Shell & Tube Condenser Design: O O O O O O

SHELL & TUBE CONDENSER DESIGN
NOTE:
DO NOT CHANGE THE FIGURES WHICH ARE COLOURED
STEP - 1
TO CALCULATE HEAT LOAD
1) SHELL SIDE FLUID (vapourizing fluid)
2) TUBE SIDE FLUID (utility)
INPUT DATA :
1) Cp OF SHELL SIDE FLUID HOT FLUID( Kcal/Kg OC)
2) Cp OF TUBE SIDE FLUID COLD FLUID( Kcal/Kg OC)
5) TEMP. OF HOT FLUID INLET ( OC )
6) TEMP. OF HOT FLUID OUTLET ( OC )
7) TEMP. OF COLD FLUID INLET ( OC )
8) TEMP. OF COLD FLUID OUTLET ( OC )
9)SP.GR. OF SHELL SIDE FLUID
10) LATENT HEAT OF VAPORISATION (Kcal/KG C)
11) FLOWRATE OF SHELL SIDE FLUID (Kg/Hr)
12) FLOWRATE OF TUBE SIDE UTILITY FLUID (Kg/Hr)
13) FLOWRATE OF TUBE SIDE UTILITY FLUID (m3/Hr)
STEP - 2
TO CALCULATE LMTD FOR COUNTER CURRENT FLOW :
HOT FLUID IN
41
COLD FLUID OUT
35
DIFFERENCE
6
HOT FLUID OUT

COLD FLUID IN
DIFFERENCE
STEP - 3
OVERALL HEAT TRANFER COEFFICIENT CONSIDERATION.
BTU/HrM2OK
CONSIDERED=
50
244
Kcal/M2.hr.C
STEP - 4
HEAT TRANSFER AREA CALCULATION
INPUT DATA
1) HEAT LOAD
2) LMTD
3) OVERALL HEAT TRANSFER COEFFICIENT
Heat Transfer Area ( M2 )

STEP - 5
AREA OF THE CONDENSER REQUIRED
(CONSIDERING 20 % DIVERSITY)
NSER DESIGN
water
water
1
0.35
41
35
30
35
1.32
87
792
42089
42
105.8 F
95 F
86 F
95 F
COLD FLUID
Total Boile up
Kg/Hr
m3/Hr
35
30
5
73656 Kcal/Hr
5.4848149
2 O
244 Kcal/Hr-M - C
55.037199
M2
66.04
M2
Acetonitrile
81.75
-47
Benzene
80.1
Carbon Bisulfide
46.3
Chloroform
Cyclohexane
DMF
152.8
EDC
600 torr
-59.4
500 torr
1.7
56.5
400 torr
139.6
Acetone
200 torr
Acetic Anhydride
100 torr
-17.2
63
80
99
105
110
82.2
100
119.8
126
133
7.7
22.7
39.5
46
51
15.9
27
43.7
62.5
68
74
7.6
15.4
26.1
42.2
60.6
67
73
-43.94
-21.16
-13.6
-5.1
10.4
28
34.57
39.5
-39.1
-29.7
-7.1
0.5
10.4
25.9
42.7
48
54
-25.4
-15.9
6.7
14.7
25.5
42
60.8
68
73
19.3
32.47
62.85
72.91
86.48
106.7
129.3
137.2
143.83
60 torr
118.1
40 torr
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
Solvent
10 torr
Acetic Acid
Sr.N
o.
5 torr
1 torr
Common Solvent Data Sheet

