Aspects of Standards

Why are they important? And, examples in Metallurgical Testing

John M. Tartaglia, Ph.D.
Senior Metallurgical Engineer & Engineering Manager Element Wixom
March 6, 2012 Aspects of Standards

Webinar Schedule
Begin lecture at 1 pm Lecture for about 50 minutes

Questions & Answers

During webinar and directly after webinar
Ask questions using the GoToWebinar question box

These questions will be answered in the remaining 10 minutes

After the webinar is posted, send me an email at

John.tartaglia@element.com
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Presentation Requests & Materials

Supplied materials
1. PowerPoint slides
You may download a copy of this webinar from our website within 48 hours You may separately download a pdf copy of this presentation from the website, without my voice

2. Element Materials Technology marketing information and scopes are available on our website: www.element.com

Topical Coverage
I picked topics based on my/our experience with these standards Ill try to keep your interest I wont cover all the notes; some of them are for reference only. This may be a good reason to download the pdf copy of the presentation. I will cover and omit topics partly based on time expenditure This presentation contains some of the presenters personal opinions.

Some parties may consider these assertions to be controversial.

The opinions do not represent ASTM, ASM, JIS, ISO or Element policy. Aspects of Standards
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Questions that will be (at least) partially answered in this webinar

How are ASTM standards developed? How often are ASTM & SAE test methods and other standards revised? What are the strengths and weaknesses of various types of specifications? What are some guidelines for citing open specifications and test methods in industrial part prints and contractual documents What are some implications of using domestic standards for products produced in foreign locations? What are some key differences between the metallurgical standards published by various organizations, e.g., SAE, ASTM, JIS, DIN, EN, ISO, etc.?
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Aspects of Standards Topics

Definition of standards ASTM society description ASTM collections and nomenclature Types of ASTM committees & standards Other standards organizations ASTM standards numbering ASTM standard revision timing ASTM versus SAE test methods and specifications Why bother and a sad story Test method standards, including ASTM vs. other types
Hardness and Mechanical Test Standards Quantitative Metallography Standards
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What is ASTM?
Originally known as the American Society for Testing and Materials (ASTM). Begun in 1898 when engineers and scientists gathered to address frequent rail breaks in the burgeoning railroad industry. Now known as ASTM International, which is one of the largest voluntary standards development organizations in the world. ASTM standards make products and services safer, better and more cost-effective.
Information on this and subsequent ASTM slides was obtained from www.astm.org and the ASTM Blue book

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ASTM

vs.

ASM

Note that ASTM and ASM are very different ASTM is a standards-making organization ASM International:
Is the former American Society for Metals, Is The Materials Information Society, Only supplies information about materials, Issues no standards, but Publishes handbooks that are an excellent source for crossreferencing various metals and alloy specifications
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7 Categories of ASTM Committees and Standards

A. B. C. D. E. F. Ferrous Metals Nonferrous Metals Ceramics, Glass, Concrete, Insulators Plastics, Paint, Rubbers, Wood, Packages Miscellaneous Subjects (mostly testing) Fasteners, Electronics, Hazards, Amusement Rides G. Corrosion, Wear, Erosion
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ASTM standards facts

12,000 standards Delivered by PDF file download, CD, or 77 book volumes of standards
Two digit section number precedes a period Two digit volume number follows the period Example:
Section 3: Metals Test Methods and Analytical Procedures Volume 03.01: MetalsMechanical Testing; Elevated and LowTemperature Tests; Metallography

With the advent of computerized standard delivery, the ASTM book volumes are becoming less significant and less used.
However, they are still extremely valuable for several specialized reasons like subject matter searches and alloy groupings because the ASTM website does not quite give you this key wording perfection.
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Volume 03.01 Metals (most common in metals labs)

1. Volume 03.01 includes tests and practices that outline the standard procedures needed to perform mechanical testing 2. Some standards define terms and explain procedures related to fatigue testing and loading 3. Also featured are metallography tests and practices
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ASTM standard is a generic description

standard, nas used in ASTM International, a document that has been developed and established within the consensus principles of the Society and that meets the approval requirements of ASTM procedures and regulations.
The term standard is also used as a generic adjective in the title of documents, such as test methods or specifications. The various types of standard documents are prescribed by the ASTM committees.
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Primary types of ASTM standards

1. specification, nan explicit set of requirements to be satisfied by a material, product, system, or service.
2. test method, na definitive procedure that produces a test result.

