LABORATORY

ORGANIZATION

MAKING SOLUTION
Member of Group 3 :
 Firyal Nabilah Q A 170301940
 Nuril Fatimah 17030194053
 Imtikhana Nur K 170301940
PKU 2017
 Materials and Equipments
Equipments :
■ Pipettes 3 pieces
■ Graduated cylinder 10 mL 1 buah
■ Glass funnel 60 mm 1 buah
■ Beaker glass 250 mL 2 pieces
■ Volumetric flask 200 mL 1 piece
■ Volumetric flask 100 mL 1 piece
■ Spatula 1 piece

Materials :
■ PP indicator Powder 0,2 g
■ CuSO4 powder 1g
■ H2SO4 17,8 M 5,6 mL
■ Ethanol 70 % 200 mL
 1. Prepare tools and materials

 
   
   
   
   
   
   
   
   

Picture 1. Tools Picture 2. Materials

 Calculation H2SO4 1 M that we need
■ H2SO4 1 M Solution
V1 x M1 = V2 x M2
100 mL x 1 M = V2 x 17,8 M
V2 = 100 mL : 17,8
V2 = 5,6 mL

H2SO4 1 M Solution
■ it is need 5 mL in the experiment
■ There are 8 groups in 5 class.
■ We need back up solution
■ So, we need : 5 x 8 x 5 x 2 = 400 mL
Lines Work of Making H2SO4 1 M
H2SO4 concentrated

1. Measuring 5,6 mL H2SO4 concentrated in graduated

cylinder
2. Poured 5,6 mL H2SO4 concentrated into measuring flask
100 mL
3. Added water drop by drop until boundary mark
4. Shaked the solution until homogeonus
5. Moved the solution to reagent
6. Repeat until 4 times

H2SO4 Solution
3. Making H2S04 1 M
 
   
   
   
   
   
   
   
   

Picture 1. Measuring 5,6 mL Picture 2. Added water Picture 3. Added water until
H2SO4 concentrated in graduated drops by drops boundary mark
cylinder and poured 5,6 mL H2SO4
concentrated into measuring flask
200 mL

   
   
   
   
   
   
   
   
   
   
Picture 4. Move the solution into  

reagent
Calculation of making CuSO4 0,5%
■ it is need 3 mL in the experiment
■ There are 8 groups in 5 class.
■ We need back up solution
■ So, we need : 3 x 8 x 5 x 2 = 240 mL
Lines Work of Making CuSO4 0,5%
CuSO4 Powder

1. Weigh 1 gram powder CuSO4

2. Poured 1 gram powder CuSO4 into
measuring flask 200 mL
3. Added water until boundary mark
4. Shaked the solution until homogeonus
5. Moved the solution to reagent

CuSO4 Solution
2. Making CuSO4 0,5 %
 
   
   
   
   
   
   
   
   

Picture 1. Weigh 1 gram Picture 2. Powder Picture 3. Dissolve

powder CuSO4 CuSO4 1 gram CuSO4 into water

   
   
   
   
   
   
   
   
   
   
   
Picture 4. Added water Picture 5. Move the
until boundary mark solution into reagent
bottle
Caculation of Penolphtalein Indicator
■ it is need 4 mL in the experiment
■ There are 8 groups in 5 class.
■ We need back up solution
■ So, we need : 4 x 8 x 5 x 2 = 320 mL
Lines Work of Making The Solution of
Penolphtalein Indicator
Indicator pp Powder

1. Weigh 0,2 gram powder of Indicator pp

2. Poured 0,2 gram powder Indicator pp into
measuring flask 200 mL
3. Added ethanol until boundary mark
4. Shaked the solution until homogeonus
5. Moved the solution to reagent
6. Repeat until 2 times
Indicator pp Solution
3. Making indicator pp
 
   
   
   
   
   
   
   
   

Picture 1. Weigh 0,2 gram Picture 2. PP indicator Picture 3. Poured 0,2 gram powder
powder of PP indicator powder indicator pp into measuring flask 200 mL
and added water until boundary mark

   
   
   
   
   
   
   
   
   
   
   
Picture 4. Move the solution
into reagent bottle
Calculation
■ CuSO4 0,5 % ( 0,5 g CuSO4 in the 100 mL CuSO4 solution )
M CuSO4 = m/BM x 1000/V
= 0,5 /250 x 1000/100
= 0,02 M
■ PP Indicator Solution
0,5 grams diluted into 100 mL ethanol.
m1/m2 = V1/V2
0,5/m2 = 100/200
m2 = 1 gram
THANK YOU 