680629.2019.1567375
Cement Grouted Bituminous Mix (CGBM) is a composite material, in which air voids present
in the bituminous mix are grouted with a cementitious material. The main aim of this study
is to develop and evaluate CGBM in the laboratory and field. A conventional dense graded
Bituminous Concrete (BC) mix is also considered for comparison. This paper presents the
details of different investigations carried out for evaluation of CGBM mix for properties such
as Indirect Tensile Strength (ITS), Resilient Modulus and Dynamic Modulus at different tem-
peratures. Performance characteristics such as rutting, fracture energy, moisture resistance, oil
spillage and durability were also evaluated for the mixes. A CGBM test section has been laid
on site and is being monitored for its performance. Results show that CGBM has better ITS,
Resilient Modulus, Dynamic Modulus, and Rutting performance than a conventional bitu-
minous mix. It shows a slight reduction in durability and crack resistance due to the relative
brittleness of the hardened cement constituent but within acceptable limits. The material is also
more resistant to damage by moisture and diesel. CGBM mixes are less temperature suscep-
tible compared to conventional bituminous mix. Dynamic Modulus and Phase Angle master
curves for CGBM mixes have been developed in the study. Full depth grouting was observed
in field core samples and Micro Computed Tomography (Micro-CT) tests were carried out to
check the air voids connectivity and their content in the CGBM mix.
Keywords: cement grouted bituminous mix (CGBM); full depth grouting; dynamic modulus;
rutting; fracture energy; durability
1. Introduction
Cement Grouted Bituminous Mix (CGBM) is a unique type of composite surface course that
consists of an open graded porous bituminous mix as its core structure, grouted with a pre-
cisely selected cementitious material. Technically, it is a designed amalgamation of concrete
pavement and bituminous pavement, thus consequently and desirably having the nature of both
rigidity and flexibility. The need for such a new kind of pavement material arises to overcome
deficiencies in conventional surfacing (Bituminous Concrete) while retaining its advantages and
benefits. Specifically, the issue of ‘rutting’ in bituminous pavements and ‘provision of joints’
in concrete pavements giving poor riding quality are likely to be completely eliminated in
‘Cement Grouted Bituminous Mix’. This kind of pavement has been christened differently by
different researchers and developers, such as Asphalt-Portland Cement Concrete Composite,
APCCC (Al-Qadi, Gouru, & Weyers, 1994), Semi-Flexible Composite Mixture (Zhang, Huang,
& Goodwin, 2013), Semi-Rigid Pavement (Dong Qing Wu & Zhang, 2011), Grouted Macadam
Composite Material (Hou, Xu, & Huang, 2015), etc. It is to be noted that CGBM has not been
adopted on Indian roads mainly due to lack of data on its performance under Indian conditions.
All the studies related to CGBM have been from outside India and mainly from the developed
world. Therefore, the present study was undertaken for the evaluation of the strength and per-
formance characteristics of cement grouted bituminous mix and its comparison with those of
conventionally used surface layers of bituminous concrete.
The main issues related to conventional mixes which can be checked or controlled using
CGBM are as follows:
CGBM shows better performance in terms of durability and strength when compared to
conventional hot mix asphalt pavements and thus can be successfully used for bridge deck
overlay (Al-Qadi et al., 1994). Comparative studies of CGBM and conventional bitumi-
nous mixes have shown that at higher temperatures, the ITS values for CGBM increase
by 2–3 times those of bituminous concrete (BC) mixes (Anderton, 2000; Oliveira et al.,
2006).
Zhang et al., 2013 examined CGBM and PG 70–22 Hot Mix Asphalt through various strength
and performance tests. CGBM was observed to have a higher dynamic modulus, better resistance
to moisture induced damage and thermal cracking, lower temperature susceptibility and lower
rutting values. CGBM samples were found to have higher fractural strength when compared
to HMA mixtures. Husain, Karim, Mahmud, & Koting, 2014 evaluated CGBM designed for
different aggregate gradations. It was found that, as the aggregate (aggregate gradation) gets
coarser, there is an increase in VIM (voids in the mix) which helps in the flow of grout slurry. In
case of less porous aggregate gradation, the movement of fluid grout was found to be delayed.