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Other types of ASTM standards

3. guide, na compendium of information or series of options that does not recommend a specific course of action. practice, na definitive set of instructions for performing one or more specific operations that does not produce a test result. This is not really true; many practices do produce a test result. terminology standard, na document comprising definitions of terms; explanations of symbols, abbreviations, or acronyms.

4.

5.

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Other standards-making organizations

In this webinar, I mostly discuss ASTM and SAE because they are the organizations that are arguably most predominant in North America and Detroit, respectively, where Element Wixom mostly operates. However, there are many organizations that issue standards.
To the left of this slide is an example, from a survey, of all the organizations that issue aerospace standards:

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JIS Background
The Japanese Standards Association is an organization that formed in December 6, 1945. The objective of the association is "to educate the public regarding the standardization and unification of industrial standards, and thereby to contribute to the improvement of technology and the enhancement of production efficiency". The primary activity of JSA is to publish and distribute JIS (Japanese Industrial Standards) JSA also publishes books on industrial standardization, quality management (control), administrative management, science and technology, JIS Handbooks, and other books.
http://www.jsa.or.jp/default_english.asp
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ISO Background
http://www.iso.org/iso/home.htm ISO standards are developed similarly to ASTM and according to the following principles: Consensus The views of all interests are taken into account: manufacturers, vendors and users, consumer groups, testing laboratories, governments, engineering professions and research organizations. Industry wide Global solutions to satisfy industries and customers worldwide. Voluntary International standardization is market driven and therefore based on voluntary involvement of all interests in the market-place. Example: Element laboratories have A2LA Accreditation International Standard ANS/ISO/IEC 17025 General requirements for the competence of testing and calibration laboratories Aspects of Standards
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DIN and EN Background

http://www.din.de/cmd?level=tpl-home&languageid=en http://www.cen.eu/cen/Pages/default.aspx

The creation of German standards is the task of DIN, a self-governing institution of trade and industry. DIN represents Germany and fulfils an equivalent function in the European and International (ISO) standards organization. An EN standard is a European standard, with the status of a DIN or BS (British) standard. CEN develops EN standards, in the same way as ASTM and ISO:
Standards are developed through a consensus process; Participants in standards development represent all concerned interests: industry, authorities and civil society, contributing mainly through their national standards bodies; Draft standards are made public for consultation at large; The final and formal vote is binding on all members; The European Standards (ENs) must be transposed into national standards and conflicting standards withdrawn.

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ASTM standards
Numbering Revision and issuance Test methods Specifications The sad stories..

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Standards Numbering
Volume 03.01 contains standards produced by the following committee(s):
E04 on Metallography E08 on Fatigue and Fracture

E28 on Mechanical Testing

E30 and E58 on Forensic Sciences and Engineering, respectively

Im a member of these three committees for Element Wixom and I vote on new and revised standards that are issued by several subcommittees of these committees. The standards themselves are preceded by their letter category and a chronological number (which varies from one to four digits).
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Standards Numbering Example E1234M-99a(2004)1

1. The E signifies that it is a Miscellaneous Subjects standard, and that it was probably published by an E committee and subcommittee. The 1234 signifies that it is the 1234th standard developed in the E category. The M means the standard version with metric units. Sometimes this is in a separate document like this example
Usually it is in the same document with the English units and called E1234(E1234M)a(2004)e1.

2.

3.

4. 5.

The 99 signifies that it was originally adopted or last revised in 1999. Standards can be revised every day, but in reality, it takes a rather long process with one or more votes.
The a signifies that it was revised once in 1999 after it was adopted or a revision was published during that year.
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Standards Numbering Continued E1234M-99a(2004)1 (with rules)

6.

The 2004 signifies that it was reapproved with no changes during 2004.
All ASTM standards must be reapproved or withdrawn (after a vote) within seven years. ASTM will automatically withdraw the standard when/if the (sub)committee does not act to submit the standard for reapproval, revision or withdrawal vote within the seven years.

