ZN5VFME-02_VF-500

Control Number ZN5VFME-02
Vertical Furnace
VF-500
Instruction Manual
CAUTION
To use the unit correctly, read this instruction manual before use.
Keep the manual at hand when operating the unit.
Nittoseiko Analytech
EC DECLARATION OF CONFORMITY
We hereby declare that the following equipment complies with the essential requirements
of:
Electromagnetic Compatibility Directive: 2014/30/EU

Low Voltage Directive: 2014/35/EC
RoHS Directive: 2011/65/EU(include(EU)2015/863)
Model Name : Vertical Furnace Model VF-500
Standard to which Conformity is Declared:
EN 61000-6-4:2019 : Generic standards-Emission standard for industrial environments
EN 61000-6-2:2019 : Generic standards-Immunity standard for industrial environments
EN 61010-1:2010/A1:2019 : Safety requirements for electrical equipment for measurement,

control, and laboratory use
EN IEC 63000:2018 : Technical documentation for the assessment of electrical and

electronic products with respect to the restriction of hazardous
substances
Name of Manufacturer : NITTOSEIKO ANALYTECH CO., LTD.
Manufacturer’s Address : 7-10-1 Chuo-rinkan, Yamato, Kanagawa 242-0007, Japan
EU Office Address : MITSUBISHI CHEMICAL EUROPE GmbH

Willstaetterstr. 30, 40549 Duesseldorf, Germany
Type of Equipment : Laboratory Equipment
Month and year of CE Marking : June, 2017
_______________________
Name : Kaoru Hayashi
Position : General Manager
Date : 16 . 07 . 2021
DD.MM.YYYY
UK Declaration of Conformity (DoC)
Object of Declaration
Product name: Vertical Furnace
Model name: VF-500
Manufacturer
Name: NITTOSEIKO ANALYTECH CO., LTD.
Address: 7-10-1 Chuo-rinkan, Yamato, Kanagawa 242-0007, Japan
(Authorized Representative)
(Name: a1-envirosciences Ltd )
(Address: Suite2, Ground Floor,910 Birchwood Boulevard, Birchwood
Warrington WA3 7QN United Kingdom )
We declare that the DoC is issued under our sole responsibility and that the object of the
declaration described above is in conformity with the following relevant UK legislation:
Electromagnetic Compatibility Regulations 2016
Electrical Equipment (Safety) Regulations 2016
The Restriction of the Use of Certain Hazardous Substances in Electrical
and Electronic Equipment Regulations 2012
The following UK designated standards and other technical specifications have been applied.
EN61000-6-4:2019
EN61000-6-2:2019
EN61010-1:2010/A1:2019
EN IEC 63000:2018
Date of issue: 01 . 04 . 2022

DD . MM . YYYY
Place of issue: Japan
Signature: ____________________
Name: Kaoru Hayashi
Position / Title: General Manager
Introduction 1
Introduction
Thank you for purchasing our Vertical Furnace Model VF-500. This vertical furnace is
used to combust samples.
This manual is the instruction manual for the Vertical Furnace Model VF-500.
To use the unit efficiently and safely, read this manual and fully understand the functions
and the operation methods before use.
This instruction manual contains the description of each part of the unit, specifications,
warranty provisions, and others.
The NSX-5000 system consists of an injector, an electric furnace, and a detector. The
units are combined according to each measurement. Read the instruction manual of each
component unit.
For the measurement operation, read the operation manual.
Some unit combinations may not be supported depending on the system configuration.
When changing the configuration of the units, update the application software and the
unit software.
Before Use
Take care of the following points about this manual.
(1) Do not reprint this manual wholly or partially without permission.
(2) The contents may be changed without notice.
(3) Though this manual was prepared carefully, contact our local distributor when
mistakes, omissions, or missing pages are found.
The application software in this manual may be different depending on the version
of the software.
(4) For any consequences of used results, we do not take any responsibility regardless
of (3).
(5) Assign specific operators and supervisors when using this unit.
(6) Always follow the contents in this manual. When problems or damages occur by
neglecting the contents in this manual, we do not guarantee the system even within
the guarantee period.
Nittoseiko Analytech has the copyrights of this manual and the unit software.
Microsoft and Windows are registered trademarks of Microsoft Corporation.
Other company and product names described in this manual are their trademarks and
registered trademarks.
VF-500 (NSX-5000)
2 Introduction
About This Manual
About Composition
This instruction manual is composed as follows.

• Sections 1 to 3 (introduction)
These sections describe the names and functions of the unit, parts list, and
installation.
• Sections 4 to 7 (operation)
These sections describe measurement, troubleshooting, error messages and
measures, and maintenance and inspection.
• Sections 8 to 11 (others)
These sections describe the disposal of the unit, specifications, guarantee
provisions, and consumables.
About Indications
The elements of windows are expressed as follows.

• The names of menus, windows, icons, buttons, and items are expressed with
brackets or double quotations.
Example: Click [OK].
Click “File”-“New”-“Folder” of the menu.
• Keyboard keys are expressed with angle brackets.
Example: Press <F5> key.
• The title of a reference chapters expressed with double quotation marks.
Example: Refer to “3-1. Installation Conditions”.
The selection of a menu item, a button or an icon is expressed as follows.

Example: Click [OK].
Click “File”-“New”-“Folder” of the menu.
Refer to “SAFETY PRECAUTIONS” for the indications of warnings and cautions.
VF-500 (NSX-5000)
Introduction 3
About Terms
This manual uses the following terms.

• Application software: Software that operates the system from a PC
• Unit software: Software that controls the unit
• System controller: Software that connects communication between the
application software and the unit software and controls the system
• System down: State where the system is shut down after a serious error is
detected in a unit
VF-500 (NSX-5000)
4 Introduction
VF-500 (NSX-5000)
SAFETY PRECAUTIONS 1
SAFETY PRECAUTIONS
Read this instruction manual the operation manual, and the instruction manuals
supplied with parts carefully before use.
Always read safety precautions before use.
Security cannot be assured if the unit is operated without following the instructions in
this manual.
Keep the manual and the instruction manuals supplied with parts at hand.
Indications of Safety Precautions
This instruction manual uses several indications to highlight critical precautions. The
items with these indications are important for the safe use of the unit. Always observe
them. The following indications are used for safety precautions.
WARNING
Information under this sign explains critical operations which contain the
risks of death or serious casualties caused by wrong handing.
CAUTION
Information under this sign explains critical operations which contain the
risks of human casualties or property damages caused by wrong
handing.
Other Indications
Besides the safety precaution indications, this instruction manual uses the following
indication to show an important or useful thing for measurement with this unit. The items
with this indication are important for the safe use of the unit. Be sure to read them
before use.
POINT
Information under this sign explains important items and tips for
measurement with this unit.
VF-500 (NSX-5000)
2 SAFETY PRECAUTIONS
Warnings and Cautions
Labels
The following labels are attached to this unit. Always follow the instructions on the labels.
Warning or Caution label Attached place

It is attached on the electric
furnace.
It is attached on the front of

the unit.
It is attached on the front of

the unit.
It is attached around the

power voltage selector switch
on the rear of the unit.
It is attached on the rear of

the unit.
It is attached at the gas

connection part on the rear of
the unit.
VF-500 (NSX-5000)
Cautions
Read the following cautions carefully to use the unit correctly and safely.
Installation
When installing the unit, always observe the following precautions.
WARNING Room temperature

Install the unit in a place where room temperature is 15 to 35 degrees
Celsius and temperature change is small.
Failure to do so may cause a fault or significantly shorten the life. It may
also cause unstable operation or a fire.
WARNING Air conditioning

Install the unit in a place where it is not exposed to direct wind from an air
conditioner.
Failure to do so may cause unstable operation or a fire.
WARNING Humidity
Install the unit in a place where humidity is 80%RH or less with no
condensation.
Failure to do so may cause condensation, leading to a fire or electric
shock. Obtain a humidity environment free from condensation using an
air conditioner.
WARNING Dust
Install the unit in a place free from much dust.
Failure to do so may cause a fire or electric shock. Clean the area around
the unit regularly. If the unit vent is blocked by dust, the inside will
become hot, which may cause a fault or significantly shorten the life.
VF-500 (NSX-5000)
WARNING Direct sunlight

Install the unit in a place free from direct sunlight.
Failure to do so may lead to a fire.
WARNING Fire
Install the unit in a place where fire is not used.
Failure to do so may lead to a fire.
WARNING Altitude
Install the unit in a place where the altitude is below 2000 meters to avoid
unstable operation, a fire, or an electric shock.
WARNING Turning off the electric furnace

When handling combustion tube parts, always turn off the electric furnace
and wait until the furnace temperature is room-temperature.
Never touch them while the electric furnace is hot. Doing so may cause
burns.
CAUTION Ventilation
Ventilate the room by an air conditioner, a ventilating fan, etc.
Failure to do so may damage health by the gas generated from
chemicals or exhaust gas from the unit.
CAUTION Corrosive gas