One day cured specimens had more abrasion loss in comparison to the 28-days cured specimens.
Moreover, the abrasion loss was found to be inversely related to the compressive strength of the
samples.
Raju, Reddy, & Reddy, 2014 examined rut resistance and moisture damage susceptibility for
CGBM and found them to be lower in comparison to normal bituminous mixes. The average
value of elastic modulus using beam flexure tests for CGBM was measured to be 10400 MPa
(at 35°C). Hou et al., 2015 report higher values of dynamic stability and fatigue life for CGBM
as compared to conventional bituminous mix. The CGBM had a flexural strength of 5.2 MPa
against 6.63 MPa for the bituminous mix. The retained Marshall stabilities of CGBM and the
bituminous mix were 110.1% and 87.8% respectively and the TSR values were 85.5% and 81.8%
respectively. The modulus of the CGBM mix has been determined in terms of resilient modulus,
flexural modulus and dynamic modulus. Al-Qadi et al., 1994 showed resilient modulus values in
the range of 3000– 3400 MPa (at 22°C). Anderton, 2000 evaluated the resilient modulus values
of CGBM and reported them to be 19200, 11200 and 5800 MPa at temperatures of 5, 25 and
40°C respectively.Based on field and laboratory studies conducted on CGBM mixes, rutting
performance has been reported superior by almost all the researchers who worked with this
material (Ding, Sun, Shen, & Huang, 2010; Gawedzinski, 2008; Hou et al., 2015; Ling et al.,
2009; Raju et al., 2014).
1696 G. Bharath et al.
2. Objective
The main objective of the present study is to evaluate the mechanical properties and perfor-
mance characteristics of CGBM mixes and compare them with those of conventional Bituminous
Concrete (BC) mix. The following main issues are examined.
• Evaluation of CGBM properties such as stability, indirect tensile strength, resilient modu-
lus, dynamic modulus, compressive strength and performance in terms of rutting, fatigue,
moisture resistance, durability and resistance to petroleum products.
• Evaluation of grout material properties with respect to water content and curing period.
• Field performance evaluation of CGBM mix.
• Comparison of the performance of CGBM with that of conventional BC mix.
3. Experimental Protocol
The laboratory studies involved material selection, characterisation and mix design for CGBM
and BC mixes. Brief details are given in the following subsections.
Figure 4. Air voids reduction with number of Marshall hammer blows in CGBM mix.
further grout penetration was observed. Sometimes the porous bituminous samples may need to
be slightly shaken to help release the entrapped air and ease the flow of grout into it. Initially
trial grouts were prepared at different water contents starting from 16% and up to 40% with an
increment of 2% after each trial. Selection criteria for finding the optimum water content was
flowability (measured in terms of Marsh Flow Time) and full depth grout penetration in the
specimens of CGBM. At 16% water content, grout could penetrate only to a small depth (partial
depth of grouting) and most of the grout was retained on the surface as shown in Figure 5 (a). At
18% water content, grout penetration was observed up to the half depth of the specimen, but at
20% water content, the grout material could be seen to penetrate to full depth of the sample (full
depth grouting) and voids in the sample appeared to be filled completely with grout, as shown
in Figure 5 (b). At such optimised value of water content, full depth grouting was observed in
both the cases of laboratory prepared samples and cores taken from the trial section laid on the
road. Air voids in the laboratory prepared CGBM (grouted samples) was found to be 2.59% as
computed using Micro-CT technique.
