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NASA Technical Memorandum 106625

AIAA-94-3259

Experimental Results of Hydrogen Slosh in a


62 Cubic Foot (1750 Liter) Tank

Matthew E. Moran, Nancy B. McNelis, and Maureen T. Kudlac


Lewis Research Center
Cleveland, Ohio

Mark S. Haberbusch
Ohio Aerospace Institute
Brook Park, Ohio

and

George A. Satomino
Sverdrup Technology
Sandusky, Ohio

Prepared for the


30th Joint Propulsion Conference
cosponsored by AIAA, ASME, SAE, and ASEE
Indianapolis, Indiana, June 27-29, 1994


National Aeronautics and
Space Administration
EXPERIMENTAL RESULTS OF HYDROGEN SLOSH IN A 62 CUBIC FOOT (1750 LITER) TANK
Matthew E. Moran, Nancy B. McNelis, and Maureen T. Kudlac
National Aeronautics and Space Administration
Lewis Research Center
Cleveland, Ohio 44135
and
Mark S. Haberbusch
Ohio Aerospace fustitute
Brook Park, Ohio 44142
and
George A. Satornino
Sverdrup Technology, Inc.
Sandusky, Ohio 44870

Abstract nonexistent. Yet the availability of such data is crucial to


characterizing the underlying phenomena driving the
Extensive slosh testing with liquid and slush thermodynamic response of a liquid or slush hydrogen
hydrogen was conducted in a 62 cubic foot spherical tank propellant tank. The evolution of accurate simulation
to characterize the thermodynamic response of the system capabilities will also rely heavily on experimental
under normal gravity conditions. Slosh frequency and databases for verification. These capabilities support not
amplitude, pressurant type, ramp pressure, and ullage only the NASP program, but potentially all launcblspace
volume were parametrically varied to assess the effect of vehicles utilizing subcritical or subcooled cryogenic
each of these parameters on the tank pressure and propellants . Furthermore, the significance of
fluid/wall temperatures. A total of 91 liquid hydrogen, thermodynamic slosh effects become ever more important
and 62 slush hydrogen slosh tests were completed. Both as future mission profIles result in greater bulk fluid
closed tank tests and expUlsions during sloshing were motion (e.g. longer coasts under low gravity conditions,
performed. This report presents and discusses highlights more abrupt vehicle maneuvers, and partial rotations of
of the liquid hydrogen closed tank results in detail, and the propellant tanks). Under these situations, complex
introduces. some general trends for the slush hydrogen fluid dynamics of the liquid cryogen primarily dictate the
tests . Summary comparisons between liquid and slush transient thermodynamic response within the propellant
hydrogen slosh results are also presented. tank. Therefore, computational fluid dynamic techniques,
coupled to interfacial heat and mass transfer algorithms,
Introduction will likely be necessary to accurately predict pressure and
temperature conditions. To the authors' knowledge, this
A critical concern for the National Aero-Space Plane analytical capability does not presently exist
(NASP) development is the thermodynamic response of
the slusblliquid hydrogen propellant tank under sloshing In order to investigate slosh and other operational
conditions. Sloshing is expected to occur during vehicle issues associated with slush hydrogen handling aboard the
taxi, takeoff, and flight maneuvers. Fluid motion NASP, a test program was undertaken at the NASA Lewis
produced during these operations can circulate subcooled Research Center's K-site facility located at the Plum
hydrogen near the liquid-vapor interface resulting in Brook Station. The tests were performed in a spherical
increased condensation and corresponding pressure tank containing slush management and measurement
collapse. Conversely, liquid contact on hot tank walls components. Results of the liquid hydrogen slosh tests,
caused by sloshing can result in rapid vaporization and and general trends with slush hydrogen, are the focus of
subsequent rapid pressure rise. It is essential that both this paper. The test series was funded by the United
scenarios are predictable and controllable in order to insure States NASP program, Joint Propulsion Office, Wright-
safe and reliable operation of the NASP vehicle. Patterson Air Force Base.