Install the unit in a place free from corrosive gas.
Failure to do so may cause a fault and lead to an accident.
Air near the sea contains sea salt particles, which may cause insulation
failure or corrosion deterioration.
VF-500 (NSX-5000)
CAUTION Combustibles
Do not place combustibles around the unit. If a fire occurs, more damage
will be caused.
CAUTION Vibration
Install the unit in a place free from strong vibration or continuous weak
vibration. Failure to do so may cause unstable operation or a fault and
lead to an accident.
CAUTION Electromagnetic field

Install the unit in a place free from strong electromagnetic field.
Failure to do so may cause errors and lead to an accident.
CAUTION Installation surface

Install the unit on a flat surface.
Failure to do so may cause the unit to drop or fall, which may result in
injury.
CAUTION Earth terminal

Check that earth terminal is properly connected.
Failure to do so may cause electric shock.
CAUTION Gases to use

Make adjustment so that the pressure of Ar gas is equal to that of O2 gas.
Adjust the setting pressure within the range of 0.3±0.1 MPa.
If the setting pressure is out of the range of 0.3±0.1 MPa, the unit may
not operate correctly or it may break.
Prepare Ar gas with a purity of 99.98% or greater and O2 gas with a purity
of 99.7% or greater.
Prepare gas with a cylinder of 7 m3 or more capacity.
VF-500 (NSX-5000)
CAUTION Connection method

Always connect lines with two spanners.
Use ferrules and inserts to connect fluororesin tubes.
If the unit is used while gas is leaking, an accident may be caused.
CAUTION Gas lines

The system gas lines vary depending on the injector and detector.
Refer to the instruction manuals for the injector and detector. If a different
gas line is connected, an accident may be caused.
CAUTION Check of O-rings

When setting an O-ring, check that it is not damaged. If it is damaged,
gas may leak and an accident may be caused. In this case, change it
immediately.
CAUTION Combustion tube breakage

Combustion tube is glass. If it is dropped or strong pressure is put on it,
an accident may be caused. Take enough care in handling.
CAUTION Transportation
When moving the unit, firmly hold it with hands and do not incline it.
Bumping the unit or falling it causes not only unit breakage but also
injuries.
VF-500 (NSX-5000)
Usage
When performing measurement or other operations with the unit, observe the following
precautions.
WARNING Prohibition of unattended

operation
Do not use this unit without attendance at night or other situations.
The unit is designed for attended operation. If there is no one around
when an error occurs, appropriate measures cannot be taken promptly,
which may lead to a serious accident.
WARNING Microsyringe to use

Always use a microsyringe specified by us.
Failure to do so may break the microsyringe or cause a fire due to
abnormal combustion.
WARNING Combustibles and combustible

gas
Keep the system off the combustibles and combustible gas.
The electric furnace of the system is hot during operation. Do not let
combustibles contact directly with the electric furnace or combustible
liquid drop around it. Doing so may cause a fire.
WARNING Power plug

Do not touch the power plug with wet hands.
Doing so may lead to electric shock.
VF-500 (NSX-5000)
WARNING Power cable

Do not bundle the power cable or use it with physical force applied to it.
Do not heat the power cable.
A hot or broken power cable may lead to a fire or electric shock.
Do not use a power cable under the rating or modified or broken one.
Use a power cable based on our specification.
WARNING Cables and connectors on the

rear of the unit
Do not touch the cables and connectors on the rear of the unit during use
of the unit.
Doing so may cause poor communication or a fire due to errors.
WARNING For protection

When handling chemicals, always wear protectors.
Failure to do so may lead to physical damage, such as chemical injury or
blindness. When handling chemicals, always check the safety data sheet
and wear protectors, such as safety goggles and safety gloves.
WARNING Gas leakage check before using

the unit
Always check for gas leaks before using the unit.
When organic matter suddenly mixes with oxygen or air in a high-
temperature environment, explosive combustion may occur. As a result,
glass parts such as combustion tubes can break and shatter, leading to
human casualties.
This unit prevents explosive combustion by mixing samples with O2 gas
and combusting them after vaporizing samples in argon gas.
VF-500 (NSX-5000)
WARNING Hot electric furnace and

combustion tube
Never touch a hot electric furnace or combustion tube.
Doing so may cause burns. Never touch them.
WARNING Prevention of fire and burns

Washing with an organic solvent may cause a fire. It may also cause
burns when the temperature of the electric furnace is raised. Be sure to
turn off the power of the unit and let the electric furnace cool sufficiently
before starting an operation.
When using a burner, take sufficient care and perform operations with
experienced people.
WARNING Indication of WARNING

When “WARNING” is displayed in the PC monitor, this indicates the risks
of serious accidents.
When these messages are displayed, deal with the problems
immediately.
CAUTION Cover of the unit

Do not remove the cover of the unit.
Doing so may cause a fault or electric shock.

Combustion tube is glass. If it is dropped or strong pressure is put on it,
an injury may be caused. Take enough care in handling.
VF-500 (NSX-5000)
CAUTION Unit supervisors and operators

Assign specific operators and supervisors for the system. The system
needs to be installed and used with due care. The supervisors should
manage and supervise the operators of the system. If the management
and supervision of this system or an operator are not enough, accidents
or injuries may be caused because of insufficient inspection or incorrect
operation.
Operation
When operating the system, observe the following precautions.
CAUTION Maintenance and inspection

Be sure to perform daily and periodical inspections before the use of the
unit.
Failure to check the unit may lead not only to the poor performance but
also to serious accidents.
CAUTION Combustion tube devitrification

When a combustion tube is devitrified, its mechanical strength decreases
and it may break. As a result, accidents or injuries may be caused.
The term “devitrification” refers to a condition where the combustion tube
color has turned white. When a combustion tube is devitrified, especially
when fine cracks are in the devitrified part, the mechanical strength is
low. Change it immediately.
VF-500 (NSX-5000)
About RCF
In accordance with the partial revision of the Enforcement Order of the Industrial Safety
and Health Law, Refractory Ceramic Fibers (RCF) is now regulated as a specially
controlled substance and a controlled class 2 substance of specified chemical
substances as stipulated in the Ordinance on Prevention of Hazards due to Specified
Chemical Substances (Specified Chemical Regulation).
Although RCF is used in this unit, the RCF is molded or has shatter-proofing measures.
Therefore, the regulations do not apply to the normal use of the unit.
Use of RCF in the Unit
This unit uses RCF as follows. Refer to the following figure.
(1) Electric furnace

RCF is used as the heat insulator of the electric furnace.
(2) Shield plate on the top of the electric furnace

RCF is used as the shield plate (a pair of two half-moon-shaped plates).
Operations Subject to the Control
If you do any work (disassembly, dismantling, etc.) where RCF is expected to be

dispersed, it is subject to the Specified Chemical Regulation. The Specified Chemical
Regulation stipulate preventive measures against health hazards and require the
following measures.
(1) Installation of a local exhaust system
(2) Appointment of a work supervisor
(3) Measures for specially controlled substances, such as posting notices and keeping
work record (30 years)
(4) Measures to prohibit access except for related personnel
VF-500 (NSX-5000)
(5) Measures to measure the working environment
(6) Implementation of health checkups
(7) Cleanup
Composition of RCF
A summary of the composition and hazards of RCF is as follows. Refer to the Safety
Data Sheet (SDS) for the details. Contact our local distributor for the SDS.
RCF composition and component information
Main component: Al2O3: 30 to 60%, SiO2: 40 to 60%, ZrO2: 0 to 20%

For the purpose of shatter-proofing, molded products contain about 5 to 15%
binder.
Substances subject to notification under the Industrial Safety and Health Law 08
PRTR Law Applicable
CAS No. 142844 - 00 - 6
RCF stability
Non-combustible
Hazard summary
(1) Molded products and those with shatter-proof treatment

• Operations using the unit is not hazardous.
• Operations with processing can be just as hazardous as non-molded products.
(2) Non-molded products