B.P. in
o
C at
Atm Pr.
6.3
17.5
43
51.7
24.8
36
62.1
70.8
-40.5
-31.1
-9.4
-2
-26.6
-16.3
7.7
-36.7
-19.6
-11.5
-73.87
-53.8
61.3
-58
80.7
-45.3
84
-44.5
-24
-13.6
10
18.1
29.4
45.7
64
70
76
Ethanol
78.4
-31.3
-12
-2.3
19
26
34.9
48.4
63.5
68
72
EPH
117.9
-16.5
5.6
16.6
42
50.6
62
79.3
98
Ethyl Acetate
77
-43.4
-23.5
-13.5
9.1
16.6
27
42
59.3
64
70
FFA
146
14.5
27.59
57.48
67.38
80.74
100.62
124.88
130.62
137.17
Formaldehyde
-19.5
-88
-70.6
-65
-57.3
-46
-33
-32
-27
IPA
82.5
-26.1
-7
2.4
23.8
30.5
39.5
53
67.8
70
77
MDC
39.75
-70
-52.1
-43.3
-22.3
-15.7
-6.3
24.1
30
34
Methanol
64.7
-44
-25.3
-16.2
12.1
21.2
34.8
49.9
55
59
33
-82.17
-62.99
-53.49
-31.65
-24.42
-14.66
-0.14
16.11
21.76
26.55
MIPA
Mono Chloro Benzene
132
-13
10.6
22.2
49.7
58.3
70.7
89.4
110
117
123
MTBE
55.2
-68.32
-47.75
-37.56
-14.14
-6.38
4.07
19.65
37
43.15
48.28
n-Butanol
117.5
-1.2
n-Hexane
68.7
Petroleum Ether
60-80
20
30.2
41.5
60.3
70.1
84.3
100.8
106
111
-34.5
-25
-2.3
5.4
15.8
31.6
49.6
56
61
172
Phenol
182
40.1
62.5
73.8
100.1
108.4
121.4
139
160
168
Pyridine
115.4
-18.9
2.5
13.2
38
46.8
57.8
75
95.6
108
108
66
-61.58
-40.34
-29.81
-5.62
2.39
13.19
29.28
47.29
53.55
58.85
110.6
-26.7
-4.4
6.4
31.8
40.3
51.9
69.5
89.5
97
102
1.2
11.2
34
41.5
51.6
66.5
79.41
86.3
92.13
THF
Toluene
Water
100
o-Xylene
139.3
-15.86
9.97
22.78
52.2
61.94
75.08
94.65
116.55
124.16
130.61
m- Xylene
144
-12.93
13.2
26.15
55.9
65.76
79
98.84
120.99
128.69
135.21
p- Xyleme
137-138
Aniline
184
35
58
69.4
97
106
119
140
162
Carbon t Chloride
76.7
-50
-30
-20
4.3
12.3
23
38.3
57.8
Di Ethyl Ether
34.6
-74
-57
-48
-28
-22
-12
2.2
17.9
Dimethyl Sulfoxide
189
33
60
73
103
114
125
146
178
Dioxane
101
-36
-13
-1.2
25
33.8
45.1
62.3
81.8
Ethelene Glycol
197
53
78
92
120
130
142
159
179
Formamide
211
71
96
110
138
147
158
176
194
Methyl Acetate
57.8
-57
-39
-29
-8
-0.5
9.4
24
40
NitroBenzene
211
44
72
84.9
115
129
140
161
186
Propanol -1
82
97.8
-15
14.7
36
43.5
52.8
66.8
Heptane
98
-34
-13
-2
22
31
42
59
78
Glycerine
290
126
154
167
198
208
220
240
263
700 torr
Latent
Heat (Cal
Sp.Gr.
/gm)
115
1.053
96.75
138
1.082
55
0.78
79
78
43.9
Sp. Heat
Cp
(Kcal/Kgo
C)
Flash Point Viscosity

