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s40962-018-0214-7
s40962-018-0214-7
s40962-018-0214-7
M. Koru
Energy Systems Engineering, Süleyman Demirel University, Isparta, Turkey
O. Serçe
ORAU R&D Center, Orhan Automotive, Bursa, Turkey
Abstract
High-Pressure Die Casting (HPDC) is a near-net shape The experiments were repeated under 64 different condi-
manufacturing method for the non-ferrous materials cast- tions, using different dynamic and thermal parameters and
ing process, and it is widely used in the automotive vacuum application drawn in the mold cavity. The samples
industry. In the HPDC method, mold (TM) and casting obtained from the experiments were subjected to tensile
temperature (TC), first- (V1) and second (V2)-phase injec- tests to identify their mechanical properties. A gas pyc-
tion velocity, injection pressure (P3), mold and casting nometer was used to measure and calculate porosity rates.
material, mold design and vacuum application are all All the tests were simulated using FLOW-3D software
important parameters for producing high-quality products, proper to the experimental conditions. In conclusion, the
as they directly affect the mechanical and metallurgical most useful thermal parameters obtained from the experi-
properties and micro–macroporosity of the product parts. mental study were found to be 1063 K for casting tem-
In this study, the effects of thermal (mold and casting perature and 493 K for mold temperature, while the
temperature) injection parameters and dynamic (pressure, optimum dynamic parameter values were determined to be
velocity and vacuum application) injection parameters on 1.7 m/s injection velocity and 10–20 MPa injection pres-
the mechanical properties and porosity of the samples were sure for vacuum application drawn in the mold cavity.
studied. In the experiments and simulations performed as
part of this study, A383 was selected as the casting mate- Keywords: high-pressure die casting, porosity, thermal and
rial and DIN 1,2344 as the hot work tool steel. The mold dynamic parameters, vacuum application
cavity was shaped according to the tensile test specimen.
Introduction process takes place in three basic stages. First, the molten
metal is pushed at a low speed (0.3–1 m/s) toward the mold
High-Pressure Die Casting (HPDC) is a widely preferred cavity. It’s here that the second phase starts, where the
casting method in the production of non-ferrous light metal is filled into the mold cavity at a high speed (1–10 m/s).
metals requiring complex shapes and dimensional accu- In the final stage, the molten metal filling of the mold is
racy. HPDC is used to produce many automotive parts, solidified by being held under high pressure. After the
including pistons, gears, valves, gear boxes, suspension solidification is completed, the mold is opened and the
parts, and fasteners. Besides automotive parts, the HPDC ejector pins push the piece away to separate it from the
method can be applied for the manufacturing of lighting mold, bringing an end to the casting process.4 Although the
parts (armature covers) and telecommunication parts.1 HPDC method has a number of advantages, like high
With HPDC, magnesium and aluminum alloys are usually production speeds and suitability to mass production and
cast.2,3 The fundamental process involved in the HPDC production of complex geometric parts, it also has disad-
method is the transferring of molten metal to a mold cavity vantages, like porosity problems (macro and micro), front
at high speeds, where it solidifies under pressure. This meeting, adhesion, stratification, flaking, cave-in issues,
were designed taking into consideration the results of the The mold was designed to be suitable for obtaining a
FLOW-3D simulations and experiments. Figure 2 shows tensile test specimen and a cylindrical piece after the
details about the mold design and casting specimen. casting process. Ventilation channels, runner and vacuum
valve connection were determined for the tensile test
Figure 2. Parts used in experimental studies, gating and vacuum channels and
macrophotograph of the casting specimen.
