Vacuum Freeze Drier

Model No.: LGJ-12G

LGJ-12G
Technical Specifications

Technical Specs LGJ-12G

Standard Type Capping Type
Effective Shelf Area 0.125m²
Standard Cold Trap Temperature ≤ -83℃ (No-load, environment ≤30℃)
Limitation Cold Trap Temperature ≤ -86℃ (No-load, environment ≤25℃)
Standard Vacuum Level ≤5Pa (No-load)
Limitation Vacuum Level ≤1Pa (No-load)
Cooling Rate of Shelf Less than 60 Mins from 20℃ to -40℃ (No-load)
Cooling Rate of Cold Trap Less Than 20 Mins from 20℃ to -40℃ (No-load)
Vacuum Pumping Rate Standard Atmospheric Pressure Down to 5Pa ≤ 10 Mins (no load)
Temperature Range of Material Shelf -50℃ to +70℃
Maximum Water Capture 4 KG
Shelf Size 325mm×385mm
Shelves 1
Spacing of the Shelves 160 mm
φ22mm Penicillin Bottles 240
φ16mm Penicillin Bottles 460
Optimal Handling for Solution Material 2.0L
Exterior Dimensions (W×D×H) 930mm×740mm×660mm
Weight 135 KG
Power Supply AC 220V/230V 50Hz
Power 2100W
Temperature to Place ≤ 30℃

Advantages

• Personalized Service
We provide personalized and accurate solutions according to user‘s requirements and material
characteristics, through one to one communication and experimental analysis.

• Modular Design
Modular design for our products that makes advantages of convenient installation and transportation,
flexible configuration, simple operation and reliable quality.

• Efficient Treatment
Digital dynamic control system to be used, to make it with system optimization and efficient drying for
materials.

• Technical Support
Dedicating technology of freeze drying and development for equipment, fast and reliable after-sales
service.

LGJ-12G
Product Introduction
• Equipped with LINUX software control system, and the freeze-drying
process is automatically controlled by programmable controller, which
can be switched to manual operation in real time to realize the whole
parameter control of the freeze-drying process. In the operation process,
the system automatically monitors, detects and records the data. Record
process ≥ 100, with each process ≥ 36, with 3 levels limited
management. Multiple fixed or customized programs can be recorded,
and monitoring, testing and maintenance can be reached through the
standard remote system with record trace function.
• Continuously record real-time data, drawing freeze-dried graphs, store data each of one minute
(adjustable). The unit is equipped with USB port for data download and edition.
• CE and NEMA certificated.
• The system is equipped with a variety of sensors, displays the real-time record of vacuum level, cold
trap temperature, material temperature, shelf temperature. An active protection system will
automatically turned on while the unit receiving the abnormal temperature and pressure from the unit,
which the abnormal information is caused by operation error alarm.
• At the end of the automatic operation of freeze-drying or in the process of vacuum pressure loss, the
equipment alarm and automatic operation to protect the material. The equipment is equipped with the
function of vacuum pump maintenance massage sending.
• Freeze-drying in situ, unique equipment design structure, can be applied to all laboratory materials
freeze-drying experiment, freeze-drying chamber inside the corner, surface roughness, shelf flatness, the
chamber inside the material meet pharmaceutical standards, smooth corrosion resistance and easy to
clean.
• The freeze-drying automatic control system adopts PID control for both heating and cooling during the
freeze-drying process, which can automatically achieve repeated pre-freezing, quick freezing and slow
freezing of materials.
• The freeze-drying automatic control system adopts PID control in both heating and cooling during the
freeze-drying process, which can automatically realize the repeated pre-freezing, quick freezing and slow
freezing of materials. The special mechanical process is manufactured to ensure the surface of the shelf
is smooth and the internal circulation channel is the same, so that the intermediate medium (low
viscosity silicone oil, 25℃, 5cSt) is evenly and steadily circulated in the shelf, the temperature is uniform,
and the cold heat conduction is good. Improve freeze-drying efficiency.
• The external cold trap improves the water catching capacity of the equipment, reduces the interference
of the cold trap temperature on the material during the freeze-drying process, ensures the consistency
of the material freeze-drying quality and the stability of the experimental data, improves the freeze-
drying efficiency and reduces the energy loss.
• Adopts imported compressor double stack refrigeration technology, international standard green
refrigerant, rapid refrigeration, low cold trap temperature, strong water capture capacity.
• Equipped with auto-defrosting function.
LGJ-12G
Model Type Selection

• Drying Chamber Device Selection

Standard Type: Suit for bulk materials (e.g. powder, granule and solution).
Capping Type: Suit for penicillin bottled materials.
Multi-manifold Bottles Hanging Type: Suit for eggplant-shaped bottled and wide mouth bottled materials,
or multiple materials drying.

