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CTC4801 practical manual 2024
CTC4801 practical manual 2024
PRACTICAL MANUAL
UNISA
Compiled according to South African National
Standards
by
TABLE OF CONTENT
PREFACE ……………………………………………………….…………………………..3
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PRACTICAL MANUAL FOR CTC4801
PREFACE
This practical manual is for Concrete Technology Module (CTC4801). The module is
offered at the Department of Civil Engineering, University of South Africa for BEng
Tech (Hons), Structures. This module will assess ECSA graduate attribute 1: Identify,
formulate, analyse and solve complex problems creatively and innovatively. After the
practical session, you are expected to submit a practical report, where each test
performed will be reported.
Use the outline below to complete your practical report.
• Cover page
• Table of content
• Chapter one: Introduction
• Chapter two: Mortar Flexural strength
• Chapter three: Mortar Compressive strength
• Chapter four: Sieve analysis
• Chapter five: Bulk density
• Chapter six: Particle shape
• Chapter seven: Bulk relative density, Apparent relative density and Water
absorption
• Chapter eight: Concrete Mix design
• Chapter nine: Slump test
• Chapter ten: Concrete Compressive strength
• Chapter eleven: Concrete Split tensile strength
• References
The guidelines for each test are explained in the subsequent sessions of this manual.
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PRACTICAL MANUAL FOR CTC4801
1.2 APPARATUS
• Stainless steel mortar mixer
• Stainless steel mortar mixer frame
• 40 x 40 x 160 mm prism moulds
• Jolting (Vibration) apparatus
• Flexural strength testing machine
• Compressive strength testing machine
• Scoop
• Rubber or plastics scraper
• Curing tanks
• Impervious sheet
• Weighing balance
1.3 PROCEDURES
1.3.1 Batching
Use standard sand, cement that has been thoroughly mixed and potable water. The
standard sand is a natural siliceous sand consisting of rounded particles and has a
silica content of at least 98%. Batch mortar for three test specimens using 450 g of
cement, 1350 g of sand and 225 g of water.
1.3.2 Mixing
Mix the mortar in a laboratory mortar mixer, in such a manner as to avoid loss of
cement and water.
(a) Weigh the materials on the weighing balance
(b) Place the water and the cement in the mixer bowl and record the time water and
cement got in contact as the zero time.
(c) Start the mixer at low speed for 30s, then add sand steadily over the next 30s.
Switch the mixer to high speed and continue to mix for another 30s. Stop the mixer
for 90s, during this period use the rubber or plastic scraper to remove the mortar
adhering to the wall of the mixing bowl into the main mortar at the middle of the
mixing bowl. Continue to mix for the next 60s at high speed to complete the mixing.
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PRACTICAL MANUAL FOR CTC4801
(b) Scoop the mortar from the mixing bowl and place in into each mould compartment.
(c) Spread the mortar in the mould and vibrate on the vibrating table for 10 seconds.
Add another layer of mortar and vibrate for another 10 seconds.
(d) Strike off the excess mortar and level the mortar.
(d) Place an impervious sheet on the mould and place in a moist air room until its
appropriate time for demoulding.
1.3.4 Curing
(a) Demould the specimens and cure the specimens in water at 200C with a built-in
thermostat to maintain the temperature in the curing tank. Place the specimen on the
gratings and keep them apart to give allowance for the six faces to have access to
water.
(b) Remove the specimen for testing at the appropriate testing time.
1 .5 F . L
Rf = b3
where:
Rf is the flexural strength, in Newtons per square millimeter (N/mm2)
b is the side of the square section of the prism, in millimeters (mm)
F is the ultimate load applied to the middle of the prism at fracture, in Newton (N)
L is the distance between the supports, in millimeters (mm)
Use the following outline to complete chapter two: Mortar Flexural strength
• Title, objectives, apparatus and pictures
• Methodology
• Safety precautions
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PRACTICAL MANUAL FOR CTC4801
• Observations
• Results and calculations
• Discussion
• Conclusion
(d) Calculate the compressive strength (Rc) using the equation below or read it off
from the automated equipment.
Fc
Rc = A
where:
Rc is the compressive strength in N/mm2
Fc is the maximum load at fracture, in N
A is the area of the load bearing plates, in mm2
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PRACTICAL MANUAL FOR CTC4801
2.3 PROCEDURES
• Pour the field sample into a riffler pan. Then pour the material through the riffler
by slowly titling the pan so that the material flows in an even stream across its
width. At the same time, move the pan to and fro along the full length of the
riffler to ensure an even flow of the material. Repeat the process with the
contents of one of the pans under the riffler until a sample of the required size
is obtained. Use Table 2.1 as a guide.