Experimental data in the open literature on the E~rimental Ri2 Description


thermodynamic effects of liquid hydrogen slosh is quite
limited. Open literature data on slush hydrogen slosh is The K-site test facility is designed for large scale
testing with liquid hydrogen. Slush hydrogen production
Copyright © 1994 by the American Institute of Aeronautics and
Astronautics, Inc. No copyright is asserted in the United States
and test capability was added to the facility in 1990. K-
under Title 17, U.S. Code. The U.S. Government has a royalty- site is believed to be the only currently operational slush
free license to exercise all rights under the copyright claimed hydrogen facility in the United States. For this test
herein for Governmental purposes . All other rights are reserved series, a three shift per day operation was conducted, with
by the copyright owner. research tests conducted during two of the shifts.

1
Operation, control and data acquisition is performed silicon diodes for temperature sensing on the tank walls
remotely in a control room located approximately 540 feet and internally; thermocouples for some fluid stream
from the test building. Cryogen and gas facility temperatures; pressure transducers; liquid level probe;
storage/delivery capacities are: 26,000 gal. LH 2; 24,500 vapor-liquid point sensors; measured mass flowrate of
gal. LN2 ; 250,000 scf GHe and GN2 each; and 140,000 pressurant and propellant streams; and a densimeter for
scf GH 2 . Pressurant gas can be thermally conditioned solid fraction measurement of slush hydrogen.
using steam, liquid nitrogen, andlor liquid hydrogen heat
exchangers. Subatmospheric conditions within the test The internal silicon diodes are mounted to an
tank are achieved through the low pressure vent system instrument tree, and provide an indication of both axial
using a single-stage vacuum pump. A sketch of the test and radial temperature distributions in the tank. External
tank internals and instrumentation used for the slosh tests tank diodes are mounted directly to the tank wall.
is shown in Fig. 1. Accuracy of the diodes at liquid hydrogen temperatures is
approximately ±l oR. Silicon diodes are also utilized as
Test Tank and Vacuum Chamber vapor-liquid sensors by using overcurrent to induce self
heating. Type E thermocouples provide fluid stream and
The aluminum test tank is mounted inside a 25 foot other system temperatures at ±20R.
diameter stainless steel vacuum chamber which maintains
a nominal vacuum range of 10-6 torr during testing (10- 7 Liquid level is measured by a capacitance-type probe
torr empty) via four diffusion pumps upstream of four which was specially designed in-house for use in liquid
more vacuum pumps. Some of the K-site test crew and slush hydrogen. The readings from the probe are
standing ill, and in front of, the vacuum chamber are compensated for pressure and temperature (due to changes
shown in Fig. 2. The test tank is visible near the center in fluid dielectric constant) in the data acquisition
of the photograph, mounted from four flexure straps. software. In situ accuracy of the probe was found to be
Around the perimeter of the vacuum chamber are the bolts nominally ± 0.25 inches when compared to the vapor-
used to secure the 20 foot diameter chamber door prior to liquid point sensors.
pulling a vacuum. At the far left of the photo are the
hinges which support the chamber door. The grating Pressurant mass flowrate is measured using orifices
inside the vacuum chamber provides access to the tank and coupled to temperature and pressure data with a calculated
does not interfere with the sloshing motion. uncertainty of ±0.00012 lbm/s. Strain gauge type
pressure transducers measure various system pressures to
Slosh is produced by a shaker mechanism capable of within ±0.5% full scale.
six inches of total displacement at a frequency of one
Hertz. The sloshing system shaft penetration at the rear The data acquisition and display system is controlled
of the vacuum chamber is shown in Fig. 3. The sbaft by a local minicomputer with 512 data channels available;
translates along a roller support (near the center of the recorded data is eventually uploaded to a mainframe system
photograph), and mounts to the test tank support structure located at Lewis for data reduction. Nominal sample rates
at the far left. Also visible at the extreme left of the are once per second, with the capability of ten times per
photograph is one of the stainless steel flexure straps. second. Several displays throughout the control room
show operational and researcb data in real time during
The test tank is shown in Fig. 4 from the front of the testing.
chamber, near the opening. Visible in the photograph is
the support structure and tank externals. The tank lid is Test Procedure
constructed of stainless steel, while the remainder of the
tank is aluminum. Steady state environmental heat leak For the closed tank slosh tests (Le. no pressurant
into the tank is 0.3 Btu/s. At the middle left of the inflow nor propellant outflow during sloshing) the test
pboto, on the upper hemisphere of the tank, is the view tank is filled to the desired level with either liquid or slush
port and video camera assembly protected by a long hydrogen, and then vented to approximately 1 atm if
cylindrical cannister. The video camera records the necessary. The pressurization gas temperature is then
internal tank conditions through the viewing port, which preconditioned using the liquid hydrogen andlor liquid
nitrogen beat excbanger(s). If the test fluid is slush
is approximately 60 degrees above the tank midline, and
hydrogen, the propeller mixer is turned on to promote
40 degrees left of the sloshing system shaft axis, from an
uniform solid fraction, and the propellant density is
observation point directly at the chamber opening. measured after the mixer is off. With the temperature of
the pressurization gas conditioned, the tank is pressurized
Instrmnentation and Data Acquisition with either hydrogen or helium to the desired tank
pressure. After stopping pressurant flow and clOSing the
Test tank instrumentation includes (refer to Fig. I): vent valve, sbaking is initiated at the preset frequency, and

