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PREFACE

PETRONAS Technical Standards (PTS) publications reflect the views, at the time of publication,
of PETRONAS OPUs/Divisions.

They are based on the experience acquired during the involvement with the design, construction,
operation and maintenance of processing units and facilities. Where appropriate they are based
on, or reference is made to, national and international standards and codes of practice.

The objective is to set the recommended standard for good technical practice to be applied by
PETRONAS' OPUs in oil and gas production facilities, refineries, gas processing plants, chemical
plants, marketing facilities or any other such facility, and thereby to achieve maximum technical
and economic benefit from standardisation.

The information set forth in these publications is provided to users for their consideration and
decision to implement. This is of particular importance where PTS may not cover every
requirement or diversity of condition at each locality. The system of PTS is expected to be
sufficiently flexible to allow individual operating units to adapt the information set forth in PTS to
their own environment and requirements.

When Contractors or Manufacturers/Suppliers use PTS they shall be solely responsible for the
quality of work and the attainment of the required design and engineering standards. In
particular, for those requirements not specifically covered, the Principal will expect them to follow
those design and engineering practices which will achieve the same level of integrity as reflected
in the PTS. If in doubt, the Contractor or Manufacturer/Supplier shall, without detracting from his
own responsibility, consult the Principal or its technical advisor.

The right to use PTS rests with three categories of users :

1) PETRONAS and its affiliates.


2) Other parties who are authorised to use PTS subject to appropriate contractual
arrangements.
3) Contractors/subcontractors and Manufacturers/Suppliers under a contract with
users referred to under 1) and 2) which requires that tenders for projects,
materials supplied or - generally - work performed on behalf of the said users
comply with the relevant standards.

Subject to any particular terms and conditions as may be set forth in specific agreements with
users, PETRONAS disclaims any liability of whatsoever nature for any damage (including injury
or death) suffered by any company or person whomsoever as a result of or in connection with the
use, application or implementation of any PTS, combination of PTS or any part thereof. The
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to PETRONAS that may issue PTS or require the use of PTS.

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arrangements, PTS shall not, without the prior written consent of PETRONAS, be disclosed by
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The copyright of PTS vests in PETRONAS. Users shall arrange for PTS to be held in safe
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to ascertain how users implement this requirement.
CONTENTS
INTRODUCTION
Modifications to the CPI
Example calculation of plate pack
(a) Oil separation
(b) Type of flow between plates
(c) Stability of flow between plates
Relation overweight of oil and depth oil/water
interface in CPI
Diagram Relation Particle size/settling velocity
Main drawings (not to scale)

Corrugated Plate Interceptor:

S 14.040 Construction - General Arrangement


S 14.041 Start-up and operation (text)
S 14.042 Assembly of Details 1 up to 11
S 14.043 Assembly of Details 12 up to 16
S 14.044 Assembly of Details 17 - 18 and 19
S 14.045 Flow Distribution Baffle
S 14.046 General Arrangement one plate assembly
S 14.047 Multiple Bay Arrangement
Appendix 1. Prefabricated steel CPI basins.
Appendix 2. CPI with inlet weir:

S 14.021 Construction, Start-up, Operation


S 14.022 General arrangement (2 bays)
S 14.024 Design principles
Detail drawings
T 960299 Assembly of steel parts (not on scale)
T 960300 Detail weir
T 960301 Detail skimmer
T 960302 Connection flanges for skimmer
T 960303 Trash pan
T 960304 Overflow outlet pipes
T 960305 Trash rack
T 960306 Detail suspension sludge suction pipe
T 960307 Detail hand railing
T 960327 Flow distribution baffle
INTRODUCTION

The basic treatment for de-oiling refinery waste water is done in gravity-type oil interceptors. The
conventional oil interceptor consists of a basin through which the waste water flows so slowly that oil
globules have time to rise to the surface. At the end of the basin, the floating oil is retained by a baffle
and skimmed off.

By subdividing an interceptor basin into longitudinal channels with parallel plates, its separating
capacity can be increased. If for instance the basin is subdivided into ten layers, the maximum path
(raising height) which an oil globule has to travel before reaching a coalescing surface is reduced to
one tenth of the depth of the water in the basin.

An additional advantage is that, at flow velocities such as used in conventional interceptors, there is
laminar flow between the plates. Laminar flow is ideal for gravity-type separation and it cannot be
obtained in the large cross section of conventional interceptors.

Good results have been obtained with the PPI (Parallel Plate Interceptor), which has found wide
application. The separation compartment of the PPI consists of a rectangular basin in which plates are
inserted at an angle of 45° in cross direction and parallel to the horizontal bottom in the longitudinal
direction.