Table 2.1: Size of the sample
1 2
Maximum particle size Approximate sample mass
Mm g
75 10 000
50 7 000
37.5 4 000
28 3 000
20 2 500
14 1 500
10 1 000
5 and smaller 500
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PRACTICAL MANUAL FOR CTC4801
• Place the test sample in a suitable container and add enough water to cover
the sample. Agitate thoroughly in the water to loses and dust particles adhering
to the aggregate and also to break down any clay lumps that may exist. Decant
the wash water over the 0.075 mm sieve protected by one or two coarser
sieves. The wash water containing the -0.075 mm material is discarded or
allowed to run away. Continue this washing until the water that passes through
the sieves is clear. Return all the material retained on the sieves to the container
by gentle and careful washing. Dry a test sample to constant mass at 105 to
110 °C in a well-ventilated oven.
• Sieve through the required or specified sieves in order of decreasing size from
to bottom into a pan (sieve sizes: 37.5 mm, 28mm, 20mm, 14mm, 10 mm, 7.1
mm, 5 mm, 2 mm, 1 mm, 0.6 mm, 0.3 mm, 0.15 mm, 0.075 mm and pan).
• Weigh the material retained on each sieve and record the mass to the nearest
0.1g.
PAN
Material
passing
0.075 by 17.5
washing (mass a-b) 3.5 - -
22.5
(mass a-b) +
Subtotal 2 (mass c) 4.5 - -
496.0
Total mass (mass of
of mass sample after
496.0 (g) test) 100 - -
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3.4 CALCULATIONS
Calculate the bulk density δ of the aggregate (compacted or uncompacted, as
appropriate), in kilograms per cubic metre, as follows:
𝑚
δ=
𝑣
Where:
m is the mass of the aggregate in the container, in kilograms;
V is the volume of the container, in cubic metres. Report the result to the nearest 10
kg/𝑚3 .
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PRACTICAL MANUAL FOR CTC4801
4.2 APPARATUS
• Test sieves (sizes: 37.5 mm, 28mm, 20mm, 14mm, 10 mm, 7.1 mm, 5 mm)
starting with the sieve that has the largest apertures.
• Flakiness gauge
• Electronic balance
4.3 PROCEDURES
• Carry out a grading analysis as described in SANS 3001-AG1, separating the
test sample into the relevant fractions
• Weigh each fraction to be gauged to the nearest 1g and record the mass (𝑀𝑆 ),
• Gauge all the particles in each fraction size (using corresponding slot),
contains the material that passes through the appropriate individual slots,
weigh to the nearest 1g and record the masses (𝑀𝑓 ).
• Calculate 𝑀𝑆 , the summation of all the fractions retained (gauged) and 𝑀𝐹 , the
summation of all the fractions passing the slots.
4.4 CALCULATIONS
Calculate the flakiness index of the sample to one decimal place as follows:
𝑀𝐹
𝐹𝐼 = 100
𝑀𝑆
𝑀𝐹 is the mass of all the fractions passing the slots, expressed in grams;
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PRACTICAL MANUAL FOR CTC4801
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PRACTICAL MANUAL FOR CTC4801
a) Bulk density;
b) Apparent density; and
c) Water absorption.
5.2 APPARATUS
• 5 mm sieve
• Riffler, with suitable openings larger than the largest particle in the sample, and
at least three pans.
• Weighing balance, fine measurement type that complies with SANS 1649, and
with a capacity of at least 12 kg, and reading to 0.1 g.
• Wire basket, approximately 200 mm in diameter and 200 mm in height,
manufacture from mesh with 1 mm to 3 mm apertures.
• Container, filled with water at temperature of between 24 ℃ and 26 ℃, suitable
for immersing the wire basket containing the test sample.
• Cloth, of chamois leather approximately 750 mm x 750 mm in size.
• Drying oven, that is capable of maintaining a temperature range of between
105 ℃ and 110 ℃, with continuous draft.
• Thermometer, capable of covering the temperature range 0 ℃ to 100 ℃, and
reading to 1℃
5.3 PROCEDURES
• Pour the field sample into a riffler pan. Then pour the material through the riffler
by slowly titling the pan so that the material flows in an even stream across its
width. At the same time, move the pan to and fro along the full length of the
riffler to ensure an even flow of the material. Repeat the process with the
contents of one of the pans under the riffler until a sample of the required size
is obtained.