2
Fig. 3. Photograph of the shaker shaft
Fig. 1. Sketch of the test tank internals and
instrumentation

Fig. 2. Photograph of the vacuum chamber Fig. 4. Photograph of the test tank installed in the
vacuum chamber

~
3
the amplitude is increased to the desired value. The test temperature distribution prior to ramp pressurization is
amplitude is reached in approximately 10 to 30 seconds. given by the circle symbols and solid line. Liquid level
Shaking is maintained for a minimum of two minutes within the tank: is also indicated in Fig. 7.
after reaching the desired frequency and amplitude at which
time the test is terminated.
6"
w 0.08
Results and Discussion
~m 0.07
RAMP HOLD
SLOSH
::::!-
In a typical slosh test, the tank: pressure is ramped w 0.06 0

from near atmospheric pressure to either 20 or 35 psia,


with either gaseous hydrogen or helium pressurant. A
~ O.OS 0
0
o~
00 0
UQUID HYDROGEN SLOSH
HYCfK>GEN PRESSURANT
brief hold phase follows where the tank: pressure is held ~u. 0.04
0
0 SHAKER: 0.74 HZ; ±1.S'
35% ULLAGE VOLUME
constant, after which the preSSurization valve is closed and ..... 0 .03
z 0 TEST RDG #870
shaking is initiated. The amplitude is gradually increased
~ 0.02 0
to the final setting in approximately 10 to 30 seconds. :J
en 0.01 ~.
For many of the large amplitude tests (i.e. 0.74 Hz, ±1.5 en 0
<&Poo
w
inches) a sudden change in the slope of the pressure curve a: o
c..
is evident when the desired amplitude is reached. An o 50 100 150 200
example of the pressure response for one such test is TIME (SEC)
shown in Fig. 5. Tank pressure response for closed tank:
slosh tests with non-heated walls ranged from complete Fig. 6. Injected pressurant mass flow as a function of
pressure collapse to a mild pressure rise, depending on time for a liquid hydrogen slosh test.
experimental conditions.

Initially, large thermal stratification generally exists


40 in the ullage. Fluid temperatures after the ramp
RAMP HOLD
SLOSH
pressurization phase are denoted by the square symbols and
<' 3S the large-dash line. A temperature rise in the ullage is
en 0
0 ~ evident as a result of the addition of pressurant gas, and
e:- 30 0
0 UQUID HYDROGEN SLOSH
w 0
HYDROGEN PRESSURANT the subsequent increase in tank pressure. Final fluid
a: 0 0
:J 0 SHAKER: 0.74 HZ; ±1 .S' temperatures following slosh are shown with the triangle
en 2S 0 0
en 0 0 36% ULLAGE VOLUME symbols and short-dash line. The temperature profile after
w TEST RDG #870
a: 0
slosh depends on the experimental conditions, ranging
c.. 20 0
0

~
z 0
0
from a high degree of ullage thermal stratification to near
~ 1S !6 equilibrium conditions.