7.

The e1 or e1 signifies that it was revised editorially.

These editorial revisions do not require a vote and are usually used to correct clerical mistakes.

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ASTM Standard Footnotes & Chronology

The footnotes at the bottom of the left hand column of each standard give more pedigree information. Chronology:
The current edition was approved on July 1, 2007. The current edition was published in September 2007. The standard was originally published as E3-21T, which was in 1921. This is the oldest surviving E standard! The last previous edition was E3-01, or the 2001 version.
The 2007 reapproval makes it a separate version!

Both a committee and a subcommittee are involved in issuance:

Jurisdiction of ASTM (Main) Committee E04 on Metallography Direct responsibility of Subcommittee E04.01 on Specimen Preparation.
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Are your ASTM standards updated in a timely manner?

ASTM standards change at any time Some changes occur multiple times throughout the year. With standards in book form, you probably dont have the latest standard. If you update once a quarter, you are more timely, but you are still behind. ASTM email notification service is available when a standard of interest is updated and downloadable as a pdf. Often entities, and even ASTM, references obsolete or withdrawn standards!
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Incorporating ASTM standard revisions

At Element Wixom, I read the standard and see what has changed. (For the major ASTM test methods, I know this because Ive voted on the standard revisions during development.) The subcommittee authors sometimes make this easy with a Notification of Changes section since the last revision. I then notify the laboratory staff who will be affected, and its their responsibility to incorporate the revisions into their daily test or certification practice. A2LA and other accreditation bodies like Nadcap require a full citation on a report for the relevant standard. This must include the year and revision designation. I am surprised at how often thats missing on many laboratory reports!

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Other documents reference ASTM standards

Besides ASTM, many companies and standardizing bodies issue test methods. Almost all of these organizations refer to ASTM standards, but not all of them do so correctly!

The major examples of incorrect (or at least inadvisable) reference are as follows:
Including a year for the reference (which is exactly opposite to the requirement for a report) Abstracting data from the cited ASTM standard, e.g., an alloy composition Both of these references are potentially out-of-date as soon as they are published.
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An example of a print exhibiting a problematic specification reference

Print DATE: 06/20/97

Material: LEADED RED BRASS PER ASTM B584-87 ALLOY UNS NO. C83600

Print requires (19)87 Version of ASTM B584 The earliest edition of the standard that we could find was (19)98a The sample was out-of-specification for 98a
This is the current (2008) version of the ASTM standard.

However, the question remains:

Was the alloy out-of-specification in the 1987 version of the ASTM standard? Aspects of Standards
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SAE vs. ASTM test methods

Test Method
Hardness Decarburization Inclusions Case Depth

SAE
J417 Dec 1983 J419 Dec 1983 J422 Dec 1983 J423 Feb 1998

ASTM
E10-10 E18-08b E140-07
E1077-01(2005) E45-11 None!

ASTM is updated much more frequently so procedures are different. SAE test methods, except for case depth, are hardly used anymore.
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SAE vs. ASTM alloy specifications

Alloy Specification
Plain Carbon Steels Ductile Iron

SAE
J403 November 2001 (wrought only) J434 Feb 2004

ASTM
A684(A684M)-10a
for strip with separate standards for wrought products of different form (sheet, plate, tube, bar, etc.) or castings

A536-84 (2009)

ASTM usually requires more and different things. SAE has more ambiguities.
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Differences in plain carbon steel specifications

SAE J403 November 2001 Requires
C range Mn range P maximum S maximum Report other elements

ASTM A684 (A684M)-10a Requires

C range Mn range P maximum S maximum Si range (although exceptions) Report other elements

Special callouts for

B and/or Si ranges Copper minimum Lead (Pb) range

Special callouts for

B and/or Si ranges Lead (Pb) range

No discussion of residuals
Ni, Cr, Mo Could lead to a tool, alloy or stainless steel being classified as a plain carbon steel

Residuals are limited

Ni, Cr, Mo, and Cu

Strip thickness is specified

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Example: A true, but sanitized and relevant story

Major OEM buys a safety-critical fastener system from fastener manufacturer in accordance with a print specifying 1050 steel per SAE J403. Fastener manufacturer buys a component for the system from heat treater
Heat Treater buys 1050 steel from Service Center #1. Service Center #1 buys 1050 steel from another service center (call it #2). Service Center #2 supplies 3150 steel, and doesnt report (to Heat Treater and Service Center #1) that the steel contains 0.8%Cr and 1.25%Ni.
Dont worry if youve never heard of 3150; it was only obsoleted in 1952.