• Screen the sample on the 5mm sieve. Retain the material that does not pass
that sieve.
• Thoroughly wash the test sample retained on a 5mm sieve so as to remove
dust from the surface of the particle, and soak for 24 h± 1 in water.
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PRACTICAL MANUAL FOR CTC4801
• Remove the sample from the water, drain off the free water for few seconds
and transfer it to the cloth.
• Roll the material in the cloth until all visible water has been absorbed by the
cloth. The saturated surface-dry condition has been reached when the cloth
has absorbed all visible water, but the surface of the particle still appear damp.
Large particles may be surfaced-dried individually using the cloth.
• Immediately weigh the test sample and record the mass, B, to the nearest 0,1
g. Use Table 5.1 as a guide. Transfer the test sample to the wire basket that
has been tared.
• Completely submerge the wire basket with the test sample in the container of
water at a temperature of between 24 and 26 ℃, taking care that no air bubbles
are entrapped. Weigh the wire basket and test sample in the water and record
the mass, C, to the nearest 0,1 g.
• Remove the sample from the wire basket, allow free water to drain off and then
dry it to a constant mass in the oven at a temperature of between 105 ℃ to 110
℃.
• Determine the mass of the oven-dried test sample, A, to the nearest 0,1 g.
5.4 CALCULATIONS
5.1 Determine the bulk relative density (BD), the apparent density (AD) and the
water absorption of the test sample given in 3.1.1, 3.1.2 and 3.1.3, respectively.
5.4.1 Determine the Bulk Relative Density, using the following equation:
𝐴
BRD = ( )
(𝐵−𝐶)
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PRACTICAL MANUAL FOR CTC4801
𝐴
ARD = ( )
(𝐴−𝐶)
5.4.3 Determine the water absorption as the loss in mass between the saturated
surface-dry and the oven-dry conditions of the oven-dried mass of the test sample, to
one decimal place, using the following equation:
𝐵−𝐴
𝑊𝐴𝐵𝑆 = 100 x ( )
𝐴
where
𝑊𝐴𝐵𝑆 is the water absorption of the test sample, expressed as a percentage (%).
5.5 Report deliverable bulk relative density, apparent relative density and water
absorption
Use the following outline to complete chapter seven: Bulk relative density, Apparent
relative density and Water absorption
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PRACTICAL MANUAL FOR CTC4801
6.2 PROCEDURES
Procedures and calculations are done according to the C&CI design method (chapter
11 of Fulton’s concrete technology, 9th edition).
The following steps summarise the procedure to follow when designing a mix using
the C & CI method:
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PRACTICAL MANUAL FOR CTC4801
Using,
cement sand stone water
1m 3 = + + +
( RDx1000) ( RDx1000) ( RDx1000) ( RDx1000)
• Make the trial mix
• Measure slump
• Assess stone content and cohesiveness of concrete
• Approve mix if okay
• Reject mix if not okay
• Modify design if necessary
• Specify mix proportions for manufacture of concrete
Calculate the batch weight required for 20 L of trial mix based on the mix design
tables provided below.
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PRACTICAL MANUAL FOR CTC4801
Approx. Compaction K
slump Nominal maximum size of stone, mm
range, mm 9.5 13.2 19.0 26.5
75 – 150 Hand compaction 0.75 0.84 0.94 1.00
25 – 100 Moderate 0.80 0.90 1.00 1.06
compaction
0 – 25 Heavy vibration 1.00 1.05 1.08 1.10
Note: Calculating the batch mix is the same as the designing of the mix.
Solution
Determine the cement content
Cement content = water content/water:cement ratio
= 210/0.6 =350kg/m3
Determine the stone content (S) = CBD(k – 0.1 FM)
k from table is 1.0
S = 1550(1.0 - 0.1 x 2.3) = 1193.5 kg/m3 (Say 1194 kg/m3)
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7.2 APPARATUS
Mould in the form of a frustum of a cone (Figure 7.1), with the following nominal
internal dimensions:
a) Diameter of base: 200 mm ± 2 mm;
b) Diameter of top: 100 mm ± 2 mm; and c) Height: 300 mm ± 2 mm
c) Height: 300 mm ± 2 mm
7.3 PROCEDURES
• Ensure that the interior surface of the mould is clean and damp.
• Place the mould on a clean, smooth, horizontal, rigid and non-absorbent
surface that is free from vibration and shock. While the mould is being filled,
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PRACTICAL MANUAL FOR CTC4801
hold it firmly in place by standing on the foot pieces or by any other suitable
means.