10
o so 100 1S0 200
60
TIME (SEC)
(j)
w
I
50 ··············j·····:;:.a-<~:::::··~·T ···········r··············-r···
Fig. 5. Pressure response for a liquid hydrogen slosh test. 0
z
f-
40
... . . . . :r·············+····:::·:ar·-·-··~·~;~~;·~··············
... ~·~-:-i."""!::~
I
(!J
30 1-..-......,j ....-...-....,g
L-...-....-...-.....;.
L-....-...-....-... LEVEL ...............
For the closed tank: tests, the pressurant mass flow' is W
nonzero through the ramp and hold phases, and goes to
I
-1
«
;i i i
20 ---.---- - .. ~.-- - -- ..---.....~ -- ... ----.. ---.i-... --•...... --.( ..•... --......--;.----------... .
zero when the tank: is locked up (closed) prior to initiating 0
f= : : -0- INITIAL
slosh. The pressurant injection mass flow as a function a:
w 1 0 ......... 7..;··············) ········· -0- AFTER RAMP
of time for the same test is given in Fig. 6. >
O~~~~~~~~~~~=+
.i i . n-. FINAL (RDG #870)

Figure 7 illustrates the thermal response inside the 30 40 50 60 70 80 90


tank during the same slosh test. Fluid temperatures are FLUID TEMPERATURE (R)
given as a function of vertical height, where the internal
top of the tank: is approximately 57 inches. Straight lines Fig. 7 . Fluid temperature distributions (liquid and
are drawn between sensor points (denoted by plot vapor): initially; after ramp pressurization; and
symbols) to aid interpretation, but do not necessarily after sloshing ("final").
imply linear temperature distributions. Initial fluid

4
- -_ .

Tank wall temperatures are given as a function of given by,


height for the same test in Fig. 8, where the external
height of the tank is 58 inches. The same symbol and line p-p .
conventions used for the fluid temperature plot is also %Collapse = ; _P~~ (100%) (1)
r mIt
used for the tank wall temperature plot. Initially, the tank
wall tends to mirror the temperature distribution trends
where: Pr = ramp pressure
evident in the fluid region. Some of the energy added to
Pmin= minimum pressure during
the system during ramp pressurization is transferred to the
slosh
wall as evidenced by a slight increase in wall temperatures
Pinit = initial pressure before ramp
for the "after ramp" case. The fmal wall temperature
proftle depends on the experimental conditions, although
Therefore, a collapse value of 100% would indicate
in all cases the upper portions of the wall remain
saturation conditions (at the initial tank pressure) exist
thermally stratified due to the mass of the lid and the
after sloshing. The maximum slope of the pressure curve
numerous piping and electrical penetrations (i.e. heat leak
(i.e. dP/dt) is also given in the table, where a positive
paths).
value indicates pressure rise. Finally, the test reading
numbers are assigned by the data acquisition system in
historical order and are unique to a specific test run.
60

t~~~~~E Il
en
w 50
Frequency and Amplitude
I
()
z
= 40 ,:.=.
. .(J : : LIQUID :
Two frequency and amplitude shaker settings were
chosen for this test series: one in the stable slosh region,
l-

. '~ 'r' ~-··"'·-··-··-··""1


I
C9 30 and one in the unstable (near resonance) region. To
W
I establish these regions, the natural frequency for a
--l
« 20 ......... ".............•.............•.
()
~~ .......
~ .........
~.......>~~:t spherical tank partially filled with liquid was found from
F ,: : : -0- INITIAL (Stofan and Armstead)l,
a: 10 .. : : -0- AFTER RAMP
w
> .........T·········T············r.. -c-- FINAL (RDG #870)

0~~~~+:~~: ~~~~F=~ (2)


30 40 50 60 70 80 90 100
WALL TEMPERATURE (R)
where: ron = natural frequency
g = gravitational acceleration
Fig . 8. Tank wall temperature distributions: initially;
after ramp pressurization; and after sloshing R = tank radius
("fmal''). A. = empirical constant based on
liquid height and tank radius
(see Tablem
Summary test conditions for selected closed tank
liquid hydrogen slosh tests are shown in Table 1. Missing
values (denoted by "-") indicate data that was not properly
Using the calculated natural frequency, stability
recorded for that test run; "n/a" is listed for parameters that
boundaries for both planar and nonplanar motion can be
do not pertain to that particular test (i.e. pressure rise
estimated from another experimentally derived relation
occurred during slosh). The table is sorted by the
(Sumner)2:
following test parameters (in order of priority) to facilitate
interpretation of trends: shaker frequency and amplitude
setting; pressurant type; ramp pressure; and ullage
volume. (3)