The tensile test specimens were produced in accordance Filling results from the performed simulation showed that it com-
with TS EN ISO 6892-1 standards, and the tests were plied with the theories proposed by Frommer et al.36 As shown in
performed at room temperature at a pull speed of 0.3 mm/ Figure 4, the liquid metal is filled into the mold by flushing it
min using a universal tensile device. Tests were repeated at through the filling surface. The liquid metal continues to flow
least three times for each parameter. The mechanical tests through the mold cavity by creating severe turbulence. Some of the
were carried out to investigate the effects of mold tem- liquid metal flows upward along the inner surface of the mold, and
perature, casting temperature, injection pressure, second- the mold-filled flow energy continues until it naturally reaches its
phase velocity and vacuum application on the tensile and end, allowing all or nearly all the liquid metal to fill the mold cavity
yield strength. completely. The mold is completely filled in about 0.26 s,
depending on the specified injection parameters (Figure 4).
85.3 11.125 2.225 0.66 0.2605 0.233 0.0476 0.059 0.047 0.03 0.011 0.0089
The solidification steps carried out in the simulations are regions, followed by the tensile test specimen and the
presented in Figure 5. As can be seen from the simulation cylinder geometry. Lastly, the runner is solidified, marking
stages, solidification occurs immediately in the thin-walled the end of the solidification process.
Microporosity results were obtained as percentages from percentage results are given as the sum of the micro- and
the simulations performed in the experimental procedure macroporosities in the sample.
using FLOW-3D. Figure 6 shows a simulation example of
the microporosity obtained from the simulation program. A
significant amount of microporosity forms at the center of Results
the cylindrical geometry part, whereas the microporosity
formations on the drawing sample are distributed more Mechanical Test Results
heavily in the upper part, where air evacuation is made
(Figure 6). The microporosity results obtained for all test The yield and tensile strength test results of the tensile test
parameters are given in the ‘Findings’ section. specimens produced by the HPDC method under non-
vacuum conditions are presented in Table 2. Table 2 shows
In addition to the mechanical tests and simulations, the that the tensile strength was affected at relatively low
densities of the components were determined by means of a values by increasing the injection velocity from 1.7 to
Micromeritics Accupyc II 1340 gas pycnometer. For this 2.5 m/s under non-vacuum conditions. Increasing the
purpose, the mass values of the samples were at first injection speed shortens the fill time, but in some cases, it
measured using a sensitive scale, followed by the use of the caused the formation of porosity during the filling of the
gas pycnometer to obtain sample density values. After liquid metal into the mold and affected the mechanical
finding the density values, percent porosity values were properties negatively. Doubling the injection pressure can
calculated using Eqn. 1. diminish this effect. In other words, it would be better to
increase the pressure instead of increasing the injection
ðqobservable qtheoric Þ speed for the less complex parts. In the case of non-vacuum
%P ¼ 100 Eqn: 1
qtheoric conditions, the best tensile strength was obtained for
TC = 1063 K, TM = 553 K, P3 = 20 MPa and for both
In this equation, qobservable is the density value measured by injection velocities (1.7 and 2.5 m/s).
