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Karl Fischer
Karl Fischer
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2/9
1/15/12
2HI
+ SO3
C5H5N.SO3 + CH3OH
Standardisation of Karl Fischer reagent Place sufficient quantity of methanol in the titration vessel and add sufficient amount of Karl Fischer reagent to give the characteristic end point. Weigh accurately 150-350 mg of sodium tartrate, (Na2C4H4O6,2H2O) accurately weighed, by difference and titrate to the end point. The water equivalence factor, F in mg of water per ml of the reagent is given by the expression 0.1566 w/v, where w is the weight, in mg, of the sodium tartrate and v is the volume, in ml, of the reagent required. The water equivalence factor F, in mgs of H2O per ml of reagent is calculated according to the formula 0.1566 x w/v, where W is the weight in mgs of sodium tartrate and V is the volume in ml of the reagent. Each mg of sodium tartrate is equivalent to:
Supercritical fluid
2H2O
36.04
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Procedure Add 30 ml of methanol into titration flask. Neutralize with Karl Fischer Reagent to the electrometric end point. Refill burette. Weigh accurately specified qty of sample and transfer into a titration flask stir for 1 minute and titrate the solution with Karl Fischer reagent to the electrometric end point. Record the volume of Karl Fischer reagent consumed.
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Calculation Formula: B.R. x F x 100 % Water (w/w) = ------------------------------wt x 1000 Where, B.R. = F wt = Volume of Karl Fischer reagent consumed in ml. Karl Fischer Reagent factor in mg/ml.
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