Service center #1 reports only C, Mn, P, S, and Si to Heat Treater

Heat treater hardens and tempers 3150, certifies it as 1050, and reports Service Center #1s composition to fastener manufacturer. Fasteners embrittle in the field and this caused a large recall. Major OEM very upset
OEM metallurgists say everyone should know that 1050 steel wasnt supplied OEM quality engineers and Tartaglia say 3150 steel is no different than 1050 steel based on SAE J403

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Ways That Failures Can Be Caused by Incorrect, Ambiguous, or Insufficient Specifications or Test Methods
Due to cost, availability, volume, or dimensional considerations
Prototypes often survive Production Part Approval Process (PPAP),* but production material fails because it is specified differently before production launch
*PPAP definition Per AIAG (Automotive Industry Action Group)

Prototype testing is only conducted on one end of the specification limit, but production parts may still fail even if they meet design specification

Specification is incomplete and inaccurate Conformance testing is not specified or ambiguously specified
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How can you be sure?

Test, test, test, TEST Ask Element about what kind of tests to run Supply Element with your specifications and ask us about certification options

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Aspects of Mechanical Testing Standards

Definitions in ASTM E6
Different ASTM tensile test methods

Determining yield strength and modulus from tensile tests

Differing elongation methods (ASTM vs. ISO & JIS) Charpy V-notch toughness (ASTM vs. ISO & JIS)
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ASTM tensile test methods

E8 standard English method
Uses psi or ksi and 4:1 gauge length to diameter/width ratio Mechanical/Uniaxial ASTM E28.04 subcommittee Now combined standard, with E8 Uses 5:1 gauge length to diameter/width ratio Same as ISO and JIS test methods, except for elongation calculations Uses MegaPascals=MPa = MN/m2 = N/mm2 ( kg/mm2) For nonferrous wrought and cast aluminum and magnesium only Light Metals and Alloys (product) ASTM B07.05 subcommittee responsibility For steel products Includes many tests besides tensile Steel (product) ASTM A01.13 subcommittee responsibility

E8M standard metric units method

B557/B557M

A370

All have virtually same requirements (now) thankfully Aspects of Standards

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Methods and terminology for strength testing in various standards

JIS Z2241, and DIN EN 10 002-1 results have the same yield and tensile strength requirements as ASTM, although the JIS and DIN test methods use different symbols for the results versus ASTM.
0.2%YS, UTS, El, and RA are yield strength, (ultimate) tensile strength, Elongation, and reduction of area respectively, in ASTM standards
Rp is proof strength, Rm is tensile strength, Z is reduction of area, and A is elongation for EN and JIS standards

Proof vs. Yield

Offset method is used for 0.2% offset YS in US & 0.1% proof stress in UK
Upper and lower yield strength is terminology reserved for discontinuous yielding in all the standards In JIS and DIN, offset method is used for proof and the word yield is reserved for discontinuous yielding

All standards define 5% EUL (extension under load); mostly for Cu alloys
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Elongation measurements
1. Elongation at fracture
Total elongation per current versions of ASTM test methods E8, B557 and A370 Measured by extensometer

2. Elongation after fracture (manual and plastic)

Measured physically by pushing fractured samples together (under 2 ksi pressure, if desired) Measure final gauge length with digital calipers
Will overestimate elongation in brittle materials because you cannot push sample ends together perfectly Will be similar to #1 for ductile materials

3. ASTM elongation calculation is all the same for JIS Z2242. 4. ASTM elongation calculation is mostly the same for DIN EN 10 002 Part 1
DIN EN has somewhat different gauge length requirements for some specimens, and thus elongation is calculated somewhat differently than ASTM and JIS.

