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Design of Seperation Presentation Team-3
Design of Seperation Presentation Team-3
Design of Seperation Presentation Team-3
DESIGN OF SEPERATION
UNITS
TEAM 3
091145088 HAZAL VARLI
131145030 LATİFE DEMİRBAŞ
131140058 CANSU İREM İZGİ
141140057 GÖZDE IŞIK Prof. Dr. Suna BALCI
131145075 ONUR POLAT Dr. Emine Kaya EKİNCİ
141140099 SİBEL YOGUN
Distillation Column Design
o Method of Calculations
PROCESSİN FOTOSU
WHAT IS DISTILLATION?
𝑲𝒎𝒐𝒍
V=7.704 𝒎𝒊𝒏
𝑲𝒎𝒐𝒍 ypropylene=0.616
F2=300 𝒎𝒊𝒏
ypropane =0.384
Xpropylene=0.003
Xpropane =0.016
XBenzene =0.353
XCumene =0.313 F3=L
XDIPB =0.313
Xpropylene=1.85*𝟏𝟎−𝟒
XBenzene =0.363
XCumene =0.321
XDIPB =0.321
Degrees of Freedom Analysis 1nd Column
+ 9 unknowns (V,L,F,Xi,Yi,SD,f,Tfeed,Pfeed)
-F = 300 kmol / min
-F= V+L
-F*Xf = V*Yi+L*Xi
-Ʃ xi= 1.0 Ʃ yi= 1.0
-SD= 0.99
-Xi,Yi= f(SD)
-F= V / L
-f=f(Tfeed,Pfeed )
Pfeed = 1.5 atm
Molar Flow rate 300kmol/min 7,704 kmol /min 292,2 kmol /min
Pressure 1,5 atm 1,4 atm 1,3 atm
Temperature 80⁰C 65⁰C 95⁰C
Phase Liquid Vapor liquid
D=22.09 Kmol/min
XBenzene =0.87
XCumene =0.09
F2=292.2 kmol/min
XDIPB =0.04
XBenzene =0.067
XCumene =0.91
XDIPB =0.026
B=270.11 Kmol/min
XBenzene =1.33𝒙𝟏𝟎−𝟑
XCumene =0.97
XDIPB =0.021
Degrees of Freedom Analysis 2nd Column
17 unknowns ( F, B, D, XF, XB, XD, Po, PT, Ki, α, Nmin, q, Q, Rmin, R, Ntheoritical, Eo, Nact)
𝐁𝒊
LnPi= Aİ -
𝑪𝒊+𝑻(𝑲)
Bubble Point
∑yi=1
Dew Point
∑xi=1
Tdew= 100˚C
Tbubble=170 ˚C
The temperature where ∑xi=1 is dew point and it was
found 100 ˚C to trial-error solution.
The temperature where ∑yi=1 is bubble point and it
was found 170 ˚C to trial-error solution.
Determination of Minimum
Number of Equilibrium Stages
The minimum number of stages was determined by using Fenske
equation.
𝐥𝐧 𝐱 𝐋𝐊Τ𝐇𝐊 𝐃
𝐱𝐋𝐊Τ𝐇𝐊 𝐁
𝐍𝐦𝐢𝐧 =
𝐥𝐧𝛂 𝐋𝐊Τ𝐇𝐊 𝐚𝐯
n
αi xF,i
=1−q
αi − θ
i=1
it’s acceptable
n
αi xD,i
R min + 1 =
αi − θ
i=1
Determination of Reflux Ratio
In most cases, ratio of actual reflux to minimum reflux is
selected at least 1.5 or above.
𝐑
= Ratio
𝐑 𝐦𝐢𝐧
𝑹𝑫 − 𝑹𝑫,𝒎𝒊𝒏 𝒀 + 𝑵𝒎𝒊𝒏
𝑿= 𝑵𝒊𝒅𝒆𝒂𝒍 =
𝑹𝑫 + 𝟏 𝟏−𝒀
Determination of Overall
Tray Efficiency
Analytical expression developed by O’Connell correlation was used
for the determination of overall tray efficiency.
