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Gail Research and Development Noida: Guide Mr. N.K. Pande D.G.M (R&D) Vaibhav Raj ECHE16034 Rgipt
Gail Research and Development Noida: Guide Mr. N.K. Pande D.G.M (R&D) Vaibhav Raj ECHE16034 Rgipt
Gail Research and Development Noida: Guide Mr. N.K. Pande D.G.M (R&D) Vaibhav Raj ECHE16034 Rgipt
ABSORPTION COLUMN
GUIDE
VAIBHAV RAJ
MR. N.K. PANDE 20TH MAY 2019-28TH JUNE 2019
ECHE16034
D.G.M ( R&D )
RGIPT
CONTENTS
• PROBLEM STATEMENT
• APPROACH FOR SOLVING
• CONCLUSION FOR APPROACH
• NEW APPROACH FOR GIVEN PROBLEM
• STOICHIOMETRIC METHOD
• SOLUBILITY CHART
• EXPERIMENTS
• CALCULATIONS
• CONCLUSION FOR SECOND APPROACH
• NEW PROBLEM STATEMENT
• APPROACH FOR NEW PROBLEM STATEMENT
• RESULTS
• REFERENCES
1. PROBLEM STATEMENT
Designing of an absorption column for absorbing co2 to bring down pH of an
alkaline aqueous solution of 1.5% NaOH to 7.5 of Gail pata plant in IOPS section.
Design Basis
• Flow rate of alkaline water = 8535 Kg/Hr. NaOH (WT %) = 1.5
• Purity of CO2 gas is 100% and available in plenty at .5 Kg/Cm2 at 250C.
Problem
• Kremser equation don’t work here as concentration of gas gets cancelled out.
• Acidic medium so there will be corrosion problem.
APPROACH FOR SOLVING
For Packed Tower
Assuming dilute solutions
• Get Equilibrium Data By Solving For psat at given operating conditions.
• Use Coulborn equation for determining Number of transfer unit.
• Do further calculations for getting other details.
Problem
• Coulborn equation don’t work here as concentration of gas gets cancelled out which yield no
result.
CONCLUSION FOR APPROACH
• Approach was related to Physical Absorption.
• Tray tower and packed tower are not suitable for these cases.
• 1 Mole of CO2 consumes 2 Mole of NaOH. ( Theoretical quantity of CO2 required for
Calculations. )
• Amount of NaOH = (8535 X 1.5)/(100 X 40) KMol/Hr.
• By help of solubility chart we can get details about how much CO 2 is soluble in water at constant
temperature.
• By solubility chart at constant temperature can get data about the pressure and if flowrate of co 2 is needed to
be decreased then pressure should be increased.
• Also from here we are getting idea about how much water is required to complete the reaction but there must
be some off gas or some excess co2 which is unaccountable till now.
• Determining flow rate of co2 based on given velocity and flow rate.
Design Basis
• http://www.chemalone.com/criteria-of-selection-between-different-types-of-absorbers/
• https://nptel.ac.in/courses/103103035/module4/lec4.pdf
• https://books.google.co.in/books?
id=a6uMtgoxjyIC&printsec=frontcover&source=gbs_ge_summary_r&cad=0#v=onepage&q&f=false