Ten years' experience with the PPI has led to the development of the CPI (Corrugated Plate
Interceptor).The latter interceptor is cheaper, it overcomes some operational difficulties experienced
with the PPI and it is better suited for a corrosion or acid proof construction.

This report gives information on the design and operation of the CPI. A set of "to scale" drawings can
be requested from PETRONAS.

MODIFICATIONS TO THE CPI

Since its introduction some 13 years ago, development of the CPI has continued. Years of experience
and a good feedback from CPI users has resulted in the introduction of a number of modifications, to
the original version of the CPI, which result in simplified construction, operation and maintenance and
thus an improved performance of the CPI.

It should be noted however, that under certain circumstances application of the original version of the
CPI is still valid. The modifications and the motivation for the introduction of these modifications are
described below:

Theoretically speaking the weir is possibly not the most ideal inlet device for a CPI, but it was adopted
since it displays certain advantages:

1. It is a simple way to distribute flow equally over several basins, especially for large batteries
of CPI's, and to allow for further settling of the structure.

2. It prevents accumulated oil from flowing back to the drainage system.

3. The difference in water levels on both sides of the weir is so small that it can be considered to
be semi- submerged weir, thus minimizing dispersion (this compares favorably with normal
weirs).

Due to changes in operating policies of the CPI, by refineries, it is now possible to introduce
modifications to the CPI inlet. The original policy was to generate a thick oil layer in order to skin off oil
free water (but at the same time accepting some emulsion forming at the oil/water interface and thus
possibly more pollution).

For ease of operation, however, skimming is now carried out on a more frequent basis (thus accepting
water-contaminated oil in the slops system). This change in operating policy has also resulted in a
improvement in effluent quality.
Example calculation of plate pack (outside dimension 1.00 x 1.00 x 1.75 m)

a) Oil separation

Interval of plates: d = 20 mm
Maximum rising height: H = d√2 = 28 mm
Total length of plates in flow direction: Ltotal = 1.50 m
Effective length of plates = Ltotal minus length required
for in and outflow: L eff = 1.25 m
Effective cross section: F = 1.00 x 0.90 = 0.90 m2

Throughput: Q = 30 m3/h (normal load on one plate pack)

Q 30 x 103
Flow velocity: V w = = = 9.26 mm / sec
F 0.9 x 3600
Overflow rate:

h x Vw 28 x 9.26
Vr = = = 0.2 mm/sec which means
L 1500
that oil globules with a rising velocity equal to or more than 0.2 mm/sec are completely
intercepted.

b) Type of flow between plates

Interval of plates: d = 20 mm
Effective cross section: F = 0.9 m2
Throughput: Q = 60 m3/hr (maximum load on one plate pack)

Q 60 x 103
Flow velocity: V w = = = 18.5 mm / sec
F 0.9 x 3600

Area between 2 plates 20 x 1000


Hydraulic Radius = = = 10 mm
Wetted perimeter 2000

Kinematic viscosity at 20° C water temperature:

υ = 1.0 x 10 m2/sec
-6

V. R. 0.0185 x 0.01 x 10 6
Reynolds No. : Re = =
υ 10
.

180 < 400 which means that at 20° C water temperature there is laminar flow between
the plates at a throughput of 60 m3/h.
Relation: Overheight of oil and depth oil/water interface in CPI

(S w − S o )
∆ho = hw
So
in which :

∆ ho = overheight of oil above water level at outlet weir


hw = depth of oil/water interface (maximum 70 cm)
Sw = specific density of water
So = specific density of oil

It is noted that under normal conditions, the overflow height of oil above the edge of the
skimmer is less than the overflow height of water above the edge of the outlet weir,
because less oil than water will enter the CPI.

Assuming the overflow heights are the same, then hw max.


will be reached when So = 940 and Sw = 1000

For oils with So > 940, the difference in level of the oil

skimmer and the outlet weir (on drawing 5 cm) can be decreased with the disadvantage that
at the maximum load (60 m3/h per plate pack) over a long period, all oil may be skimmed off
and water may enter the oil sump.

c) Stability of flow between the plates

V2
For stable flow: Froude No. : F = . −5
> 110
R. g
(in which g = acceleration caused by the force of gravity)

∴ V > 10 X R x g = 10 x 0.01 x 9.81 x 10 = 0.981 mm2/sec2


2 -5 -5 6

∴ V > 0.99 mm/sec

0.99 x 0.9 x 3600


∴Q>VXF= = 3.2 m3 / h
1000

Consequently for a plate interval of 20mm, there is stable flow between the plates at a
throughput of more than 3.2 m3/h.

For a plate interval of 39 mm there is stable flow at a throughput of more than 4.5 m3/h.
APPENDIX 2

CPI WITH INLET WEIR

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