The extent of grout penetration into the voids of bituminous mix structure is not only linked
to initial air voids but also affected by morphological characteristics of air voids, void structure
and size which significantly influence the interconnectivity of voids in the mix structure (Vavrik,
Pine, Huber, Carpenter, & Bailey, 2001). The voids are either opened; partially opened or closed
in the bituminous mix. The degree of grouting depends on the quantity of opened and partially
opened voids and their size. The grout material does not penetrate easily into closed voids. To
improve the extent of grouting of the bituminous mix, closed voids should be reduced as far as
possible.
stability and compressive strength of the two mixes are given in Table 2. The laboratory test
results for ITS at three test temperatures of 25°C, 35°C and 45°C are shown in Figure 6.
BC 1 16.9 2.3
2 18.0 17.3 2.0 2.2
3 17.2 2.2
CGBM 1 109.6 5.6
2 119.1 114.6 5.9 6.0
3 115.2 6.4
the repeated Indirect Tension Test method. Three specimens were prepared for both mixes for
determining the resilient modulus at different temperatures. Table 3 gives the percent reduction
in the modulus value at a higher temperature with respect to the value obtained at 25°C. CGBM
mixes have a higher resilient modulus value as compared to that of the normal bituminous mix.
Resilient modulus values of both CGBM and BC mixes decreased with an increase in test tem-
perature, which is quite obvious and expected. The resilient modulus of BC mix reduced from
5895 MPa to 1050 MPa (82.2%) when test temperature was changed from 25°C to 45°C. The cor-
responding reduction in the MR value of CGBM was 45% only. This shows that CGBM mixes
are less temperature susceptible as compared to bituminous concrete mixes.
Table 4. Dynamic modulus and phase angle values for selected mixes.
25 26,971 19,680 13,602 14,054 6020 2112 6.1 7.9 12.0 15.0 27.4 37.0
20 26,553 19,225 13,168 13,537 5775 2004 6.1 8.1 12.4 15.5 27.1 35.2
10 25,372 18,041 11,884 12,064 4806 1553 6.2 8.3 13.5 16.9 28.5 34.5
5 24,230 16,889 10,602 10,665 3943 1194 6.3 8.8 14.9 18.4 29.8 33.8
2 22,777 15,402 8905 8956 2968 825 6.4 9.6 17.0 20.6 31.3 33.1
1 21,678 14,261 7623 7771 2359 639 6.5 10.5 18.5 22.2 31.9 32.1
0.5 20,630 13,105 6467 6678 1866 498 6.8 11.5 19.7 23.8 32.2 30.9
0.1 18,144 10,200 4454 4458 1048 297 7.6 14.3 19.4 27.8 32.3 28.5
0.1 Hz were considered. Phase angle (φ) is a visco-elastic characteristic of bituminous mixes.
Phase angle is obtained as an output of the dynamic modulus (E*) test. The average dynamic
modulus and phase angle values are given in Table 4. The test was performed asper AASHTO
TP 79 (2013). Master curves for the dynamic modulus and phase angle at a reference temperature
of 35°C are shown in Figures 7 and 8 respectively. The model adopted for developing the master
Road Materials and Pavement Design 1703
curves for phase angle was a modified version of the sigmoidal model given by Yang & You,
2014.
Dynamic modulus (E*) values decreased with a decrease in frequency and with an increase
in test temperature. Dynamic modulus values of CGBM are significantly higher than those of
conventional bituminous mixes at the same temperature and frequency. Phase angle (φ) increased
with a decrease in frequency and with an increase in test temperature. For bituminous concrete
(BC) mixes, the phase angle values are higher as compared to the values obtained for CGBM
mixes. Phase angles for combinations of high temperature and low frequency have been found
to have a reversing trend which is commonly attributed in the literature to the aggregate locking
effect.
5. Performance evaluation
5.1. Rutting
Rutting performance of the two mixes was studied at 60°C temperature using a wheel tracker
device. The slabs (size 30 × 30 cm) were prepared with a roller compactor at the design density.