• They may be carcinogenic (IARC 2B)
• Contact with the eyes or skin may cause transient mechanical irritation.
• Prolonged or repeated exposure may cause respiratory problems.
VF-500 (NSX-5000)
Precautions during Work
Take following precautions during work (processing molded products and handling non-
molded products)
• Do not eat, drink or smoke during work.
• Exhaust the air to minimize the inhalation of dust.
• Wear protective gloves.
• Wear respiratory protectors.
• Wash hands thoroughly after handling.
Precautions during Work
Take the following precautions during work (processing molded products and handling
non-molded products)
• Do not eat, drink or smoke during work.
• Exhaust the air to minimize the inhalation of dust.
• Wear protective gloves.
• Wear respiratory protectors.
Wash hands thoroughly after handling.
VF-500 (NSX-5000)
VF-500 (NSX-5000)
Table of Contents 1
Table of Contents
Introduction ...................................................................................................................... 1
Before Use ................................................................................................................ 1
About This Manual .................................................................................................... 2
SAFETY PRECAUTIONS ................................................................................................ 1
Indications of Safety Precautions .............................................................................. 1
Other Indications ....................................................................................................... 1
Warnings and Cautions............................................................................................. 2
Labels ............................................................................................................... 2
Cautions............................................................................................................ 3
About RCF ...................................................................................................... 11
Section 1: Names and Functions of the Unit................................................................. 1-1
1-1. Names and Functions of VF-500 Front ........................................................... 1-1
1-2. Names and Functions of VF-500 Rear ........................................................... 1-2
1-3. Names and Functions of VF-500 Electric Furnace ......................................... 1-4
1-4. Names and Functions of VF-500 Combustion Tube Top ................................ 1-5
Section 2: Parts Check ................................................................................................. 2-1
2-1. VF-500 Parts .................................................................................................. 2-1
2-2. Other Parts ..................................................................................................... 2-2
Section 3: Installation ................................................................................................... 3-1
3-1. Installation Conditions..................................................................................... 3-1
3-2. Installation Space ........................................................................................... 3-1
3-3. Power Preparation .......................................................................................... 3-2
3-3-1. Power .................................................................................................. 3-2
3-3-2. Grounding ............................................................................................ 3-2
3-3-3. Power Voltage Selector Switch ........................................................... 3-2
3-4. Cable Connection ........................................................................................... 3-2
3-4-1. Communication Cable Connection ...................................................... 3-2
3-4-2. Power Cable Connection ..................................................................... 3-3
3-5. Supply Gas Lines............................................................................................ 3-3
3-5-1. Line Preparation .................................................................................. 3-3
3-5-2. Line Connection .................................................................................. 3-4
3-6. Combustion Tube Setting ............................................................................... 3-5
3-7. Sample Injection Port Setting ......................................................................... 3-9
VF-500 (NSX-5000)
2 Table of Contents
Section 4: Measurement .............................................................................................. 4-1

4-1. Parameters .................................................................................................... 4-1
4-1-1. Parameters Set in a Method ............................................................... 4-1
Section 5: Troubleshooting .......................................................................................... 5-1
5-1. No Power to the Unit ...................................................................................... 5-1
5-2. No Communication with the Unit .................................................................... 5-2
5-3. No Temperature Rise of Electric Furnace ...................................................... 5-2
5-4. No Gas Flow .................................................................................................. 5-3
5-5. Abnormal Noise during Measurement............................................................ 5-3
5-6. Start Icon Not Enabled ................................................................................... 5-4
5-7. Troubles Occur after Changing of a Line or Cylinder ..................................... 5-4
5-8. Incomplete Combustion Occurred.................................................................. 5-5
Section 6: Error Messages and Measures ................................................................... 6-1
Section 7: Maintenance and Inspection ....................................................................... 7-1
7-1. Daily Inspection and Maintenance ................................................................. 7-1
7-2. Periodical Inspection and Maintenance ......................................................... 7-2
7-3. Storage of the Unit ......................................................................................... 7-6
Section 8: Disposal of the Unit ..................................................................................... 8-1
Section 9: Specifications .............................................................................................. 9-1
9-1. VF-500 Unit Specifications ............................................................................. 9-1
Section 10: Guarantee Provisions ............................................................................. 10-1
10-1. Guarantee Provisions for Japan................................................................. 10-1
10-2. Guarantee Provisions for Products Sold Overseas .................................... 10-3
Section 11: Consumables .......................................................................................... 11-1
11-1. VF-500 Consumables ................................................................................ 11-1
VF-500 (NSX-5000)
Names and Functions of the Unit 1-1
Section 1: Names and Functions of the Unit

This section describes the names and functions of VF-500 parts.
1-1. Names and Functions of VF-500 Front
Fig. 1-1 shows the VF-500 unit front and Table 1-1 shows the names and functions.
Fig. 1-1. VF-500 Front
Table 1-1. Names and Functions of VF-500 Front
No. Name Indication Function

1 Power switch POWER VF-500 power switch. After turning on the
rear main power switch, turn on this switch
to supply power and light the lamp.
2 Heater lamp HEATER When the electric furnace is turned on, the
lamp lights.
3 Electric furnace door Punched holes on the door are air vents.
Open the door to access the electric
furnace.
VF-500 (NSX-5000)
1-2 Names and Functions of the Unit
1-2. Names and Functions of VF-500 Rear
Fig. 1-2 shows VF-500 rear and Table 1-2 shows the names and functions.
2 3
1
4
5
6
8
9 7
10
11
12 13 14
Fig. 1-2. VF-500 Rear
Table 1-2. Names and Function of VF-500 Rear

1 Communication COMPUTER Connector for the VF-500 unit and a
connector PC. Use a USB cable for this
connection.
2 Communication ACCESSORIES Connectors for the VF-500 unit and
cable connector accessories. Use the attached
communication cable for this
connection.
3 Hole for line When using both a gas injector and the
connection ASC-550L unit, pass the sample gas
line through this hole.
4 Function switch FUNCTION DIP switch for each setting is built in.
They are operated only by servicemen.
Do not touch them.
VF-500 (NSX-5000)

5 Signal cable Connectors for I/O connection
connectors for
accessories
6 Exhaust fan Fan for cooling. Set the exhaust plate.
7 Circuit protector for HEATER It is for the protection of heater circuit
heater POWER overcurrent.
8 Power voltage Switch that switches the power voltage
selector switch between 100/115 V and 230/240 V.
(behind the blank It is set to 230/240 V on delivery. Be
panel) sure to set it to the voltage in your area.
9 Main power switch MAIN POWER It is with a leakage breaker. It always
should be on during operation.
10 Leak test button Button for testing the leakage breaker
attached to the main power switch
11 Power connector a.c. POWER Connect the power cable to supply
power.
Use a power cable based on our
specification.
12 Oxygen gas inlet GAS IN Connect the inlet to the corresponding
O2 gas purification filter to supply O2 gas to
the VF-500 unit. The diameter of the
connector is 4 mm.
13 Argon gas inlet GAS IN Connect the inlet to the corresponding
Ar gas purification filter to supply Ar gas to
the VF-500 unit. The diameter of the
connector is 4 mm.
14 Detector connection Hole through which the Gas tube dryer,
hole heating cable, or other lines pass
VF-500 (NSX-5000)
1-3. Names and Functions of VF-500 Electric Furnace
Fig. 1-3 shows the VF-500 electric furnace and Table 1-3 shows the names and functions.
Fig. 1-3. VF-500 Electric Furnace
Table 1-3. Names and Functions of VF-500 Electric Furnace
No. Name Function

1 Shield plate Shield plate for preventing electric furnace heat from
conducting upward
2 Electric furnace Openable electric furnace. Use the electric furnace by
setting a combustion tube.
When the electric furnace is hot, never touch the surfaces.
3 Electric furnace hook Lift the lever while pulling it to unlock the electric furnace.
To lock the electric furnace again, lower the lever while
pulling it.
VF-500 (NSX-5000)
1-4. Names and Functions of VF-500 Combustion Tube Top
Fig. 1-4 shows the VF-500 combustion tube top and Table 1-4 shows the names and
functions.
1 2 3
Fig. 1-4. VF-500 Combustion Tube Top
Table 1-4. Names and Functions of VF-500 Combustion Tube Top
No. Name Function

1 Sample injection port Port through which a sample is injected to the inner
combustion tube. The shape of the part to be connected to
the injection port varies depending on the injector.
2 Flange Flange that sets the sample injection port
3 Gas line for inner Line that supplies gas to the inner combustion tube.
tube Connect this line to the flange.
VF-500 (NSX-5000)
VF-500 (NSX-5000)
Parts Check 2-1
Section 2: Parts Check

This section describes delivered VF-500 parts.
When initially opening the package, check that all listed parts are included. For
consumables, refer to “Section 11: Consumables”.
* For a PC and printer, refer to the packing list attached to each device.
2-1. VF-500 Parts
Table 2-1 shows VF-500 parts.
Table 2-1. VF-500 Parts
No. Parts name Quantity Check Remarks

1 VF-500 unit 1 unit
2 Rear fan cover 1 pc
3 Fluororesin tube 4/2, 0.9 m, blue 1 pc For gas purification
filter (Ar gas)
4 Fluororesin tube 4/2, 0.9 m, black 1 pc For gas purification
filter (O2 gas)
5 Nut 4 (with front and back ferrules 2 sets For connection on
and insert) main unit rear
6 Reducer (J-4R3-S) 2 pcs For gas purification
filters
7 Insert 2 pcs For gas purification
filters
8 Connector 6/4 1 pc For connection of
branch tube of
combustion tube
9 Shield plate 2 pcs
10 Clip (long) 18 (for ball joint) For connection of
combustion tube
1 pc bottom
11 Gas purification filter fixing board 1 pc
12 Gas purification filter fixing metal 4 pcs
13 Gas purification filter fixing screw
M3×6 8 pcs
14 Double-end spanner 3/8×7/16 inch 1 pc
15 Double-end spanner 1/2×9/16 inch 1 pc
16 Double-end spanner 10×12 mm 2 pcs
17 Hexagonal spanner 3 mm 1 pc
VF-500 (NSX-5000)
2-2 Parts Check