• Fill the mould with concrete in three layers, each layer being approximately one-
third of the height of the mould.
• Tamp each layer with 25 strokes applied with the hemispherical end of the
tamping rod, distributing the strokes uniformly over the cross-section of the
layer and throughout its depth, ensuring that when the second and third layers
are being tamped, the strokes penetrate into the underlying layer.
• While tamping the third layer, ensure that excess concrete is maintained above
the top of the mould, if necessary, by adding more concrete while tamping.
• Strike off the excess concrete, using a sawing and rolling motion of the tamping
rod.
• Clean off any concrete that may have leaked or spilled around the base of the
mould during the tamping.
• Demould the concrete by slowly and carefully raising the mould vertically, taking
5 to 10 s to do this.
• The entire process of moulding and demoulding should be carried out within
150 s.
• Immediately after demoulding, measure the slump of the concrete to the
nearest 5 mm by determining the difference between the height of the mould
and the highest point of the specimen under test. If the specimen collapses or
if lateral shearing of concrete occurs, consider the test invalid and repeat it on
a fresh sample of concrete. If, during two consecutive tests, collapsing or lateral
shearing of the test specimen occurs, the concrete lacks the necessary
plasticity and cohesiveness for the slump test to be applicable.
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PRACTICAL MANUAL FOR CTC4801
8.2 APPARATUS
• Concrete mixer
• Shovel
• Compressive testing machine
• Cube moulds
• Steel float
• Vibrating table
• Scoop
• Curing tanks
• Impervious sheet
8.3 PROCEDURES
8.3.1 Batching
Use aggregate that has been oven-dried or air-dried, cement that has been thoroughly
mixed and potable water. The aggregate for each batch of concrete may be added
either in separate size fractions or with an all-in grading.
8.3.2 Mixing
Mix the concrete in a laboratory mixer, in such a manner as to avoid loss of water or
other materials.
(a) Load the mixer with approximately half of the coarse aggregate, then with the
cement, then with the fine aggregate, then with the rest of the coarse aggregate, and
always in such a way as to prevent loss of material. Mix the dry materials for not longer
than 30 s, and finally add the water slowly.
(b) Continue the mixing until the concrete is uniform in appearance, but in any case,
for a period of not less than 2 min and not more than 3 min after all the materials have
been loaded in the mixer.
(c) After machine mixing, rework the concrete with a trowel to ensure that any mortar
or fine material sticking to the pan of the mixer is worked into the concrete mass.
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PRACTICAL MANUAL FOR CTC4801
8.3.4 Curing
Cover the specimens (as marked in their moulds) with an impervious sheet and then
store them in a place that is free from vibration and in an atmosphere with a relative
humidity of at least 90% and at a temperature of 22 to 25 °C for 20 to 24 h after the
time of the addition of water to the dry ingredients. Demould the specimens and
submerge them, until just prior to testing, in potable water that is maintained at a
temperature of 22 to 25 °C. Ensure that specimens do not become dry at any time
before testing.
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PRACTICAL MANUAL FOR CTC4801
2P
F =
.a 2
where:
F = tensile strength (N/mm2)
P = compressive load at fracture (N)
a= size of cube (mm)
Calculate and record the average results to the nearest 0.05 MPa
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PRACTICAL MANUAL FOR CTC4801
REFERENCES
SANS 50196-1:2006: Methods of testing cement: Part 1- Determination of strength
SANS 3001-AG1: Civil engineering test methods: PartAG1: Particle size analysis of
aggregates
SANS 5845:2006: Bulk densities and voids content of aggregates
SANS 5847:2008: Flakiness index of coarse aggregates
SANS 3001-AG4:2015: Civil engineering test methods: PartAG4: Determination of
flakiness index of coarse aggregate
SANS 3001-AG20:2011: Civil engineering test methods: PartAG20: Determination of
the bulk density, apparent density and water absorption of aggregate particles retained
on the 5 mm sieve for road construction materials
Fulton’s concrete technology 9th edition, Chapter 11: Concrete mix design. Edited by
Gill Owens. ISBN: 978-0-9584779-1-8
SANS 5862-1:2006: Concrete tests – Consistence of freshly mixed concrete – Slump
test
SANS 5861-1:2006: Concrete tests: Part 1- Mixing fresh concrete in the laboratory
SANS 5861-3:2006: Concrete tests: Part 3 – Making and curing of test specimens
SANS 5863:2006: Concrete tests – Compressive strength of hardened concrete
SANS 6253:2006: Concrete tests – Tensile splitting strength of concrete
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