gas pycnometer (g/cm3), and qtheoric is the density value
obtained by pulverizing the sample and measuring it in the In looking at Table 3 and all the results it shows when there
gas pycnometer. Porosity percentage was calculated using is an increase in the injection rate of 32% for fixed mold
theoretical and apparent density values to determine the temperature and casting temperature values in the experi-
effects of thermal and dynamic casting parameters on ments performed under vacuum conditions, it can be seen
porosity. The experimentally determined porosity that the tensile strength results improved by around 2-5%,
983 373 153.16 155.92 158.61 156.92 126.34 130.58 134.43 132.18
1063 373 166.03 168.98 181.45 174.76 131.16 139.08 150.9 142.4
983 433 166.47 175.54 182.98 180.94 132.09 143.22 154.16 152.04
1063 433 171.02 174.47 176.58 182.57 135.1 139.36 146.65 155.79
983 493 172.69 180.63 182.65 184.97 136.7 145.92 151.09 152.15
1063 493 172.99 182.17 186.33 185.89 136.66 147.83 148.25 147.25
983 553 176.22 179.28 183.27 181.64 141.63 148.78 149.21 148.99
1063 553 179.62 180.7 189.95 190.29 143.4 145.75 150.56 153.59
Table 3. Tensile Strength and Yield Strength Results Under Vacuum Conditions
983 373 167.24 171.03 171.08 173.45 140.03 141.07 141.33 147.5
1063 373 166.22 175.77 177.85 190.22 135.52 140.59 143.52 157.59
983 433 169.89 177.26 184.22 187.26 133.54 145.14 149.23 158.26
1063 433 174.14 178.53 183.99 189.43 138.93 140.58 152.63 158.99
983 493 176.51 179.77 185.44 192.16 137.83 142.55 159.12 162.55
1063 493 177.34 184.31 187.34 191.94 138.55 145.78 160.3 164.86
983 553 203.4 190.19 194.24 195.15 167.64 163.03 165.28 167.66
1063 553 186.56 190.22 193.88 199.71 138.55 145.78 160.3 164.86
with the best results acquired at TC = 983 K, TM = 553 K, Figure 9 shows the tensile test results for the casting
V2 = 1.7 m/s and P3 = 10 MPa. Doubling the injection temperature at 983 K, in relation to different values of
pressure for constant values of mold temperature, casting mold temperature, injection pressure and injection velocity.
temperature and injection speed under vacuum conditions In the general evaluation made, a significant increase was
resulted in an increase in around 2–6% in strength and observed in the tensile strength results when the mold
2–4% in yield strength. When both Tables 2 and 3 are temperature was increased. At fixed injection speed and
considered together, the effect of mold temperature, casting pressure values and with an increase in the mold temper-
temperature and vacuum application is seen to have a ature from 373 to 553 K under vacuum conditions, tensile
greater impact on mechanical properties than other strength was observed to improve around 13–15%.
parameters. Taking all injection parameters into consider- Applying the vacuum to the mold cavity affected the ten-
ation, a vacuum application improved the tensile strength sile strength positively in accordance with the increase in
up to 14% and also improved yield strength by about the mold temperature.
8–15%.
Improvements in tensile strength by around 17–18% were
ANOVA results for tensile and yield strength were exam- observed when the mold temperature was increased in
ined and it was found that if P values were under 0.05 that experiments with fixed thermal and dynamic parameters
parameter was considered to be significant. When we under vacuum conditions. Taking into account all the
considered ANOVA results with tensile and yield results parameters for the 1063 K casting temperature, the appli-
together all of the casting parameters are significant for cation of vacuum to mold cavity served to improve tensile
mechanical properties. You can see the ANOVA results for strength by about 2–5% compared to non-vacuum condi-
tensile strength at Table 4 and Figure 7, and yield results in tions. By increasing the mold temperature, the effect of the
Table 5 and Figure 8. vacuum application was even more evident. In vacuum
applications to the mold cavity, lower injection dynamic
parameters should be selected to prevent the problems vacuum experiments improved the tensile strength values
caused by high pressure and velocities during operation of by about 1–7%. Similar results were obtained in vacuum
the system. applied conditions too. With vacuum application, tensile
strength improved by around 8%. In evaluating Figures 9
Figure 10 shows the tensile strength results obtained for the and 10 together, it was found that increasing the casting
tests conducted at the casting temperature of 1063 K. By temperature from 983 to 1063 K had only a minor effect on
increasing the casting temperature from 983 to 1063 K, the the tensile strength.
tensile strength results were less affected than when
changes were made to the mold temperature. Increasing the The changes in the yield strengths of the samples obtained
casting temperature by 373 K at constant dynamical by the HPDC method were also investigated in terms of
parameters and constant mold temperature values in non- different thermal and dynamic parameters. Figure 11 gives
the yield strength results obtained from experimental tests performed under the conditions of fixed thermal and
studies conducted on the impact of mold temperature, dynamic parameters with vacuum application. In looking at
injection pressure and injection velocity at 983 K casting the tests performed at all parameters for the 983 K casting
temperature. Yield strength results that were similar to temperature, it was seen that vacuum application improved
tensile strength results were obtained by increasing mold the yield strength by about 3–5% compared to non-vacuum
temperature. Increasing the mold temperature at constant conditions (Figure 11). When vacuum is applied to the
injection velocity and pressure values under non-vacuum mold cavity, there is an increase in the yield strength values
conditions improved yield strength values by around for almost all injection thermal and dynamic parameters.
