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C2. Experimental Techniques
C2. Experimental Techniques
C2. Experimental Techniques
-
states :
liquid # ,
-
[ h_ ] → [ -1 ]
until
evenly spread out
* make faster ?
-
•
same to ,
different rates
→
Mr d → of
C2 .
Experimental techniques
C2 1
.
.
Measurements
unit equipment
liquids
2
-
'
volume ?m3 [ ]
accuracy
-
⇐
em
✗ precise :
variable V accurate :
3 fixed V
O -
50cm
⇒ minions -
10cm
}
3
-
25cm
gases
↳
Criteria of
c. 2.2 .
purity
how ?
↳
melting and
boiling point analysis * → data tables
g. pure water b.
e. :
p
:
I
.
M.p.
:
ww
Paper chromatography
•
(
in a solvent
•
solvent travels via
capillary action
>
dif rates
•
Retention factor ( Rf ) values
/ I.
7
ratio
/ )
units )
Rf = d moved
by compound ¥ ( no
d solvent
Cmf
" "
£1
?
highest / lowest solubility
-
pure / impure ?
C 2.3 .
Methods of purification
difference physical properties ?
-
rely on a in such as
Mixture of solids
-
f ,
magnetic properties , solubility ,
. . .
decanting (
pouring carefully ) separate undissolved solid from mixture of centrifugation
• •
*
crystallisation
•
yet;¥eÑ heat
•
•
cool
→
( once cooled ) o
filter to collect crystals
•
wash w/ cold , distilled water to remove impurities
•
dry
Simple Distillation Fractional distillation
separate soluble solid from solution
separate 32 miscible liquids
•