• Optional Accessary
Multi-manifold Bottles Hanging Device,
Bottles (Wide Mouth Bottle and Eggplant-shaped Bottles),
Holder for Ampoule Bottles

Imported Vacuum Pump,

High Speed Vacuum Pump Oil,
Vacuum Pump Exhaust Port Oil Mist Filter,
Vacuum Pump Inlet Dust Filter

Bottle Sealer for Ampoule Bottles,

Capping Machine for Penicillin Bottles

Eutectic Point Tester,

Charging Port for Inert Gas.

Capping Device Multi-manifold Bottles Hanging Device

Control System
The control system is composed of programmable logic controller, man-machine interface device, sensor,
terminal relay and digital to analog conversion module. The industrial intelligent control software is
based on professional programmable controller and developed by advanced configuration software for
vacuum freeze – drying equipment. It can display the system status, process flow, alarm point and
operation situation of each component, and can be monitored remotely.

• It can automatically control the whole freeze-drying process with one key, and also can realize the
LGJ-12G
freeze-drying process manually.

• The system can show a variety of language interfaces such as English, Russian Etc. The system vacuum
can be freely converted at mBar, Pa and Torr. The temperature can be expressed in degrees Celsius and
Fahrenheit.

• During the operation, the system can automatically monitor and detect and record and store the
relevant data. It can also be monitored by remote systems.

• From freeze-drying process to defrosting process, all materials can be programmed automatically and
many programs can be stored.

• The system is equipped with variety sensors, it can alarm immediately during the operation of abnormal
temperature or pressure, and take active protection to ensure safe and stable operation.

• Many data such as real-time-record of Vacuum, cold trap temperature, material temperature, shelf
temperature, operation error alarm is recorded in the system.

• Data was recorded once a minute with freeze-drying curve. The system can record real-time data
continuously and has USB data storage serial port.

• The freeze-drying process can be recorded, the freeze-drying curve is drawn and the eutectic point test
is achieved.

• The man-machine interface equipment of the control system can work stably in the environment
temperature from -20℃ to 60℃. It conforms to the NEMA (International Election Manufacturing
Association) protection regulations and the European CE Electrical Certification standards.

• Automatic vacuum regulation is achieved in this system.

Vacuum System

The system is composed of vacuum pump or roots pump

(optional), freeze-drying box, vacuum gauge, pipeline and
controller. The vacuum pump is equipped with redundancy.

The vacuum degree is controlled by PID mode, and the

whole automatic control can be realized.

Systematically standardized test procedures are took in order to avoid potential vacuum leaks.

A device at the suction port of the vacuum pump is provided to prevent the gas flowing back when the
equipment was stopped. An oil mist filtering device at the exhaust port is provided to prevent the exhaust
gas polluting the surrounding environment.

LGJ-12G
The vacuum can be adjusted automatically or manually. The
efficiency of the heat transfer and freeze drying was increased and
the equipment and energy consumption is reduced.

The butterfly valve of the pilot freeze-drier between the freeze-

drying chamber and the ice condenser should be closed before
freeze-drying preparation and the terminative process. So the
material can be handled and pre-frozen in a clean environment.

Refrigeration System
The utility model is composed of a refrigeration compressor, a condenser and an expander etc. An
imported compressor is adopted in the system. The shelf and the water catcher are respectively cooled
by the silicon oil and the condensing pipe. The system was simple and reliable. The cold capacity is
enough also. The environment-refrigerant was used in the system. The system can be delay started and
automatic controlled.

Freeze-drying Process
The freeze-drying cycle system consists of intermediate medium, circulating pump, heater, plate heat
exchanger, freeze-drying chamber, shelf and pipeline. The freezing and heating of materials are
completed with this system.

The freeze-drying process is managed. A number of mature and safe freeze-drying process is stored in
the management system. Users can make up for different products of freeze-drying process when they
adjusted freeze-drying process data.

Material can be observed and the freeze-drying parameters can be adjusted at any time in the freeze-
drying process.

The freeze-drying chamber can effectively pre-freeze the material, and it is suitable for various serum
bottles or vials.

PID algorithm is used in the automatic control. Materials can be repeated freeze quickly or slowly.

The temperature is even by accurately controlling the medium circulating in the shelf heating system and
the shelf is smooth with the special process. The quality of freeze drying and the drying efficiency are

LGJ-12G
improved.

In order to avoid the contamination of the material after freeze

drying, the protection system can be filled with pure nitrogen gas or
other protective gas through the system.

The gland system can perform manual or automatic accurate and

reliable sealing of the material container in the freeze-drying chamber
in a vacuum state, the container lid and the container can be reliably
sealed.

The ice condenser can be defrosted repeatedly through the defrost system after freeze-drying process
so as to freeze the material again.

Certificates
Certificated with CE, ISO9001:2008

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LGJ-10E LGJ-24D LGJ-40G

Fuzhou Fangjing Technologies Co., Ltd.

Rm. 8-3, 8F, Boss Software Building,
No. 5 Gaoxin Avenue Shangjie Town,
Minhou County, Fuzhou City Fujian China
Tel.: +86 0591 2351 0807
E-mail: info@fangjing-tech.com
Web: www.fangjing-tech.com

LGJ-12G