18 Cross slot and flat-blade
screwdriver 1 pc
19 USB cable 5 m 1 pc
20 Thermal fuse 93 C (with 1 pc
fluororesin tube)
21 Female ball joint, 12.5 For connection of
1 pc branch tube of
combustion tube
22 Clip 12 (for ball joint) For connection of
branch tube of
1 pc combustion tube
23 Quartz wool 5 g 1 pc
24 Quartz wool poker 1 pc
25 Gas purification filter 2 pcs
26 Sheet for electric furnace carriage 1 pc
27 Parts packing list 1 pc
28 Instruction manual 1 pc Supply by electronic
data
29 NSX-5000 application program 1 pc
2-2. Other Parts
Table 2-2 shows other parts.
Table 2-2. Other Parts

1 Power cable (100 V or 230 V) 1 pc 100 V or 230 V
VF-500 (NSX-5000)
Installation 3-1
Section 3: Installation
Necessary space, power, and gas lines for VF-500 installation are described in this
section.
3-1. Installation Conditions
Install the unit indoors to meet the following conditions for the long-term stable use.
Refer to “SAFETY PRECAUTIONS” in this manual for details.
• Room temperature is 15 to 35 degrees Celsius. Temperature change is small.
• The unit is not exposed to direct wind from an air conditioner.
• Humidity is under 80%RH. (No condensation)
• No much dust
• No direct sunlight
• Fire is not used.
• The room is ventilated.
• No corrosive gas
• No flammable materials around the unit
• No strong vibration and continuous weak vibration
• No strong electromagnetic field
• The surface for installation is flat and stable.
• Altitude is less than 2000 meters.
If problems or damages are caused by negligence of the above conditions, we cannot

guarantee the unit even within the guarantee period. Please be aware of this in advance.
3-2. Installation Space
VF-500 installation space is as follows.

Depending on the system configuration, prepare enough space for the complete system.
• Table size: Width 500 mm × Depth 470 mm
• Table withstand load: About 35 kg
• Do not place objects in front of the rear fan for ventilation.
• Set aside more than 150 mm space between the unit and the back wall for
ventilation.
• Install the VF-500 unit to the right of the detector.
VF-500 (NSX-5000)
3-2 Installation
3-3. Power Preparation
3-3-1. Power
VF-500 consumption power is as follows. Voltage fluctuation range should be within ±10%.
Therefore, when voltage fluctuation is over 10%, use a voltage stabilizer.
• 100/115 V, 50/60 Hz: 1100 VA
• 230/240 V, 50/60 Hz: 1800 VA
3-3-2. Grounding
The VF-500 power cable is a 3-line type cable including a grounding wire. Prepare either
of the following appropriate outlets with ground on the table, and securely ground the
power cable. Select an outlet with ground according to the power supply voltage in your
area. If you cannot prepare the following outlet with ground, prepare a grounded outlet
and a grounded cable that satisfy the rating and unit power consumption conditions.
• 100/115 V Rating: 125 VAC, 15 A (JIS C 8303)
• 230/240 V Rating: 250 VAC, 16 A (SE type)
CAUTION Earth terminal

Check that earth terminal is properly connected to prevent electric shock.
Failure to do so may cause electric shock.
3-3-3. Power Voltage Selector Switch
There is a power voltage selector switch on the rear of the VF-500 unit. Switch the voltage
between 100/115 V and 230/240 V according to the voltage to be used. 230/240 V is set
on delivery. Set it to the voltage in your area before use.
3-4. Cable Connection
3-4-1. Communication Cable Connection
Connect communication cables as follows.
(1) Connect the communication connector (COMPUTER) on the rear of the VF-500 unit
and a USB port of the PC with an attached USB cable.
(2) Connect a USB port of the PC and the USB connector of the printer with an attached
USB cable.
VF-500 (NSX-5000)
Installation 3-3
3-4-2. Power Cable Connection
Connect the attached power cable to the power connector (a.c. POWER) on the rear of
the VF-500 unit.
3-5. Supply Gas Lines
3-5-1. Line Preparation
Prepare the gas lines for the VF-500 unit as follows.

• Prepare Ar and O2 gas supply lines up to the center of the table.
• Use a metal line with an external diameter of φ3 to connect to the unit.
• When connecting a line to the unit, keep about 1 m margin at the end.
CAUTION Gases to use

Make adjustment so that the pressure of Ar gas is equal to that of O2 gas.
Adjust the setting pressure within the range of 0.3±0.1 MPa.
If the setting pressure is out of the range of 0.3±0.1 MPa, the unit may not
operate correctly or it may break.
Prepare Ar gas with a purity of 99.98% or greater and O2 gas with a purity
of 99.7% or greater.
Prepare gas with a cylinder of 7 m3 or more capacity.
POINT Impurities from lines

After connecting new lines or changing or reconnecting lines, large
volumes of impurities may get into them. Thoroughly purge them before
using the unit.
POINT Gas grades

Impurities in general-grade gas may affect measurement because the
container is used repeatedly and the history of gas is left therein. This
problem can be avoided by using high-purity, high-grade gas in a dedicated
container. However, doing so does not eliminate impurities.
VF-500 (NSX-5000)
3-4 Installation
3-5-2. Line Connection
Use the following procedure to connect the supply gas lines and the gas purification filters
and further connect the lines to the VF-500 unit. Fig. 3-1 shows line connection. Refer to
the details of A to connect the fluororesin tube.
CAUTION Connection method

Always connect lines with two spanners.
Use ferrules and inserts to connect fluororesin tubes.
If the unit is used while gas is leaking, an accident may be caused.
CAUTION Gas lines

The system of gas lines varies depending on the injector and detector.
Refer to the instruction manuals for the injector and detector. If a different
gas line is connected, an accident may be caused.
(1) Connect 1. metal line φ3 that is the Ar or O2 gas supply line to the bottom of each of
the two gas purification filters.
(2) Connect 2. reducer (J-4R3-S) to the top of each of the gas purification filters.
(3) Connect 3. blue fluororesin tube φ4/2 (0.9 m) to the top of the gas purification filter
to which the Ar gas line is connected. Connect the other end to the argon gas inlet
(GAS IN Ar) on the rear of the VF-500 unit.
(4) Connect 4. black fluororesin tube φ4/2 (0.9 m) to the top of the gas purification filter
to which the O2 gas line is connected. Connect the other end to the oxygen gas inlet
(GAS IN O2) on the rear of the VF-500 unit.
VF-500 (NSX-5000)
Installation 3-5
3.
A A
2.
GAS IN
4. O2 Ar
A A
Gas purification
filters
Details of A
Front ferrule Nut
Ar gas
1.
O2 gas
Insert Back ferrule Fluororesin tube
Fig. 3-1. Line Connection
3-6. Combustion Tube Setting
A combustion tube consists of outer and inner tubes whose fillers vary depending on the
system.
For the combustion tube preparation procedure, refer to the operation manual of each
system. Even new combustion tubes need washing.
Set a prepared combustion tube to the VF-500 unit by the following procedure.
WARNING Turning off the electric furnace

When handling combustion tube parts, always turn off the electric furnace
and wait until the furnace temperature is room-temperature.
Never touch them while the electric furnace is hot. Doing so may cause
burns.
CAUTION Check of the condition of O-

rings
When setting an O-ring, check that it is not damaged. If it is damaged,
gas may leak and an accident may be caused. In this case, change it
immediately.
VF-500 (NSX-5000)
3-6 Installation

Combustion tube is made of glass. If it is dropped or strong pressure is put
on it, an accident may be caused. Take enough care in handling.
POINT Washing of outer combustion tube