The test slabs were subjected to vertical pressure of 620 kPa applied through 50 mm wide wheels
having a diameter of 200 mm and running at a speed of 60 passes per minute. Each sample was
subjected to 20,000 passes (10,000 to and fro repetitions) of the wheel load. Rutting performance
of both CGBM and BC mixes is shown in Figure 9. The CGBM mix showed much smaller rut
deformation than the BC mix.
BC 1 33,770 34300
2 34,920
CGBM 1 32,530 31800
3 31,110
BC 1 1.00 0.76
2 0.97 0.99 0.87 0.80 80.87
3 1.01 0.78
CGBM 1 2.37 2.18
2 2.31 2.33 2.30 2.24 96.28
3 2.31 2.25
cyclic loading is used. The test parameters were set as: pressure at 275 kPa; temperature at 60°C
corresponding to PG64-22 (VG30) bitumen; the number of cycles to be 3500. After conditioning,
the specimens were kept in a water bath (at 25°C) for 2 h and then tested for their retained indirect
tensile strength. The Tensile Strength Ratio (TSR) evaluated using Eq. 1is given in Table 7.
T2
TSR (%) = × 100 (1)
T1
where T2 is ITS value of the conditioned specimen and T1 is ITS value of the unconditioned
specimen
Moisture damage resistance evaluated in terms of TSR was measured for CGBM and BC
mixes. The CGBM mix was found to have significantly better resistance to moisture damage as
compared to the bituminous concrete mix as shown in Table 7.
5.6. Durability
To check the durability of the two surface materials, the Cantabro Test was conducted using the
Los Angeles abrasion machine but without the charge (steel balls) as per ASTM D7064 (2013).
1706 G. Bharath et al.
BC 1 0.55 0.32
2 0.52 0.537 0.36 0.343 63.98
3 0.54 0.35
CGBM 1 1.79 1.70
2 1.75 1.797 1.62 1.657 92.21
3 1.85 1.65
This test was performed as an indicative measure just to aid and indirectly assess the cohesion,
bonding and effects of traffic abrasion (wear and tear) on the two distinct comparative mixes i.e.
the conventional BC and the CGBM. To perform this test, Marshall samples were conditioned
for 6 h at 25°C prior to abrasion. The loss in weight of the samples expressed as a percentage
of the initial weight is the indicative property for the abrasion loss caused due to wearing and
tearing action. The test results are given in Table 9. CGBM samples were found to be nearly 10
times more susceptible to abrasion loss in comparison to BC samples.
6. Field investigations
For the field performance study, CGBM resurfacing was laid on two test sections in the city of
Surat, Gujarat state, west coast of India with a length of 100 m each. The PG 64–22 (VG-30)
grade bitumen was used for the preparation of the mix for the test section. The existing bitumi-
nous surface was cleaned, and the emulsion was used for tack coat and 40 mm compacted hot
high void bituminous mix was laid using the paver. The bituminous mix was spread uniformly
and compacted after the selected compaction temperature range was reached. The paved bitumi-
nous mix was rolled with a 10-ton static steel wheel roller to obtain the target air voids. Once
the bituminous surface was cooled to ambient temperature, the required amount of cementitious
grout material mixed thoroughly with water was poured on the high void bituminous mix surface
and spread uniformly over the entire surface of the test section. Any excess grout observed on
the surface was removed and any unfilled air voids observed were again filled with grout. After
the grout was allowed to set for one day, the section was cured by sprinkling of water which was
repeated for 3 days. Various stages of CGBM construction in the field are shown in Figure 11 (a)
to (f). After the grout was set, cylindrical core samples of 100 mm diameter were extracted from
test sections to observe the extent of grout penetration and to measure the properties of the mix.
Road Materials and Pavement Design 1707
Figure 11. Stages of CGBM construction at field. (a) Brooming; (b) tack coat application; (c) laying
bituminous mix; (d) compaction of bituminous mix; (e) grout application and (f) finished surface.
