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PRODUCTION OF BLEACH SOLUTION AND COMPARATIVE STUDY OF COMERCIALLY PRODUCED BLEACH SOLUTION
PRODUCTION OF BLEACH SOLUTION AND COMPARATIVE STUDY OF COMERCIALLY PRODUCED BLEACH SOLUTION
com
BLEACH SOLUTION
BY
(OND)
(IMT), ENUGU
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AUGUST 2005
TITLE PAGE
BY
(OND)
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(IMT), ENUGU
AUGUST 2005
CERTIFICATION
The Project has been read and found worthy of submission to the
BY
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DEDICATION
protection throughout our stay in the polytechnic. And to our parents who
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ACKNOWLEDGEMENT
IKEYI, who in spite of her commitments devoted time to direct and guide us
Adebayo, Mr. Apkagu, Mr. Ugwuoke, Mr. J. N. Amuh, who is our Head of
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ABSTRACT
research work is oxochtorale: (i) acid solution (Hocl). The bleach was
produced when 100mls of hydrochloric acid was pound into the flask and
20g of potassium tetraozo magnate (vii) was also put into the round bottom
flask. The flask containing the Hcl was connected into one of the opening,
so that the Hcl ran into the round flask to make contact with the potassium
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tetraoxomaganate (vii) Kmno4. The chlorine gas was liberated and passed
on till the water became saturated form exochlorate (i) acid, which is the
control bleach used was Jik a product of PZ Nigeria plc. The result sowed
that there was significant difference between the laboratory produced bleach
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TABLE OF CONTENTS
Title page
Certification
Dedication
Acknowledgement
Abstract
Table of contents
CHAPTER ONE
1.0 Introduction
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1.3 Hypothesis
CHAPTER TWO
CHAPTER THREE
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CHAPTER FOUR
4.1 RESULTS
4.2 DISCUSSION
CHAPTER FIVE
5.1 CONCLUSION
5.2 RECOMMENDATION
REFERENCES
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CHAPTER ONE
1.0 INTRODUCTION
from a fiber to make it white. This process can be extended to other uses for
Bleach solution ranges from simple to complex types in various trade names
like parazone, Jik etc. They completely depend on the makes up of the
ingredient materials.
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various producing firm in Nigeria. This study is set to assess the production
Nigeria.
“SUB PROBLEM 1”
The reason for this study is to produce a bleach solution that will be of
below:
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1.3 HYPOTHESIS
Having stated the problems and the objectives of the study, the
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1. FINANCE
Finance has been the major factor in any type of project. Lack of
2. TIME
The interval between choosing the project topic, the submission of the
infinitesimal, but these are logjam and hence the researchers were
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research work.
For sometime now, there has been great public concern over the low
because things like domestic work in our homes. For example, washing
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CHAPTER TWO
the Greek and Roman used this neutralization method until the mid –
by digesting the seaweed cleans the material. After the alkaline treatment,
the cloth was treated with sour milk to remove any calcium salt and to
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scorning. After scorning, the cloth was rinsed and laid in the sun for days at
By the 1800 century, there was a strong demand for bleached cloth.
The classical sequence of scour, some and bleach remained the only method
available. The first two steps in the sequence was later improved some what
by the use of alkali solution, in the scouring process and the replacement of
stage was set for the introduction of a chemical process for bleaching.
chlorine, but he found out that this weakened the cloth excessively. He later
fully accepted chemical bleaching process with lime and soda ash being used
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for the scour, oil of vitriol for the scour and potassium hypochlorine for the
bleach.
soda and by the turn of the century, labarraque solution has completely
crafting.