Before setting a combustion tube, wipe the outside of the outer combustion
tube with clean ethanol-soaked tissue paper or cloth. Contamination
accelerates devitrification of the combustion tube and the life may be
shortened.
(1) Assemble a combustion tube by the following procedure while referring to “Fig 3-2.
Assembly of Outer and Inner Combustion tubes”.
• Put 2. inner combustion tube φ22 L227 in 1. outer combustion tube φ30 L375,
ensuring that the positions of the protrusions are aligned.
• Fix them with 3. combustion tube springs.
2.
3.
1.
Fig. 3-2. Assembly of Outer and Inner Combustion Tubes
(2) Operate the electric furnace hook on the right of the electric furnace to open the
electric furnace.
(3) While referring to “Fig. 3-3. Combustion Tube Setting”, make preparations for setting
the combustion tube to the flange by the following procedure.
• Put 4. O-ring holder in the top of the inner combustion tube.
• Put 5. O-ring P-16.
VF-500 (NSX-5000)
Installation 3-7
5.
4.
Fig. 3-3. Combustion Tube Setting
(4) While holding the bottom of the combustion tube, slowly lift it to insert it into the hole
of the flange.
(5) Tighten more the O-ring holder to fix the top of the inner combustion tube. At this
time, turn the branch tube of the outer combustion tube to the front.
(6) Close the electric furnace. Operate the electric furnace hook on the right of the
electric furnace to fix it.
(7) Connect 6. gas supply line to the outer combustion tube and 8. female ball joint
φ12.5 with 7. connector φ6/4 (30-6RU4-S). Connect 8. female ball joint φ12.5 and
the male ball joint of the branch tube of the outer combustion tube, and fix them with
the 9. clip φ12 for ball joint. Refer to “Fig. 3-4. Electric Furnace Top”.
(8) Put 10. shield plates on the electric furnace, ensuring that the chamfered surfaces
face upward. Align them to each other so that they surround the combustion tube.
Refer to “Fig. 3-4. Electric Furnace Top”.
6. 7. 8. 9. 10.
Fig. 3-4. Electric Furnace Top
VF-500 (NSX-5000)
3-8 Installation
(9) Connect a line appropriate for each detector to the combustion tube outlet.
When a Nitrogen or Sulfur Detector is Used
Connect lines by the following procedure while referring to “Fig. 3-5. Fixing Female Ball
Joint”.
• Pull the Gas tube dryer out of the detector connection hole of the VF-500 unit
toward the rear, and connect it to the buffer tank. Refer to the instruction manual
of each detector for details.
• Connect 11. female ball joint φ18 to the combustion tube outlet, and fix them with
12. clip φ18 (long). For nitrogen measurement of aqueous sample, connect the
trap tube φ18 to the combustion tube outlet.
11. 12.
Fig. 3-5. Fixing Female Ball Joint
When a Coulometric Detector is Used
Connect lines by the following procedure while referring to “Fig 3-6. Fixing Heating Tube”.
• Pull 13. cable for a heating tube out of the detector connection hole of the VF-
500 unit toward the rear, and connect it to the heating tube connector (HEATING
TUBE) on the rear of the MCD unit.
• Connect 14. heating tube to the combustion tube outlet, and fix it with 15. clip
(long) φ18. The male ball joint of the heating tube should face the MCD unit.
• Connect 13. cable for a heating tube and 16. heating tube cable.
VF-500 (NSX-5000)
Installation 3-9
13.
16. 14. 15.
Fig. 3-6. Fixing Heating Tube
3-7. Sample Injection Port Setting
For the procedure for setting the sample injection port, refer to the instruction manual of
each injector.
VF-500 (NSX-5000)
3-10 Installation
VF-500 (NSX-5000)
Measurement 4-1
Section 4: Measurement
This section describes VF-500 parameters. For operation as a system, read the
instruction and operation manuals of the units that constitute the system.
Always check for gas leaks before starting measurement. The gas leak check
procedure varies depending on measurement items and the detector. Refer to the
operation manual of each system for details.
4-1. Parameters
There are VF-500 parameters set in a method. For parameters which are set in a
method, they are reflected into the whole schedule.
4-1-1. Parameters Set in a Method
This section describes VF-500 parameters which are set in a method. Table 4-1 lists the
parameters. For details on how to check parameters, refer to the operation manual.
Some parameters may not be used depending on the system configuration. They are
not displayed. For gas control, refer to “Fig. 4-1. Gas Change Timing Chart”. After
sample injection, the gas between the inner combustion tube and outer combustion tube
is changed to completely burn the organic matter in the inner combustion tube. Then,
the gas is changed again and it returns to the original state.
Table 4-1. Parameters List
Name Contents Setting range Default

Heater Inlet (ºC) Set the temperature of the 0 to 1100 900 *1
temp. inlet side of the electric
furnace.
Outlet (ºC) Set the temperature of the 0 to 1100 900 *1
outlet side of the electric
furnace.
Inlet (Standby) You can set the 0 to 1100 300
(ºC) temperature of the inlet
side of the electric furnace
in an electric furnace
standby state.
Outlet (Standby) You can set the 0 to 1100 300
(ºC) temperature of the outlet
side of the electric furnace
in an electric furnace
standby state.
VF-500 (NSX-5000)
4-2 Measurement

Gas flow Ar (mL/min) Set Ar gas flow. 36 to 500 100 *1
O2 (mL/min) Set O2 gas flow. 36 to 500 500 *1
Ar (Standby) Set Ar gas flow in gas 36 to 500 50
(mL/min) standby.
O2 (Standby) Set O2 gas flow in gas 36 to 500 50
(mL/min) standby.
*1. Varies depending on the system.

Time Ar Time (s) Set the time for which Ar 0 to 999 30
gas should flow into the
inner combustion tube
after sample injection.
O2 Time (s) Set the time for which O2 0 to 999 120
gas should flow into the
after valve selection.
Ar Replace Time Set the time for which Ar 0 to 999 30
(s) gas should flow into the
after valve selection.
Injection
Start End
Ar→O2 valve selection O2→Ar valve selection

Injector Sample (inner tube) (inner tube)
injection
Ar Time O2 Time Ar replace time
Inner
O2
combustion Ar O2 Ar
tube Ar
Outer O2
O2 Ar O2
combustion Ar
tube
O2→ Ar valve selection Ar→O2 valve selection
(outer tube) (outer tube)
Fig. 4-1. Gas Change Timing Chart
VF-500 (NSX-5000)
Troubleshooting 5-1
Section 5: Troubleshooting
This section describes the troubleshooting of the VF-500 unit. When problems are not
solved even by taking countermeasures, contact our local distributor.
CAUTION Cover of the unit

Do not remove the cover of the unit except for our servicemen.
Doing so may cause a fault or electric shock.
5-1. No Power to the Unit
Cause Countermeasure
□ The main power switch on Turn on the main power switch.
the rear of the unit is off.
□ The power cable is Connect the power cable firmly to the power
disconnected from the connector.
power connector.
□ The power plug is not Connect the power plug firmly to the outlet.
inserted properly into the
outlet.
□ Power is not supplied to Check that power is supplied to the outlet by using
the outlet. another instrument.
VF-500 (NSX-5000)
5-2 Troubleshooting
5-2. No Communication with the Unit
□ The power of the unit is off. Turn on the power of the unit by referring to “5-1. No
Power to the Unit”.
□ The USB cable is Connect the USB cable firmly to the communication
disconnected from the connector.
communication connector.
□ The USB cable is broken. Change the USB cable with new one.
□ Communication is stopped. Restart the whole system. When communication does
not recover even by restarting the system, contact our
local distributor.
□ The port setting in the Check the COM port number in “Device Manager” on
application software is the PC, and select the corresponding COM port in the
wrong. application software.
□ VF-500 is not selected in Select VF-500 in the unit configuration in the
“Unit Composition” in the application software.
application software.
5-3. No Temperature Rise of Electric Furnace
□ The error window is Perform operations by following the error message.
displayed in the PC
window.
□ The heater switch is off in Turn on the heater switch.
the PC window.
□ The setting of the power Set the power voltage selector switch on the rear of
voltage selector switch the VF-500 unit.
does not match the power
voltage to be used.
□ The circuit protector for If the circuit protector for heater on the rear of the VF-
heater is operating. 500 unit is projected, then the circuit protector is
operating. The heater circuit may be faulty. Contact
our local distributor.
□ A heater line of the electric The electric furnace needs replacement. Contact our
furnace is broken. local distributor.
VF-500 (NSX-5000)
Troubleshooting 5-3
5-4. No Gas Flow
□ The gas cylinder valve is Open the gas cylinder valve.
closed.
□ Remaining gas is Change the gas cylinder.
insufficient.
□ The gas supply valve is Open the gas supply valve.
closed.
□ Lines are disconnected. Connect the lines firmly.
□ A line is clogged. Check for any clogging in the lines. Replace any
clogged parts.
□ The power switch is off. Turn on the power switch.
□ The gas valve switch is off Turn on the gas valve switch in the PC window.
in the PC window.
5-5. Abnormal Noise during Measurement
□ The secondary pressures Set the same secondary pressure for the Ar and O2
of the Ar and O2 gas gas cylinders within the range of 0.3±0.1 MPa.
cylinders are different from
each other.
□ Foreign particles are Increase the gas flow, and switch the gas of the inner
included in the solenoid combustion tube between Ar and O2 several times.
valve. From the menu, select “Control” - “Gas Controller” -
“VF-500” - “Change Gas”, and change the gas in the
displayed window.
□ The cooling fan is broken. Contact our local distributor.
VF-500 (NSX-5000)
5-4 Troubleshooting
5-6. Start Icon Not Enabled
□ No schedule is set to Click [Prepare] in a schedule to set the schedule to
“Measurement schedule”. “Measurement schedule”. Parameters are transmitted
into the unit and the unit is ready after stabilization.
□ All steps in the schedule Add a new step into the schedule.
are already performed.
□ There is no communication Select “File” - “Connect” of the menu to reconnect to
with the injector or it.
detector.
□ The temperature of the Wait until the temperature of the electric furnace
electric furnace has not reaches the target temperature and becomes stable.
reached the target
temperature.
□ There is no gas flow. Flow gas, and wait until the flow becomes stable.
When the gas does not flow, refer to “5-4. No Gas
Flow”.
5-7. Troubles Occur after Changing of a Line or Cylinder
Possible causes are dirt in the lines and impurities in gas. Troubleshooting is as follows.
• Raise gas pressure slightly and purge lines.
• When troubles are not solved even by purging, change the gas cylinder with a
new one.
VF-500 (NSX-5000)
Troubleshooting 5-5
5-8. Incomplete Combustion Occurred
When oxygen becomes insufficient due to rapid combustion or the combustion

