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    Preparation and Analysis of Trisacetyl Acetonato Cobalt (Iii) Complex

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    Abubakar Suleiman
    This document outlines the preparation and analysis of trisacetylacetonatocobalt(III) complex. It describes mixing cobalt(II)carbonate with the ligand acetylacetone, preparing a peroxide solution, and heating the reaction setup. The complex was analyzed by testing its solubility in solvents, calculating its percentage yield of 76.89%, determining its decomposition temperature of 204°C, and performing spectroscopic analysis. Infrared spectroscopy was used to analyze the ligand and final complex.

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    Preparation and Analysis of Trisacetyl Acetonato Cobalt (Iii) Complex

    Uploaded by

    Abubakar Suleiman
    20 views7 pages
    This document outlines the preparation and analysis of trisacetylacetonatocobalt(III) complex. It describes mixing cobalt(II)carbonate with the ligand acetylacetone, preparing a peroxide solution, and heating the reaction setup. The complex was analyzed by testing its solubility in solvents, calculating its percentage yield of 76.89%, determining its decomposition temperature of 204°C, and performing spectroscopic analysis. Infrared spectroscopy was used to analyze the ligand and final complex.

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    Original Title

    Abdulrahman Dauda Gaya

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    This document outlines the preparation and analysis of trisacetylacetonatocobalt(III) complex. It describes mixing cobalt(II)carbonate with the ligand acetylacetone, preparing a peroxide solution, and heating the reaction setup. The complex was analyzed by testing its solubility in solvents, calculating its percentage yield of 76.89%, determining its decomposition temperature of 204°C, and performing spectroscopic analysis. Infrared spectroscopy was used to analyze the ligand and final complex.

    Copyright:

    © All Rights Reserved
    Download as PPTX, PDF, TXT or read online from Scribd
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    20 views7 pages

    Preparation and Analysis of Trisacetyl Acetonato Cobalt (Iii) Complex

    Uploaded by

    Abubakar Suleiman
    This document outlines the preparation and analysis of trisacetylacetonatocobalt(III) complex. It describes mixing cobalt(II)carbonate with the ligand acetylacetone, preparing a peroxide solution, and heating the reaction setup. The complex was analyzed by testing its solubility in solvents, calculating its percentage yield of 76.89%, determining its decomposition temperature of 204°C, and performing spectroscopic analysis. Infrared spectroscopy was used to analyze the ligand and final complex.

    Copyright:

    © All Rights Reserved
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    of 7

    PREPARATION AND ANALYSIS OF TRISACETYL ACETONATO

    COBALT(III) COMPLEX

    BY

    ABDULRAHMAN DAUDA GAYA


    (SCI/13/CHE/00252)
    OUTLINE
    • Aim and Objective
    • Materials
    • Method
    • Analyses
    • Results
    • Conclusion
    Materials and Method

    AIM AND OBJECTIVES


    The aim is to prepare and analyses the complex of trisacetylacetonatocobalt(III)

    APPARATUS
    The apparatus used include
    50ml beaker, Magnetic stirrer, Hot plate, Test tubes, 500ml Beaker, Dropper,
    50ml measuring cylinder, Watch glass, Thermometer

    REAGENTS
    The reagent used were:-
    Acetylacetone, Cobalt(II)carbonate, 10% hydrogen peroxide, Ethanol, Methanol,
    Carbontetrachloride, DMF, DMSO, Distilled water, and chloroform
    PREPARATION OF THE COMPLEX

    Steps
    • Mixing the ligand with the metal
    • Preparation of peroxide
    • Reaction Setup
    • Heating

    ANALYSES

    • Solubility test of the complex


    • Calculation of percentage yield
    • Determination of decomposition temperature of the complex
    • Spectroscopic analysis of the complex
    Results and Discussions
    Solubility of Co(acac)3 in solvents:
    Decomposition Percentage yield Color of the
    Temperature complex

    Temperature= %yield=76.89% Dark Green


    204oC
    Acetylacetone I.R Spectra Co(acac)3 I.R Spectra

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