The ullage volume shown in the table indicates the


percentage of the total tank volume which is occupied by where: ~ = excitation frequency
gas. Pressurant temperature is a time-weighted average Xo = excitation amplitude
(i.e. not weighted for mass flowrate); instantaneous values Kl,2 = empiricaIconstants
fluctuated less than 25°R during the ramp and hold
pressurization phases unless otherwise noted. The (see Fig. 9)
pressure collapse values are a measure of the degree of
saturation in the tank resulting from the slosh, and are

5
---. --

Table II. Values for Constant in Eqn. (2)1 provide the desired liquid response for ullage volumes
between 15% and 50%, as indicated in Fig. 10. The
nonplanar stability limit establishes the boundary where
h/2R
rotary slosh becomes unstable (to the left of the limit
0.1 1.0573 line). Similarly, the upper and lower planar stability
limits defme the region where wave motion parallel to the
0.2 1.0938 excitation axis becomes unstable (within the limit lines).
Superposition of these regions defines areas of stable and
. 0.3 1.1370 unstable slosh, wbere stability is defmed as a steady state
harmonic slosh response.
0.4 1.1893

0.5 1.2540
0.74 Hz; :t 1.5 "
0.6 1.3376 NON PlANAR lJ'PER

0.8 1.4528 1.5 e


I STABIUTY
UMIT

PLANAR
STABILITY
UMIT
1!!JQ:!J~V&.!NJf1~ :
0.9 1.9770 [}iJ~@O@Q:!J
••
X0 •••
(:tinch) •
I
I
LONER
• ~il&'@Jfb~

-
PLANAR I

l~ 0 .5 STABILITY I
I
• ~ [}iJ~@O@Q:!J
UMIT I
1)0." ...... ~j 0.95 Hz; :to.5"
loo ~ O~~~~~~~~~~~~~~~~
~ [)"'"
0 .6 0.8 1 .2 1.4 1.6 1.8
K} . 96
r\ (ro lro )2
o '1

.92 \ (a) 15% ullage


\
~ 2~~~~~~~~~~~~~
.88 1!!JQ:!J~il&'@Jf1~ : R • 2.45 It
I UPPER hl2R • O.SO
[}iJ~@O@Q:!J : PLANAR ..J)..= 12540
-20 20 1.5 __ e: STABIUTY CD =O.72HZ
I I I I I I .14 Hz; :t1.5": LIMIT
f...-~

-'
N
-16 ..
~
-' N
6f...-~
0
Stlbilfty boundary
Pllnlr. lower limit
Xo
NON PlANAR
STABILITY
LIMIT
!

~... E~ (:tlnch)

. -12
=... c-.. f...-
12 f...-
0
<>
Pllnlr. upper limit
Nonpllnlr
J
LONER
PLANAR

l'gE STABILITY
~
..
~ 1 0 .5 LIMIT
/e
~
c!

E
-8
c!1i
-
.. c:
~g.
.. 8
))
fl V-
O~~~~~~~~~~~~~~~~
0.95 Hz; :to.5"

..
lIi
c:
ii: -4
:;~
..
c
4 Il?'
0.6 0 .8 1 .2
(ro lro )
2
1.4 1.6 1.8

-
ii: ~~ o '1
a (b) 50% ullage
0
0 .2 .4 .6 .1 1.0
Uqulct-~th rltlo. hID
Fig. 10. Slosh stability map for two ullage volumes;
Ib) Vllues 01 constant K2. and chosen shaker settings.

Fig. 9. Values of constants for eqn. (3)2


Considerably less pressure decay is observed for the
low amplitude slosh setting (0.95 Hz, ±OS') as compared
Equations (2) and (3) were used to construct slosh to the high amplitude setting (0.74 Hz, ±1.5"). An
stability maps for the test tank as a function of slosh example of the difference in pressure response is shown in
amplitude and frequency, and ullage volume (i.e. liquid Fig. 11 for two tests with all other test parameters beld
height). Using these maps, a setting of 0.95 Hz, ±0.5 constant. Examination of the fluid temperature data and
inches was chosen for stable slosh, and 0.74 Hz, ±1.5 video recordings indicate that the high amplitude, unstable
inches was chosen for unstable slosh. These settings slosh causes significant circulation of the subcooled bulk