temperature is insufficient, incomplete combustion occurs and soot is generated. Soot
adheres to the sample gas path and, depending on the composition of the sample, may
become adhesive. Conduct maintenance by referring to the daily and periodical
inspection items in “Maintenance and Inspection”. This section describes the
maintenance of the combustion tube. When there is no improvement even by taking the
countermeasures or the combustion tube is devitrified severely, change it with a new one.
WARNING Prevention of fire and burns

Washing with an organic solvent may cause a fire. It may also cause burns
when the temperature of the electric furnace is raised. Be sure to turn off
the power of the unit and let the electric furnace cool sufficiently before
starting an operation.
When using a burner, take sufficient care and perform operations with
experienced people.

Combustion tube is glass. If it is dropped or strong pressure is put on it, an
accident may be caused. Take enough care in handling.
Contamination cause Countermeasure

Contamination due to Remove the quartz wool and filler, and remove the
incomplete contamination by combustion removal with a burner or the
combustion like. Then, change the quartz wool and filler with new ones.
Contamination due to Remove the quartz wool and filler, and carefully wipe the
organic samples inside of the combustion tube with an acetone-soaked cloth.
Then, after acetone vaporizes, change the quartz wool and
filler with new ones.
Contamination due to Remove the quartz wool and filler, and wash the inside of the
inorganic samples combustion tube with a test tube brush or the like and neutral
detergent. Then, wash it fully with tap water, rinse with pure
water, and dry it. After it dries, put quartz wool and filler.
VF-500 (NSX-5000)
5-6 Troubleshooting
VF-500 (NSX-5000)
Error Messages and Measures 6-1
Section 6: Error Messages and Measures

This section describes displayed error messages and measures when problems occur.
WARNING Indication of WARNING

When “WARNING” is displayed in the PC monitor, this indicates the risks
of serious accidents. When these messages are displayed, deal with the
problems immediately.
When an error occurs, a message is displayed on the PC monitor. When the problem is
not solved even by taking countermeasures, check the version of the application software
from “Help” of the menu and contact our local distributor.
VF-500 Error Messages
Table 6-1 shows VF-500 error messages
Table 6-1. VF-500 Error Messages
ERROR Error messages Countermeasure

No.
01 Electric furnace Since thermocouple disconnection was detected
thermocouple while the electric furnace was under control, the
disconnection system was shut down.
Turn off the VF-500 power switch and contact our
distributor.
02 Electric furnace bimetal Since the electric furnace temperature rose and
switch operation the bimetal switch operated while the electric
furnace was under control, the system was shut
down.
distributor.
03 Electric furnace Since thermal fuse disconnection was detected
thermal fuse while the electric furnace was under control, the
disconnection system was shut down.
distributor.
04 The detected Since the detected temperature is 0 C or less
temperature of the while the electric furnace was under control, the
electric furnace is 0 C system was shut down.
or less. Turn off the VF-500 power switch and contact our
distributor.
VF-500 (NSX-5000)
6-2 Error Messages and Measures

No.
05 The detected Since the detected temperature is 1150 C or
temperature of the more while the electric furnace was under
electric furnace is 1150 control, the system was shut down.
C or more. Turn off the VF-500 power switch and contact our
distributor.
07 The electric furnace Since the detected temperature change was over
control temperature is ± 50 C of the preset value after stabilization, the
out of the range. system was shut down.
distributor.
09 Electric furnace cooling Since the electric furnace fan stopped while the
fan stop electric furnace was under control, the system
was shut down.
distributor.
11 Argon gas flow The argon gas flow decreased while gas
decrease monitoring was in progress and the system was
shut down.
Check the cause.
12 Oxygen gas flow The oxygen gas flow decreased while gas
decrease monitoring was in progress and the system was
shut down.
Check the cause.
13 Flow control error The gas flow was more than +5% of the preset
(upper limit) value while gas monitoring was in progress and
the system was shut down.
distributor.
14 Flow control error The gas flow was below -5% of the preset value
(lower limit) while gas monitoring was in progress and the
system was shut down.
distributor.
15 The gas control unit The gas control unit sensor problem occurred
sensor problem while gas monitoring was in progress and the
occurred while gas system was shut down.
monitoring was in Turn off the VF-500 power switch and contact our
progress. distributor.
16 The gas control unit The gas control unit data was incorrect while gas
data was incorrect monitoring was in progress.
while gas monitoring Turn off the VF-500 power switch and contact our
was in progress. distributor.
VF-500 (NSX-5000)

No.
23 The invalid command The invalid command was received while the
was received while the system was down.
system was down. Restart the system. When the same error occurs
even after the restart, contact our local
distributor.
24 The valve change The valve change command was received during
command was measurement.
received during Restart the system. When the same error occurs
measurement. even after the restart, contact our local
distributor.
25 The purge valve control The purge valve control command was received
command was while purge monitoring was in progress.
received while purge Restart the system. When the same error occurs
monitoring was in even after the restart, contact our local
26 Gas monitoring Gas monitoring command was received while
command was gas control is unready.
received while gas Restart the system. When the same error occurs
control is unready. even after the restart, contact our local
distributor.
28 Electric furnace Electric furnace thermocouple disconnection was
thermocouple detected.
disconnection Turn off the VF-500 power switch and contact our
distributor.
29 Electric furnace bimetal The electric furnace temperature rose and the
switch operation bimetal switch operated.
distributor.
30 Electric furnace The electric furnace thermal fuse was
thermal fuse disconnected.
disconnection Turn off the VF-500 power switch and contact our
distributor.
31 The detected The detected temperature was 0 C or less.
temperature of the Turn off the VF-500 power switch and contact our
electric furnace is 0 C distributor.
or less.
32 The detected The detected temperature was 1150 C or more.
temperature of the Turn off the VF-500 power switch and contact our
electric furnace is 1150 distributor.
C or more. (1100 C
furnace)
VF-500 (NSX-5000)

No.
34 Electric furnace cooling The electric furnace cooling fan stopped.
fan stop Turn off the VF-500 power switch and contact our
distributor.
42 Electric furnace (Inlet) The electric furnace (Inlet) temperature
temperature parameter parameter is out of the range.
error The application software version may be
inconsistent with the system controller or the VF-
500 unit software. Check each version and
contact our local distributor.
43 Electric furnace The electric furnace (Outlet) temperature
(Outlet) temperature parameter is out of the range.
parameter error The application software version may be
44 Parameter range error The gas flow or gas change time is out of the
range.
The application software version may be
45 Memory reading error The error occurred when registered data was
read.
Turn off the VF-500 power switch and restart the
system. When the same error occurs even after
the restart, contact our local distributor.
51 Gas control unit 1 The gas control unit communication error
communication occurred.
problem (parameter Contact our local distributor.
error)
problem (parameter Contact our local distributor.
error)
problem (flow Contact our local distributor.
acquisition error)
problem (flow Contact our local distributor.
acquisition error)
VF-500 (NSX-5000)