9–12%. Improvement of the yield strength by 12–17% was At 373 and 553 K mold temperatures, the effect of vacuum
observed when the mold temperature was increased in the application on yield strength was more clearly evident.
Figure 12 gives the yield strength test results obtained for Density and Porosity Percent Values
the tests conducted at 780 K casting temperature. By
increasing the casting temperature from 983 to 1063 K, the Table 6 shows the results of density measurements made
yield strength results were less affected than when changes with gas pycnometer and Table 7 shows percent porosity
were made to the mold temperature. When the constant values based on density results.
dynamic parameters and mold temperature values are taken
into consideration in the experiments conducted under non- At Table 7 porosity calculated using density of the mate-
vacuum conditions, the yield strength improved by 1–9%. rial. Density of the material measured with gas pycnometer
A similar situation was seen in the experiments conducted (2.7312 g/cm3) and it is really close literature data for
under vacuum conditions; that is, a maximum of 10% A380 (2.74 g/cm3).37 When the results presented in
improvement was observed in yield strength values under Table 7 are examined, it can be clearly seen that the
vacuum conditions. amount of porosity decreases with vacuum application. The
983 373 2.6609 2.6341 2.6646 2.6513 2.6612 2.6896 2.6502 2.6526
1063 373 2.6351 2.6688 2.6759 2.6948 2.6972 2.6996 2.6953 2.6471
983 433 2.6856 2.6787 2.6741 2.6702 2.7114 2.7008 2.6871 2.6785
1063 433 2.6873 2.6681 2.6318 2.6027 2.7016 2.6597 2.6476 2.6536
983 493 2.6738 2.6203 2.6882 2.6735 2.6751 2.6640 2.6887 2.6813
1063 493 2.6848 2.6300 2.6443 2.6001 2.7125 2.6664 2.6864 2.6329
983 553 2.6761 2.6937 2.7050 2.6801 2.6855 2.6511 2.6627 2.6649
1063 553 2.6679 2.6919 2.6243 2.7031 2.6744 2.6461 2.6824 2.6912
Table 7. Calculated Percent Porosity Rate (qtheorical: 2.7312 g/cm3) Based on Density Results
983 373 2.5727 3.5546 2.4373 2.9248 2.5618 1.5219 2.9645 2.8779
1063 373 3.5168 2.2829 2.0248 1.3309 1.2449 1.1546 1.3120 3.0792
983 433 1.6696 1.9192 2.0907 2.2316 0.7225 1.1131 1.6147 1.9296
1063 433 1.6055 2.3103 3.6364 4.7025 1.0838 2.6167 3.0597 2.8400
983 493 2.0986 4.0599 1.5726 2.1108 2.0540 2.4605 1.5549 1.8246
1063 493 1.6964 3.7035 3.1787 4.7970 0.6847 2.3726 1.6391 3.5967
983 553 2.0156 1.3712 0.9581 1.8698 1.6733 2.9328 2.5056 2.4251
1063 553 2.3158 1.4365 3.9110 1.0289 2.0772 3.1134 1.7855 1.4646
decrease in the amount of porosity ranged between 30% the mold and the casting temperature increases, the cooling
and 75%. In examining the porosity in terms of injection becomes unbalanced, causing porosity formation.