7
liquid toward the interface. This circulation results in Note that no purges were performed between helium
increased condensation at the interface, and a ramp tests. Therefore, the initial quantity of gaseous
correspondingly larger pressure drop in the ullage for this helium in the ullage is generally unknown. For this
slosh setting. reason, comparisons of pressure response among helium
pressurant tests must be made cautiously; general
comparisons between helium and gaseous hydrogen
40 pressurant tests, however, are valid. Also, note that
average pressurant temperatures vary greatly among some
;? 35 : ~···· · ·······:··············· ("· ·· ········ ·t·········· .....j............. tests depending on the conditioning heat exchanger(s) used
(j) (e.g. liquid nitrogen or liquid nitrogen and liquid
e:-
UJ
30 .. ······-·-1··1···········~---··--·-··-···l···-·-·-·······1--············ hydrogen).
a:
::>
l: . . .
(f)
: . - 0 .95 Hz; ±C .5 ' (RDG 869)
(f)
25 · ·· ··-··-··~··- T ·····
Ullage Volume
UJ : I ---·0 .74 Hz; ±1 .5' (RDG 870)
a: l: ~, .: .: .: .:
0.. 20 • • • • • • • • • • • • .; . . . . . .. . . . . . . . . . ; • • • • • __ • • ___ • • • : • • • • • • • • • • • u • • ~._ . __ • • • • • • • • • ..:. • • • • _ • • • • • _ • •

~ No consistent trend can be extracted relating ullage


z
~ 15 · · · · · i····:: T ::-::1"-:::t:::::[::::- volume to pressure response for the high amplitude liquid
hydrogen slosh tests. For the low amplitude (stable)
slosh, however, it appears that the final tank pressure is
10
0 50 100150 200250300 directly proportional to the ullage volume, as
TIME (SEC)
demonstrated in Fig. 13. Temperature data and video
indicates that much less mixing of the bulk propellant
Fig. 11. Pressure response of two tests with different occurs for the low amplitude slosh, resulting in a stratified
slosh frequency and amplitude, and all other liquid layer near the interface. Consequently, the rate of
test parameters held constant. condensation at the interface is much less than the high
amplitude slosh, and probably is not significantly affected
by the ullage volume. Therefore, the highest pressure
Helium Pressurant decay is seen at the smallest ullage volume since there is
less ullage mass to maintain tank pressure (i.e. ullage
The presence of helium in the unage results in a pressure is more sensitive to interfacial condensation with
gradual pressure increase (primarily due to environmental lower ullage volume).
heat leak) for all of the slosh tests with liquid hydrogen.
By contrast, the tests with gaseous hydrogen pressurant
exhibit pressure decay during slosh. A comparison of the 40
effects of pressurant gas type is shown in Fig. 12 for two
<' 35 , --••.~.:. ~.:-:..::
...~~...::...::...::...:::...:-:...:-::...-.. jL....--..._
..._
..._
..._ ....J
... _
small amplitude slosh tests with similar parameters. (j)
\ .~ ... ~:...... -- ----
I :L= i:::::e-: - -:-
e:- .
UJ 30
a:
:::l
30 (f)
(f) 25 f : ... -~_ ~
-HELIUM PRESSURANT (RDG 187) UJ
--_. HYDROGEN PRESSURANT (RDG 302) a:
0..
f . ~ --r---- ,
;? ~ 20 ./ .................. ~ ....................... ;....................... ...............•......
(j) 25 -.............. -.-.-.~ ...--.-.-.- ............ ...-.. ---.- ....-.. --.-.~ ; z r -51 % ULLAGE (RDG 886)
e:-
UJ
~
15 I ........ ---'33% ULLAGE (RDG 869) .................... .
a: - -13% ULLAGE (RDG 877)
::>
(f)
: . :
20

::~I-~:-:~~-r~~~::-~-[~--
(f) 10
UJ
a: 0 50 100 150 200
0..
~ TIME (SEC)
z 15
~
Fig . 13. Pressure response of three low amplitude slosh
tests with different ullage volumes, and all
10
0 50 100 150 200 other test parameters held constant
TIME (SEC)