No.
57 Flow control error The gas flow was more than +5% of the preset
(upper limit) value while gas monitoring was in progress.
Restart the system. When the same error occurs
distributor.
58 Flow control error The gas flow was below +5% of the preset value
(lower limit) while gas monitoring was in progress.
distributor.
59 The gas control unit The gas control unit sensor problem occurred
sensor problem while gas monitoring was in progress.
occurred while gas Restart the whole system. When the same error
monitoring was in occurs even after the restart, contact our local
60 The gas control unit The gas control unit data was incorrect while gas
data was incorrect monitoring was in progress.
while gas monitoring Restart the whole system. When the same error
was in progress. occurs even after the restart, contact our local
distributor.
80 The electric furnace The electric furnace door is open.
door is open. Close the door.
99 Initialization in progress Please wait for a while.
VF-500 (NSX-5000)
System Controller Error Messages
Table 6-2 shows system controller error messages
Table 6-2. System Controller Error Messages
ERROR
Error messages Countermeasure
No.
21 Invalid command The unknown command was received. The
reception application software may be inconsistent with the
system controller version.
Check each version and contact our local
distributor.
22 Invalid command The command was received before unit
reception registration.
Turn on the power switch again.
23 Invalid command The command was received during measurement
reception and it can not be dealt.
even after the restart, the application software
may be inconsistent with the system controller
version. Check each version and contact our
local distributor.
46 Communication time- The command reception timeout error occurred.
out error Check the power and communication cables
connection. Check the unit status.
47 BCC error The system controller detected the BCC error of
command reply.
Check the communication cable connection.
inconsistent with the system controller or the
peripheral device software. Check each version
and contact our local distributor.
48 BCC error The system controller detected the BCC error of
status request command reply.
VF-500 (NSX-5000)
ERROR
Error messages Countermeasure
No.
49 BCC error The connection device detected the BCC error of
the command.
79 No COM port detection The system can not communicate with the PC.
Check the power and communication cables
connection. Check the unit status.
99 Initialization in progress Please wait for a while.
VF-500 (NSX-5000)
Maintenance and Inspection 7-1
Section 7: Maintenance and Inspection

This section describes the maintenance and inspection to use the VF-500 unit safely in
the proper conditions. Perform maintenance and inspection on not only the VF-500 unit
but also other units that constitute the system.
7-1. Daily Inspection and Maintenance
Table 7-1 shows the daily inspection items. If any problems are found, solve the problem
and re-check the unit. When problems cannot be solved or they may be inside the unit,
CAUTION Daily inspection and

maintenance
Be sure to perform daily inspection and maintenance before the use of the
unit.
Failure to do so may lead not only to the performance reduction but also to
serious accidents.
Table 7-1. Daily Inspection Items
No. Item Contents

1 Check of the condition of Check that the combustion tube outlet is not
the combustion tube contaminated with soot.
outlet
2 Gas leakage check Check that gas is not leaking, using the flow meter for
gas leak check.
The details of each daily inspection item and maintenance are as follows.
Check of the Condition of the Combustion Tube Outlet
Visually check combustion tube outlet for soot contamination caused by incomplete
combustion. If it is contaminated, remove the combustion tube from the electric furnace,
remove quartz wool and filler, and wash the combustion tube. To wash combustion tube,
refer to “7-2. Periodical Inspection and Maintenance”.
Gas Leakage Check
Connect the ball joint of a flow meter for gas leak check to the combustion tube outlet and
check that the preset gas flow agrees with the indicated value of the flow meter. For
details on gas leakage check, refer to the operation manual.
VF-500 (NSX-5000)
7-2 Maintenance and Inspection
7-2. Periodical Inspection and Maintenance
Table 7-2 shows the periodical inspection items. If any problems are found, solve the
problem and re-check the unit. When problems cannot be solved or they may be inside
the unit, contact our local distributor.
CAUTION Periodical inspection and

maintenance
Always conduct periodical inspection and maintenance in the specified
cycle.
Failure to do so may lead not only to the performance reduction but also to
serious accidents.
Table 7-2. Periodical Inspection Items
No. Item Contents Frequency

1 Check of the Visually check for contamination and Every 2
appearance of the unit dust. weeks
2 Check of the condition Visually check the condition of quartz Every 3 to
of quartz wool and filler wool and filler in the combustion tube. 4 weeks
in the combustion tube
3 Check of the condition Visually check the condition of the Every
of the combustion tube combustion tube. month *
4 Cleaning of air vents Clean the punching part of the electric Every 3
furnace door and the area around the months
rear exhaust fan.
5 Check of gas flow Check that Ar and O2 gas flow Every year
indication indications are correct.
6 Change of gas Change the gas purification filters with Every year
purification filters new ones.
7 Check of the electric Check that the electric furnace Every year
furnace temperature temperature displayed on the PC is
correct.
8 Overall inspection Our local distributor conducts periodical Every year
inspections upon request.
* The check frequency differs depending on the samples to be measured.
The details of each periodical inspection item and maintenance are as follows.
VF-500 (NSX-5000)
Check of the Appearance of the Unit
Visually check the unit for contamination and dust every two weeks. If there is
contamination and dust, clean the unit.
POINT Unit cleaning

When cleaning the unit, do not use organic solvents.
Doing so may cause the coating of the unit to peel off.
Check of the Condition of Quartz Wool and Filler in the Combustion Tube
Visually check the condition of quartz wool and filler in the combustion tube every three
to four weeks. If there is a residue on the quartz wool in the inner tube or the quartz wool
has shrunken or been powderized, change it with new quartz wool. However, the
condition check needs to be conducted more frequently when alkaline samples or
samples containing metals are measured. If the condition of the filler has changed,
change or renew it. For the change of the quartz wool and filler, refer to the operation
manual. If any abnormalities are found in the combustion tube during visual check, wash
or change the combustion tube.
Check of the Condition of the Combustion Tube
Visually check the condition of the combustion tube every month. However, the condition
check needs to be conducted more frequently when alkaline samples or samples
containing metals are measured, because they facilitate devitrification of the combustion
tube. When the combustion tube is contaminated, wash it as follows.
(1) Remove the quartz wool and filler, and wash and brush the combustion tube with a
brush or the like and neutral detergent. If the contamination cannot be removed with
a brush, immerse it in washing solution overnight or longer, and then wash it again.
(2) After washing, rinse the combustion tube thoroughly with pure water and dry it
before use.
When the combustion tube is devitrified and mechanical strength is determined to be low,
change the combustion tube with a new one immediately. For the change method, refer
to “3-6. Combustion Tube Setting”.
VF-500 (NSX-5000)
CAUTION Combustion tube devitrification

When a combustion tube is devitrified, its mechanical strength decreases
and it may break. As a result, accidents or injuries may be caused.
The term “devitrification” refers to a condition where the combustion tube
color has turned white. When a combustion tube is devitrified, especially
when fine cracks are in the devitrified part, the mechanical strength is low.
Change it immediately.
Cleaning of Air Vents
Clean the punching part of the front door of the unit and the area around the air vents of
the rear fan with a cleaner every three months. If the unit continues to be used with dust
adhered around the air vents of the unit, the cooling time of the electric furnace may
become longer or temperature rise around the electric furnace may cause a system down.
When the unit in a dusty environment, cleaning needs to be conducted more often.
Check of Gas Flow Indication
Check that Ar and O2 gas flow indications are correct every year. Check that the flow
indication agrees with the value of the flow meter.
(1) Connect the ball joint of the combustion tube outlet to the flow meter for gas leak
check.
(2) Set a gas flow of 100 mL/min for Ar and 300 mL/min for O2, and check that the flow
meter for gas leak check indicates 400±40 mL/min.
Change of Gas Purification Filters
Change the gas purification filters with new ones every year. For the change method,
refer to “3-5-2. Line Connection”.
VF-500 (NSX-5000)
Check of the Electric Furnace Temperature
Check every year that the electric furnace temperature displayed on the PC is correct.
Insert a thermometer into the combustion tube center by the following procedure. Check
that the electric furnace temperature displayed on the PC is within the range.
(1) Set a commercial thermometer (R-type thermocouple) into the combustion tube
center by referring to “Fig. 7-1. Thermometer Setting”. Always use a calibrated
thermometer and a calibrated display. Set the thermometer at a center position,
viewed either from the direction of the depth of the electric furnace or the direction
of the radius of the combustion tube. To prevent heat from escaping through the
inlet of the electric furnace, implement heat insulation at the electric furnace inlet.
Insertion direction of
the thermometer
Heat insulation
Fig. 7-1. Thermometer Setting
(2) Create a new method and schedule, and set the inlet and outlet temperatures of the
electric furnace to 900 degrees Celsius using a parameter setting.
(3) Turn on the electric furnace, and raise its temperature.
(4) Check the temperature indicated by the thermometer 30 minutes after the inlet and
outlet temperatures displayed in the PC window reaches 900 degrees Celsius. If the
thermometer indicates a temperature within 900±50 degrees Celsius, then the
indication is normal. If the temperature is out of the range, contact our local
distributor.
Overall Inspection
Contact our local distributor. They determine inspection items and others according to the
condition of the unit and the use frequency.
VF-500 (NSX-5000)
7-3. Storage of the Unit
Store VF-500 as follows when it is not used for long time.
The cautions for storing the unit on a table are as follows.

• Disconnect the power cable and gas lines.
• Disconnect cables for connection with each unit.
• Remove optional units from the VF-500 unit.
• Remove both lines of the gas inlet and outlet of the gas purification filter and put
the closing plugs.
• Seal tube ends with parafilm and store them to avoid the inside contamination.
• Put the cover over the whole unit.
The cautions of the storage place are as follows.

