INFRARED ABSORPTION

SPECTROSCOPY

VISHAL P. TIWARI
ROLL NO : 06
MSC PART 1, CHEMISTRY
SS &LS PATKAR VARDE COLLEGE
 Introduction

For analyzing both organic and

inorganic compounds.
Non destructive analysis .
Simple method.
 Three infrared portions

Near infrared region(0.8-2.5µm wavelength)

Mid infrared region (2,5-25 µm wavelength)
Far infrared region (25-1000µm wavelength)
Instrumentation

 IR radiation source
 Monochromators
 Sample cells and sampling of substances
 Detectors
IR radiation source

Incandescent lamp
Nernst glower
Globar source
Mercury arc
Monochromators
Prism monochromator
1.Monopass &
2.Double pass monochromator
Grating monochromator
Sample cells and sampling of substance

 Sampling of solids,
1. Solid run in solution
2. Solid films
3. Mull technique
4. Pressed pellet technique
Sampling of liquids
Sampling of gases
Detectors
 Bolometers
 Thermocouple
 Thermistor
 Photoconductivity cell
 Semiconductor detectors
 Despersive Instrument
Single beam spectrophotometer
Double beam spectrophotometer
 Non Despersive Instrument
Filter photometers
Non filter photometers
 References

1. D.A.Skoog, F.J. Holler, T.A. Nieman, Principle

of Instrumental Analysis , 5th Edition
,Harcourt Asia Publishers ,Chapter 16,17
2. R.D. Braun, Introduction to Instrumental
Analysis McGraw Hill Publishers . Chapter
12.