Fig . 12. Pressure response of one test using helium ramp Slush HydrQ~en
pressurization, and the other using gaseous
hydrogen, with all other parameters similar. Slush hydrogen exhibits greater pressure
decay/collapse than liquid hydrogen under similar slosh

-j
conditions due to the greater subcooling available. This pressure - and propellant, ullage, and wall temperatures -
subcooling results in much greater interfacial condensation have been characterized for a variety of test conditions in
rates, and subsequently greater pressure decay/collapse. both stable and unstable slosh regimes. Information on
Figure 14 demonstrates this trend for two slosh tests with pressurant mass and flowrate requirements for pressurizing
similar tes~ conditions. static tanks containing liquid and slush hydrogen bas been
added to the existing database. Pressure collapse
magnitude and rate has also been recorded.
40

35
i -LIQUID HYDROGEN (RDG 895) The nature of the slosh excitation frequency and
: ..::.~ ----SLUSH HYDROGEN (RGD 889)
amplitude dramatically effects the tank thermodynamic
<" 30
Ci5 response. Sloshing near the natural frequency of the tank-
e::. liquid system (i.e. in the unstable region) can result in
w 25
a: severe ullage collapse; whereas, slosh in the stable regions
::::>
CI)
CI)
20 generally has little effect on the pressure response of the
w
a: 15 tank. Equations (2) and (3), coupled with estimates of the
a.
~ antiCipated excitation frequencies and amplitudes for a
z 10
;:: given vehicle and mission profile, can be utilized to map
5 the slosh stability regions for a spherical tank. Results of
this test series can then be used to give a qualitative idea
0
0 50 100150200250300 of what the thermodynamic tank response will be. Thus,
TIME (SEC)
corrective action (e.g. baffles, modified mission profile,
additional pressurant, etc.) can be undertaken in the design
Fig. 14. Comparison of pressure response for liquid stage to mitigate potential slosh problems. These test
versus slush hydrogen. results may also have limited application to other tank
geometries (see Refs. 4 and 5 for calculation of natural
frequency for cylindrical and circular crossection tankage) .
The same trends previously described for liquid
hydrogen slosh (i.e. frequency and amplitude, pressurant Other parameters found to affect the tank
type, and ullage volume) are observed for the slush thermodynamic response include pressurant type and
hydrogen tests. In addition, some unique features are ullage volume. The effects of these secondary parameters
evident from the video and sensor data for the slush have been characterized under a variety of conditions.
hydrogen tests. For instance, the solid particles tend to Finally, significant differences in the pressure response
settle quickly to the bottom of the tank. In fact, a between liquid and slush hydrogen bas been observed, as
completely homogeneous mixture of liquid and solid well as some peculiarities associated with the handling of
particles was never achieved, even with the large slush hydrogen.
amplitude sloshing and the propellant mixer on.
Consequently, a layer of thermally stratified liquid Data collected and analyzed from this test program
hydrogen was prevalent in the upper portion of the provides an empirical database with which to gauge the
propellant; while the solid particles mixed with liquid importance of potential thermodynamic slosh response on
hydrogen ~t constant triple point temperature remained in future launch/space vehicles. Perhaps a more vital use for
the lower portion of the propellant. During expUlsions, this data, however, is the validation of
this separation of liquid and slush hydrogen resulted in analytical/numerical simulation methods. The coupling
solid particles being expelled from the tank rather quickly of computational fluid dynamic techniques to accurate
as the fill/drain valve was opened. As reported in earlier thermodynamic algorithms will undoubtedly be required to
studies 3 , no significant handling problems were adequately predict slOShing effects for a wider variety of
encountered. However, greater care was required in the tank geometries, hardware, and conditions.
chilldown of transfer lines/components and the test tank to
retain an acceptable solid fraction . The solid fraction for References
all slush slosh tests ranged from approximately 30% to
1. Stofan, A.J ., and Armstead, A.L., "Analytical and
50%, with a mean value of 37%.
Experimental Investigation of Forces and Frequencies
Resulting from Liquid Sloshing in a Spherical Tank",
Concluding Remarks NASA TN D-1281, July, 1962.

Results from this test series have shed new light on 2. Sumner, LE., Experimental Investigation of Stability
how various parameters affect the thermodynamic response Boundaries for Planar and Nonplanar Sloshing in
of a liquid/slush hydrogen tank undergoing slosh. Tank Spherical Tanks", NASA TN D-321O, January, 1966.