velocity change, increasing the injection velocity at low
mold temperatures decreased the amount of porosity, while Table 8 gives the microporosity results obtained from the
the opposite was true when high mold temperatures were FLOW-3D simulation program. The table shows that
used, i.e., porosity increased. In terms of the injection increasing the mold and casting temperature leads to a
pressure, when the vacuum was not applied, the increase in decrease in the amount of porosity. Similarly, the table re-
the injection pressure caused a decrease in porosity per- veals that an increase in the second-phase velocity leads to
centage, whereas when the vacuum was applied, there was a decrease in the amount of porosity. The lowest amount of
a slight increase in porosity percentage. For vacuum porosity was determined when the mold temperature was at
applied conditions, the increase in mold temperature and 433 and 553 K. Moreover, when the mold and casting
pressure caused a decrease in the amount of porosity. temperature were higher, the vacuum application reduced
According to the data presented in Table 7, the best results the amount of porosity, but lower mold and casting tem-
based on a porosity percentage of around 72% were perature values increased porosity, even under vacuum
obtained using the following thermal and dynamic application. According to the simulation, when the best
parameters under vacuum application: TC = 983 K, parameters are selected, the amount of porosity can be
TM = 433 K, V2 = 1.7 m/s, and P3 = 10 Mpa. Again, for decreased by approximately 45%. Considering the casting
the same dynamic parameters and TC = 1063 K, temperature parameter alone (most of the time, this
TM = 553 K, the porosity result was around 0.68%. As can parameter had no effect on simulation results), porosity can
be clearly understood with this information, when the be decreased by around 22, 20% at best, considering the
casting temperature is increased, the mold temperature injection velocity parameter alone, and 15% at best, con-
must also be increased, because as the difference between sidering the injection pressure parameter alone. Therefore,
983 373 1.383 1.406 1.507 1.395 1.414 1.339 1.221 1.306
1063 373 1.368 1.406 1.507 1.395 1.414 1.339 1.221 1.306
983 433 1.333 1.069 1.19 1.028 1.237 1.237 1.313 1.018
1063 433 1.333 1.19 1.069 1.028 1.68 1.27 1.512 1.271
983 493 1.583 1.179 1.578 1.308 1.608 1.27 1.512 1.271
1063 493 1.583 1.179 1.578 1.308 1.237 1.156 1.341 1.018
983 553 1.144 1.065 1.257 1.08 1.266 1.069 1.218 0.978
1063 553 1.144 1.065 1.257 1.08 1.266 1.069 1.218 0.978
it can be said that mold temperature is the most influential percentage according to the simulation were obtained using
parameter for lowering porosity percentage. Table 9 and the following parameters with vacuum application:
Figure 13 show ANOVA results for calculated porosity P3 = 10 Mpa, TM = 433 K, TC = 1063 K, V2 = 1.7 m/s.
results and Table 10 and Figure 14 show it for simulated Comparing the simulation results with the experimental
porosity results. results, it was seen that only minor changes occurred in the
microporosity results by changing casting parameters in the
The best results for porosity percentage were obtained simulation. In addition, the porosity percentage for some
using the following parameters with vacuum application: parameters in the simulation results was well below that of
P3 = 20 Mpa, TM = 553 K, TC = 1063 K, and the experimental results. This could be attributed to the fact
V2 = 2.5 m/s. In contrast, the worst results for porosity that in the experimental studies both micro- and
macroporosity was summed up together. On the other hand, • During the filling of the mold cavity with
however, the simulation program showed better results aluminum alloys, turbulence and air gaps have a
when the injection velocity was higher, whereas the negative impact on the mechanical properties. For
experiments showed the opposite. this reason, mold design directly affects product
quality. In this study, analyses were performed
with the FLOW-3D program to ensure a good
Discussion and Conclusion mold design. Based on these analysis results and
field experience, the most suitable mold design
Aided by the studies found in the literature, the following was determined.
can serve as a general evaluation of the tensile strength, • Another factor that affects product quality is mold
yield strength and porosity results of the samples obtained temperature. When mold temperature increased,
from the high- pressure casting process: tensile strength increased by around 13–15%