ND B xHK xHK
2 𝑵𝑫
log = 0.206 log
B = √
NB D xLK xHK 𝑵𝑩
D
𝑵𝑫 = 𝟖 𝒕𝒓𝒂𝒚𝒔
𝐍𝐚𝐜𝐭𝐮𝐚𝐥 = 𝑵𝑫 + 𝑵𝑩
𝑵𝑩 = 𝟏𝟕 𝒕𝒓𝒂𝒚𝒔
Feed Tray = 25
Determination of Net Vapor
Velocity at Flooding Conditions
𝟎.𝟓
𝛔 𝟎.𝟐 𝛒𝐋 − 𝛒 𝐯 𝐦
𝐕𝐧𝐟 = 𝐂𝐬𝐛 ∗ ∗ 𝐕𝐧𝐟 = 𝟎, 𝟕𝟖𝟒
𝟐𝟎 𝛒𝐯 𝐬
𝐦
𝐕𝐧 = 𝟎. 𝟔 ∗ 𝐕𝐧𝐟 𝐕𝐧 = 𝟎. 𝟒𝟕𝟎
𝐬
Determination of Net Column
Area
𝐦′ሶ 𝐯
𝐀𝐧 = 𝐀 𝐧 = 𝟏. 𝟔𝟖 𝐦𝟐
𝐕𝐧
𝝅𝑫𝟐 𝐃 = 𝟏, 𝟓𝟖 𝐦
𝐀𝐜 =
𝟒 r = 0,79
D: diameter of column, m
𝐀𝐜 : cross-sectional area of column, 𝐦𝟐
Height Evaluation of Column
HC=(NACT-1)HS+∆H
HS= 0,46 𝐦 HC = 13,04 𝐦
Process fluid
Th,i=100˚C Th,o=100˚C
Capacity 120kg/min
Pipeline No 3
Molar flow rate 292,2kmol/min 22,09 kmol /min 270,11 kmol /min
Propylene - - -
Propane - - -
D=0.99 Kmol/min
XDCumene =0.99
F=267.16 Kmol/min
XCumene =0.95
XDIPB =0.005
B =0.01 Kmol/min
XBCumene =0.005
Tdew= 155˚C
Tbubble=163 ˚C
0.9
0.8
0.7
0.6
x=y line
Eq. Curve
0.5
Feed Line
RS Op. Line
0.4 SS Op. Line
0.3
0.2
0.1
0
0 0.1 0.2 0.3 0.4 0.5 0.6 0.7 0.8 0.9 1
Condenser Design Calculation
Th,i=158 ˚C Th,o=158˚C
Tc,i= 25˚C
Pump Design Calculation
Equipment No P-102
Pipeline No 5
Pipe Size 0.1 m
Pipe Lenght 2m
Th,i=170 ˚C Th,o=160˚C
Heat transfer
area=2.25𝐦𝟐
Heat duty= 4.34 𝐤𝐖 Tc,o= 163˚C
Tc,i= 160˚C
U = 900 W/𝐦𝟐 ˚C
Feed Distillate Bottom
Pressure 1,1 1 1
D= 4 m D= 1.58 m
H= 19.1 m H=13,04 m
𝟗𝟕𝟎.𝟏
(Cp)2016 =(𝟔𝟗𝟗.𝟐)x(4800) = 6660$
Cost of Reboiler
Q= 21387 kW A = 4m2
Purchased cost of condenser is 1300 $
𝟓𝟓𝟖.𝟗
(Cc)2016 =( )x(1300) = 2035$
𝟑𝟓𝟔.𝟗
Cost Of Cumene Column Cost of condenser
H= 6.67 A=3.5 m2
D= 2.9 m 𝟓𝟓𝟖.𝟗
(Cc)= 407.090$ (Cc)2016 =( )x(1000) = 1565.9$
𝟑𝟓𝟔.𝟗