9
3. Hardy, T.L., and Whalen, M.V., "Technology Issues
Associated With Using Densified Hydrogen for Space
Vehicles", NASA TM-I05642, 28th Joint Propulsion
Conference, AIAA-92-3079, July, 1992.

4. Budiansky, B., "Sloshing of Liquids in Circular


Canals and Spherical Tanks", Journal of the Aero/Space
Sciences, Vol. 27, No.3, pp 161-173, March, 1960.

5. McCarty, J.L., and Stephens, D.G., "Investigation of


the Natural Frequencies of Fluids in Spherical and
Cylindrical Tanks", NASA TN D-252, 1961.

10
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REPORT DOCUMENTATION PAGE OMB No. 0704-0188
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1. AGENCY USE ONLY (Leave blanK)

4. TITLE AND SUBTITLE


r' REPORT DATE
June 1994
1.
3 REPORT TYPE AND DATES COVERED
Technical Memorandum
5. FUNDING NUMBERS

Experimental Results of Hydrogen Slosh in a 62 Cubic Foot (1750 Liter) Tank.

6. AUTHOR(S) WU-763-22-21

Matthew E. Moran, Nancy B. McNelis, Maureen T. Kudlac,
Mark S. Haberbusch, and GeorgeA. Satornino

7 . PERFORMING ORGANIZATION NAME(S) AND ADDRESS(ES) 8 . PERFORMING ORGANIZATION


REPORT NUMBER

National Aeronautics and Space Administration


Lewis Research Center
E-8916
Cleveland, Ohio 44135-3191

9. SPONSORINGJMONITORING AGENCY NAME(S) AND ADDRESS(ES) 10. SPONSORINGJMONITORING


AGENCY REPORT NUMBER

National Aeronautics and Space Administration NASA TM- I06625


Washington, D.C. 20546-0001 AIAA-94-3259

11. SUPPLEMENTARY NOTES


Prepared for the 30th Joint Propulsion Conference cosponsored by AlAA, ASME, SAE, and ASEE, Indianapolis, Indiana, June 27-29, 1994.
Matthew E. Moran, Nancy B. McNelis, and Maureen T. Kudlac, NASA Lewis Research Center; George A. Satomino, Ohio Aerospace Institute,
22800 Cedar Point Road, Brook Park, Ohio 44142; and Mark S. Haberbusch, Sverdrup Technology, 6100 Columbus Ave., Sandusky, Ohio 44870
(work funded by NASA Contract NAS3-25517). Responsible person, Matthew E. Moran, organization code 5340, (216) 433-7525.
12a. DISTRIBUTION/AVAILABILITY STATEMENT 12b. DISTRIBUTION CODE

Unclassified - Unlimited
Subject Category 34

13. ABSTRACT (Maximum 200 words) ,


Extensive slosh testing with liquid and slush hydrogen was conducted in a 62 cubic foot spherical tank. to characterize
the thermodynamic response of the system under normal gravity conditions. Slosh frequency and amplitude, pressurant
type, ramp pressure, and ullage volume were parametrically varied to assess the effect of each of these parameters on
the tank pressure and fluid/wall temperatures. A total of 91 liquid hydrogen, and 62 slush hydrogen slosh tests were
completed. Both closed tank. tests and expulsions during sloshing were performed. This report presents and discusses
highlights of the liquid hydrogen closed tank. results in detail, and introduces some general trends for the slush hydro-
gen tests. Summary comparisons between liquid and slush hydrogen slosh results are also presented.

14 . SUBJECT TERMS 15. NUMBER OF PAGES


12 I
Cryogenics; Liquid hydrogen; Sloshing; Slush hydrogen; Liquid propulsion 16. PRICE CODE
A03 I
17. SECURITY CLASSIFICATION 18. SECURITY CLASSIFICATION 19. SECURITY CLASSIACAnON 20. LIMITATION OF ABSTRACT
OF REPORT OF THIS PAGE OF ABSTRACT
Unclassified Unclassified Unclassified I
NSN 7540-01-280-5500 Standard Form 298 (Rev. 2-89)
Prescribed by ANSI Std. 239- 18
298- 102
I
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