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Whats the results section of the standard test method require?

Assumption:
In this age of computers, you can get sophisticated data

Potential problem:
But should you trust it (GIGO=garbage in-garbage out)?

Example:
ASTM E8, JIS Z2242, and DIN EN 10 045 Results Reports only ultimate tensile strength (UTS), yield strength (YS), elongation (%El), and reduction of area (%RA) and a few other items under some conditions in all three types of standards What about modulus (E) and digital stress-strain curves?

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Elastic modulus and digital stress-strain determination: ASTM E111

Only small difference between extensometer and strain gauge here
Although this full curve looks OK,
300 250

200

Stress (ksi)

150

100

Extensometer Strain %
50

Strain Gauge Strain %

0 0.000

significant inaccuracy has occurred at low strains here, so strain gauge must be used!
1.000 1.200 1.400 1.600

0.200

0.400

0.600

0.800 Engineering Strain %

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Charpy impact toughness

ASTM E23 and the other worldwide standards
Fast and inexpensive Constant overall standard geometry (10 mm by 10 mm by 55 mm) and apparatus V-notch is the same throughout the world All standards report energy in Joules or ft-lbs
Multiply ft-lbs by 1.355 to obtain Joules (J)

U-notch can have different depth in US versus Europe

ASTM E23 and JIS Z2242 = 5 mm depth (although JIS allows 2 mm in special instances) EN 10 045 = 5 mm DIN 50 115 = 3 mm for DVM (special for some ductile cast irons) Notch depths will give much different energy results

No testing standard allows or discusses reporting of energy density (Joules per mm2), but many users scale energies for subsize samples
Although some product testing standards allow this calculation, this energy density calculation is fraught with peril!
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Inclusion Definitions & Analyses

Indigenous (endogenous): A nonmetallic material that precipitates from the melt. An indigenous inclusion is native.

Exogenous: A nonmetallic constituent produced by entrapment of foreign material in the melt.

Inclusion cleanliness severity ratings are usually applied to indigenous inclusions only, and mostly in steels. I will discuss ASTM, German DIN, and Japanese JIS methods for these. Inclusion content determinations and elemental analyses can be applied to all inclusion types and metal alloys. I wont discuss these, but they are covered in ASTM test methods and practices E1245, E2283, and E2142.
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Inclusion Cleanliness Severity Standards

American ASTM E45 German DIN 50602 Japanese G0555

All three rate by color and morphology only

No composition determination Severity is defined as thickness/width and length, except for JIS which is in %
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Sample requirements (ASTM+DIN+JIS)

Careful mount polishing is required to avoid
Corrosion of inclusions Pullout of inclusions JIS requires hardened samples

Required sample orientation

in the radial longitudinal orientation (G) for round stock in the long transverse orientation (E) for flat stock

Required sample state

in the semi-finished state only (e.g., not after being forged or formed into a product) JIS suggests hardening some samples

Required minimum sample size of

minimum 160 mm2 (0.25 in2) rated area
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International Comparison:
(Same types, but different abbreviations)
Type Morphology and Color
Elongated, gray, and continuous (stringers) elongation (orientation) in working direction Elongated, dark, and continuous elongation (orientation) in working direction Elongated and fragmented (granular) with discontinuous elongation (orientation) in working direction Rounded and individual with no preferred orientation with respect to the working direction

Hardnes s
Soft & plastic
Soft & plastic

ASTM

DIN

JIS

Sulfide

SS

A1

Silicate

OS

A2

Alumina

Hard

OA

Globular

Hard

OG

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To take away
Standards are part of our lives and societies
Accept them Use them Contribute to their improvement

Standards have precision and provide

Requirements Test methods Rules for commerce

There are fine points that are similar and different between various worldwide standards
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Contact for questions

John M. Tartaglia, Ph.D., FASM
Senior Metallurgical Engineer & Engineering Manager

Element Materials Technology 51229 Century Court Wixom, MI 48393-2074 Tel: 248-960-4900 Ext. 329 Fax: 248-960-5973 E-mail: john.tartaglia@element.com

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