All the cored specimens showed full depth grout penetration as can be seen in Figure 12 (a) and
12 (b). Measured strength parameters of the field core samples included Indirect Tensile Strength
(ITS) and Resilient Modulus (MR ). The results are given in Table 10.
In order to verify the actual field samples in terms of their volumetric analysis, the field core
samples were checked for their air void content. This analysis was done using the technique
called ‘Micro Computed Tomography’ or ‘Micro-CT’. The air voids in the field core sample
were found to be 3.16%. These remaining air voids relate to the closed voids in the bituminous
mix which were unable to be filled with the grout material. Micro-CT images of a field core
1708 G. Bharath et al.
sample showing the air voids as observed for the plan view and the side view are shown in
Figure 13 (a) and (b) respectively, wherein the blue coloured region indicates the isolated voids
and the other (yellow) coloured region indicates the inter-connected voids. Voids marked in blue
colour are significantly smaller in size in comparison to the voids marked in yellow colour, as
can be inferred from the legend mentioned in Figure 13.
Road Materials and Pavement Design 1709
Figure 13. Micro-CT image for the top and side views of field core samples.
For having a check on the field performance, regular site visits were made to the CGBM test
sections. No rutting has been observed in the field section even after 12 months (0.3msa). The
CGBM surface was also checked for its skid resistance using British Pendulum Tester (BPN
instrument) as per ASTM E303. The observed value of skid resistance as measured in terms of
BPN were 60 for wet condition and 70 for the dry condition. The permissible skid value for the
wet condition is 55 as suggested by Hosking, 1992. The skid resistance of the CGBM surface is
found to be adequately enough for the dry as well as wet conditions.
7. Concluding remarks
The main objective of the present study was to evaluate CGBM for its mechanistic properties
and performance in rutting, fatigue, moisture resistance and oil spillage resistance. The following
main issues were examined in the present study.
• Grouted mixes had significantly smaller rutting, nearly 1/10 times as compared to the
BC mix.
• CGBM had a Tensile Strength Ratio (TSR) value of 96% indicating significantly better
resistance to moisture induced damage in comparison to the BC mix having a TSR
value of 80%.
• CGBM mix shows approximately 3, 7 and 10 times higher value of resilient modulus
corresponding to test temperatures of 25, 35 and 45°C, when compared to the BC mix
at the same conditions. This trend shows lower temperature susceptibility of CGBM in
terms of Resilient Modulus, when compared to the BC mix. A similar trend is observed
for the Indirect Tensile Strength (ITS) of the CGBM with about 2.5 times higher values
than the BC mix.
• In terms of compressive strength and stability; CGBM shows respectively, approxi-
mately 6.5 and 2.75 times higher values in comparison to the BC mix.
• CGBM mix was found to be more resistant to the damaging effect of oil spillage than
the BC mix. The retained ITS value for CGBM mix immersed in diesel for 24 h was
92.21 percent against 63.98 percent for BC mixes.
• Dynamic moduli of CGBM specimens are substantially higher than those of BC mixes,
at all temperatures and frequencies.
• IDT test results show that CGBM is less fatigue resistant when compared with the
control BC mixture. The fracture energies for BC and CGBM mixes were 34.3 × 103
and 31.8 × 103 Nmm respectively.
• Air void content in the laboratory prepared CGBM (grouted) samples and the field core
CGBM samples were checked using Micro-CT technique and they were found to be
2.59% and 3.16% respectively.
• Full depth grouting was observed in the laboratory prepared samples and cores taken
from the trial section laid on the road. No rutting has been observed in the field trial
section even after 12 months (0.3 msa).
Acknowledgements
The Surat Municipal Corporation, Gujarat, India; Sardar Vallabhbhai National Institute of Technology,
Surat, Gujarat, India and M/s. International Combustion (India) Limited are thankfully acknowledged for
their help and support during laying of test section of CGBM.
Funding
This work was supported by Council of Scientific and Industrial Research [grant number FTT-MLP-0581].
Road Materials and Pavement Design 1711
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