• Store the unit in a place where room temperature is 0 to 45 degrees Celsius.
• Store the unit in a place where humidity is 80%RH or less with no condensation.
• Store the unit in a place free from much dust.
• Store the unit in a place free from corrosive gas.
• Store the unit in a place where fire is not used.
• Store the unit in a place free from direct sunlight.
• Store the unit in a place free from strong vibration and continuous weak vibration.
• Store the unit in a place free from strong electromagnetic field.
• Store the unit in a horizontal and stable place.
VF-500 (NSX-5000)
VF-500 (NSX-5000)
Disposal of the Unit 8-1
Section 8: Disposal of the Unit

This section describes how to dispose of a used VF-500 unit for some reason.
If you dispose of the used unit, comply with the ordinances of your local government.
Please directly contact your local government for details.
If there are any unclear points, contact our local distributor.
VF-500 (NSX-5000)
8-2 Disposal of the Unit
VF-500 (NSX-5000)
Specifications 9-1
Section 9: Specifications
This section describes VF-500 unit specifications.
9-1. VF-500 Unit Specifications
Table 9-1 shows VF-500 unit specifications.
Table 9-1. VF-500 Unit Specifications
Item Specifications
Model VF-500
Electric furnace Openable electric furnace: 2-section type (inlet/outlet)
Temperature: Maximum 1100 C
Gas Ar gas (with a purity of 99.98% or greater, 0.3±0.1 MPa)
O2 gas (with a purity of 99.7% or greater, 0.3±0.1 MPa)
Dimensions About 500 (W) × 430 (D) × 500 (H) mm
Weight About 35 kg
Power 100/115 VAC, 50/60 Hz: 1100 VA
230/240 VAC, 50/60 Hz: 1800 VA
Interface COMPUTER: USB 2.0
ACCESORIES: Communication cable
I/O: Input/Output connector
IN1 to 4: Non-contact input
O1: Non-contact output (for system down errors)
O2 to O4: Non-contact output
AIN1: Analog input
AIN2: Analog input
Temperature 15 to 35 C
Humidity 80%RH or less (No condensation)
Overvoltage CategoryⅡ (IEC61010-1)
category
Pollution degree 2 (IEC61010-1)
VF-500 (NSX-5000)
9-2 Specifications
VF-500 (NSX-5000)
Guarantee Provisions 10-1
Section 10: Guarantee Provisions

10-1. Guarantee Provisions for Japan
Guarantee Terms
1. Guarantee period is one year from the date of delivery.
2. If the product is used in Japan and is used under normal usage during the
guarantee period and a problem occurs, Nittoseiko Analytech will repair
defective parts or replace them with new ones or equivalents free of charge.
The replaced old parts will be owned by Nittoseiko Analytech.
3. In the following cases, repairs will be charged even within the guarantee period:
(1) Failure due to improper handling or misuse
(2) Failure due to handling, use, storage, or breakage by storage that deviates
from the design and specification conditions
(3) Failure and damage due to transportation after delivery, dropping or
vibration during movement
(4) Failure caused by modification and repair by a person other than a
serviceman commissioned by the Company
(5) Replenishment of consumables and naturally consumed parts*
(6) Failure and damage due to accidental force such as fire, flood,
earthquakes, lightning, salt damage, abnormal voltage, and other natural
disasters
(7) Failure due to use in an environment outside the specifications
(8) Failure due to use with options and consumables other than certified
products
(9) Insufficient maintenance management of cleaning, maintenance,
inspection, and use of consumables other than those specified by the
Company.
(10) Other failures that are not considered to be our responsibility
* Items listed in " Consumables" at the end of the section are consumables.
4. Judgment as to whether or not failures correspond to free repair depends on
the company or a person commissioned by the company.
5. The contact for the failures shall be Nittoseiko Analytech or its agent.
6. Methods of returning defective products will be decided in consultation with the
contact place each time.
VF-500 (NSX-5000)
10-2 Guarantee Provisions
7. Nittoseiko Analytech does not make any express or implied guarantees

(including implied guarantees regarding merchantability or suitability for a
specific purpose) other than those expressly provided in the guarantee
provisions. Nittoseiko Analytech disclaims any guarantee anything other than
that stated in the guarantee provisions. Even if implied guarantees are applied
by law, they are limited to those specified in the guarantee provisions.
Guarantee Limitations
Nittoseiko Analytech is not liable for any damages (including lost profits and other
indirect damages) caused by the product or its use. Nittoseiko Analytech is not
responsible for any claims from third parties or the ones made by customers on
behalf of third parties.
These limitations shall apply regardless of whether the claim for damages or other
claims is based on the guarantee provisions, tort (including negligence and strict
liability), contractual claims or other causes of claims.
These limitations are valid even if Nittoseiko Analytech or its authorized agent is
aware of the possibility of such damage. However, they do not apply to damages
that Nittoseiko Analytech is liable for under the Product Liability Act.
VF-500 (NSX-5000)
Guarantee Provisions 10-3
10-2. Guarantee Provisions for Products Sold Overseas
Guarantee Terms
1. If you purchased a product from a Nittoseiko Analytech distributor outside
Japan, please contact the distributor for inquiries about the guarantee period
and terms as well as for failures.
Please note that Nittoseiko Analytech may not support even if you contact us
directly.
2. The preceding paragraph does not apply to inquiries regarding damages
(limited to those for which Nittoseiko Analytech may not be exempted in whole
or in part) related to Product Liability Act applicable to Nittoseiko Analytech.
VF-500 (NSX-5000)
10-4 Guarantee Provisions
VF-500 (NSX-5000)
Consumables 11-1
Section 11: Consumables

This section describes consumables related to the VF-500 unit. For consumables of the
system, refer to the instruction manuals of respective units. For information for purchasing
consumables, contact our local distributor.
11-1. VF-500 Consumables
Table 11-1 lists VF-500 consumables.
Table 11-1. VF-500 Consumables List
No. Parts name Parts Quantity Picture

number
1 Fluororesin tube φ4/2, TX3RPP 1 pc
10 m
2 Connector φ6/4 QF2JGT 2 pcs
3 Shield plate FN2RIN 2

pcs/set
4 Clip (long) φ18 DT1BJC 1 pc
5 Thermal fuse 93 °C FU93TT 2 pcs

(with fluororesin tube)
6 Female ball joint, φ12.5 FN2BFE 1 pc
7 Ball joint clip, φ12 VABCLP 2 pcs
VF-500 (NSX-5000)
11-2 Consumables
No. Parts name Parts Quantity Picture

number
8 Quartz wool 10 g TNQWL 1 pc
9 Quartz wool poker TX2RTL 1 pc
10 Gas purification filter TS6GPR 1 pc
11 O-ring P-16 TX020 5 pcs
VF-500 (NSX-5000)

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Control Number ZN5VFME-02

Electromagnetic Compatibility Directive: 2014/30/EU

Model Name : Vertical Furnace Model VF-500

Standard to which Conformity is Declared:

EN 61000-6-4:2019 : Generic standards-Emission standard for industrial environments

EN 61000-6-2:2019 : Generic standards-Immunity standard for industrial environments

EN 61010-1:2010/A1:2019 : Safety requirements for electrical equipment for measurement,

EN IEC 63000:2018 : Technical documentation for the assessment of electrical and

Name of Manufacturer : NITTOSEIKO ANALYTECH CO., LTD.

Manufacturer’s Address : 7-10-1 Chuo-rinkan, Yamato, Kanagawa 242-0007, Japan

EU Office Address : MITSUBISHI CHEMICAL EUROPE GmbH

Type of Equipment : Laboratory Equipment

Month and year of CE Marking : June, 2017

Date of issue: 01 . 04 . 2022

Place of issue: Japan

Take care of the following points about this manual.

(1) Do not reprint this manual wholly or partially without permission.

(2) The contents may be changed without notice.

About This Manual

This instruction manual is composed as follows.

The elements of windows are expressed as follows.

The selection of a menu item, a button or an icon is expressed as follows.

Refer to “SAFETY PRECAUTIONS” for the indications of warnings and cautions.

This manual uses the following terms.

Indications of Safety Precautions

Warnings and Cautions

Warning or Caution label Attached place

It is attached on the front of

It is attached on the front of

It is attached around the

It is attached on the rear of

It is attached at the gas

When installing the unit, always observe the following precautions.

WARNING Room temperature

WARNING Air conditioning

WARNING Direct sunlight

WARNING Turning off the electric furnace

CAUTION Corrosive gas

CAUTION Electromagnetic field

CAUTION Installation surface

CAUTION Earth terminal

CAUTION Gases to use

CAUTION Connection method

CAUTION Gas lines

CAUTION Check of O-rings

CAUTION Combustion tube breakage

WARNING Prohibition of unattended

WARNING Microsyringe to use

WARNING Combustibles and combustible

WARNING Power plug

WARNING Power cable

WARNING Cables and connectors on the

WARNING For protection

WARNING Gas leakage check before using

WARNING Hot electric furnace and

WARNING Prevention of fire and burns

WARNING Indication of WARNING

CAUTION Cover of the unit

CAUTION Combustion tube breakage