bleaching powder was of great importance since this solid form of chlorine
plants adjacent to the textile mills. For the next century, bleaching powder
remained the chief source of textile bleach and has the impetus for much of
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reducing agent Ababid (1984). Almost invariably the oxidizing agent gives
a more permanent white than the reducing agent. When the colour is acted
upon by a reducing agent, there is always the possibility that the oxygen in
fibers was bleaching powder, which is more convenient to handle and more
oxygen Ababid (1984), p. 165 and the method of bleaching was to lay the
methnal out in a field where it was exposed to the sun and air. This was
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dothionatic has been the most popular reducing bleach used in the textile
unlike most of the metal hydrides. It can dissolve in cold water, and thus
i. Chlorine,
ii. Chloramines
v. Perborales
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vi Chlorine dioxide
a) CHLORINE
b) CHLORAMINE
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c) HYDROGEN PEROXIDE
e) PERBORALES
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f) CHLORINE DIOXIDE
the pulp industry in the past decade. The principal processes used to
g) CALCIUM HYPOCHLORITE
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h) SODIUM HYPOCHLORITE
chain that is a double bond, which alternate with single bonds. If one of the
destroyed; therefore any agent, which will remove a double bond linkage,
may be effective as bleach. A bleaching agent may also act on the groups at
a double bond has been destroyed. In some instances in which colours can
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groupings.
may remove the remaining colour. Sodium hypochlorine has the widest
range of attack and may be used up to the point where it attacks the fiber.
This acid is very instable and breaks down releasing nascent oxygen
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Excess NaOH and the PH condition control the nascent oxygen release
hundred gallons of water will yield of the other of 1.45glc this will fall
hypochlorine is never free from the risk of tendering due to the formation of
oxycellulose.
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CHAPTER THREE
2. Hydrochloric acid
3. Water
2) Connecting tube
3) Beaker
4) Cork
7) Spatula
8) Weighing disc
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9) Weighing balance
Retor
t
stand
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Tetraoxomanganate
(VII)
CHLORINE Crystals
(Kmno4)
OXOCHLORATE ACID
SOLUTION.
100mls of hydrochloric acid was poured into the flask with tap and
also put into the round bottom flask with two openings. The flask
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containing the HCL was connected into one of the openings of the round
bottom flask with the help of a cork. The tap was turned on so that the HCL
ran into the round bottom flask to make contact with the potassium
through the other opening into the connecting tube and into a beaker
containing distilled water. The chlorine gas passed on till the water became
saturated to form oxochlonate (i) acid,which is the bleach solution when the
water in the beaker turned yellow, the reaction was stopped. The equation is
thus:
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CHAPTER FOUR
4.1 RESULTS
The table below shows the time taken to saturate 50mls of beaker of
TABLE I
I 10
II 15
III 20
The table shows the cleansing ability of the different samples and the
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TABLE II
I Effective
II More Effective
I Not Effective
II Effective
III Effective
The table below shows the Irritability test of the laboratory produced
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TABLE III
BLEACH SOLUTION
SAMPLE IRRTATION
I Non Irritable
II Non Irritable
III Irritable
BLEACH SOLUTION
SAMPLE IRRTATION
I Irritable
II Irritable
III Irritable
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4.2 DISCUSSION
TIME OF SATURATION
The experiment shows that the longer the time last to saturate the
water, the more concentrated the solution becomes and the more bleaching
effect.
CLEANSING ABILITY
effective in sample (I) than the commercially produced bleach solution also
shows that the laboratory produced bleach solution of sample II was more
these were done on the same timing after 10, 15, 20 minutes each.
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IRRITABILITY TEST
chlorine. But the irritability test for commercially produced bleach solution
shows that there were irritations on the samples due to excessive chlorine
concentration.
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CHAPTER FIVE
5.1 CONCLUSION
CLEANSING ABILITY
Due to the experiment carried out and with the help of the results, the
researchers were able to conclude that sample III, which was most
after washing for about 5 minutes. At this, concentration, the smell was
acceptable and appealing to the end user and non irritating and hence will
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5.2 RECOMMENDATION
that the small-scale industries can grow and chlorine produced will not be
wasted.
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REFERENCES
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