Vap.
Melting
(Close Cup) in CP (25 Density point
o
(oC)
C)
(Kg/m3)
(oC)
0.522
39
1.15
2.07
96.44
0.236
48.8
0.91
124.3
0.538
-18
0.33
0.783
173.68
0.541
0.38
0.8787
103
0.419
-11
0.65
1.263
59.35
-30
NA
59
1.484
59.01
0.231
none
0.57
78.5
0.7781
93.81
0.44
-18
0.98
149.6
0.945
137.81
0.486
58
0.82
82
1.2569
77.33
0.3015
13
0.9
3.35
76
0.789
204.26
0.68
13
1.2
1.62
1.183
97.95
94.26
0.457
-4.4
0.46
Mol.
Wt.
Solubility
in water at
20 oC (%
w/w)
16.7
60.05
3.52
-73
102.09
12
-94.6
58.08
infinite
1.5
0.41
41.05
infinite
5.5
78.11
0.18
-108.6
76.13
4.12
-63.5
119.4
0.82
2.9
6.6
54.16
0.0052
-61
73.1
infinite
-40
98
NIL
-112
46.07
infinite
-25.6
92.53
-82.4
88.1
3.05
infinite
74
0.901
142.87
1.03
7.7
-24
0.815
-92
30.03
Very soluble
80
0.785
159.35
0.67
-11.7
0.34
2.07
-101
60.1
infinite
37.5
1.3255
77.077
0.2888
None
0.44
2.93
-96.7
84.94
63
0.7915
269.79
0.605
12
..65
1.1
-97.8
32.04
infinite
30.72
0.692
119.09
0.65
129
1.107
78.3
0.311
29
0.8
52.75
0.747
78.196
0.508
-28
0.35
114
0.81
141.26
0.687
35
294
66
0.6591
80.48
0.527
-18
0.31
infinite
60
0.635
0.498
-40
59.111
3.04
2.97
-45.2
112.56
-109
88.15
0.049
4.8
-79.9
74.12
7.45
-94
86.17
0.001
2.5
178
1.071
0.561
79
2.8
113
0.982
107.36
40.6
94.11
8.2
0.431
20
0.88
-42
79.1
infinite
63.47
0.889
92.414
107
0.866
88.17
0.325
4.4
0.59
97.22
0.99
540
0.99
NA
0.89
136.22
0.88
81.86
0.4
27
0.85
140.89
0.87
81.86
0.4
32
0.86
81.86
0.4
1.032
103
0.512
46
0.2
0.713
123
0.473
-40
0.24
74.12
6.9
1.101
178
0.7
85
1.99
78
Fully Miscible
1.034
102
0.4
12
1.3
88
Fully Miscible
1.113
191
0.573
>110
20.9
62
Fully Miscible
1.134
112
0.595
154
3.8
45.04
Fully Miscible
0.932
98
0.4
-9
0.37
-98.7
74.08
24.5
1.196
79
0.339
87
1.86
5.7
123.11
0.19
0.804
164
0.582
15
1.72
60.1
Fully Miscible
0.684
87.18
0.518
-1
0.41
1.261
124.17
0.4
160
945
-17.22
2.5
-108
72.1
Fully Miscible
3.14
-95
92.13
0.06
18
100
3.6
-47.4
106.1
NIL
0.6
3.6
-25
106.4
0.02
27
0.65
3.6
13-14
106.1
NIL
70
3.8
-6.2
93.13
3.8
-22.6
153.84
9.5-10.5
9.6
100.21
0.005
92.09
Fully Miscible
Acetone Condenser
Tray Oven
Acetone Liquid
Coolant Fluid Out

Heat Input
Basis of Drying Oven Operation:

1.
2.
3.
4.
Wet solid product is put into Tray Oven; oven is sealed closed.
Heat input is applied to oven;
Cooling fluid is circulated through acetone condenser;
vacuum pump is started;
As the wet solid is heated in the oven, the vapor pressure of the acetone increases and the acetone starts to vaporiz
produced by the vacuum pump;
The vacuum pump works to maintain the set partial vacuum that is controlled by allowing atmospheric air to "bleed" i
vacuum pump - under ideal conditions - would not not normally have to continue to operate after extracting all non-co
in the real world situation, there will be air infiltration into the partial vacuum system through the oven door seals, the
These air infiltrations try to defeat the vacuum created and, as a consequence, the vacuum pump is left to continue t
by allowing the atmospheric air to bleed in and keep the pump working at capacity.
The partial vacuum is really set by the temperature of the cooling fluid in the acetone condenser. The acetone has t
that corresponds to the acetone vapor pressure equal to the partial vacuum setting. This allows the acetone to cond
as a liquid and not be "sucked" (extracted) out of the system by the vacuum pump.
If the temperature of the condensed acetone is sufficiently cold, there will little or undetected losses of acetone exitin
The addition of heat into the oven accelerates the rate of acetone evaporation and speeds up the drying process; the
the cold energy that has to be inputted into the condenser as the coolant fluid.
Vacuum Pump
ant Fluid Out
acetone starts to vaporize at the lower, partial vacuum pressure
mospheric air to "bleed" into the vacuum pump suction. The

after extracting all non-condensables from the system. However,
the oven door seals, the gaskets, equipment and piping joints, etc., etc.
pump is left to continue to operate - although at a reduced capacity
nser. The acetone has to be cooled and condensed at a temperature

llows the acetone to condense and drop out of the condenser
d losses of acetone exiting in the vacuum pump exhaust to atmosphere.

up the drying process; the price to pay for this capacity increase is

Shell & Tube Condenser Design: O O O O O O

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Shell & Tube Condenser Design: O O O O O O

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SHELL & TUBE CONDENSER DESIGN

DO NOT CHANGE THE FIGURES WHICH ARE COLOURED

HOT FLUID OUT

Heat Transfer Area ( M2 )

Common Solvent Data Sheet

Flash Point Viscosity

Coolant Fluid Out

Basis of Drying Oven Operation:

ant Fluid Out

acetone starts to vaporize at the lower, partial vacuum pressure

mospheric air to "bleed" into the vacuum pump suction. The

nser. The acetone has to be cooled and condensed at a temperature

d losses of acetone exiting in the vacuum pump exhaust to atmosphere.

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