SIMPLE DISTILLATION

(Ethyl alcohol)
Time (min) Temperature Time (min) Temperature
Initial temp
1 32 16 34.1
2 32 17 34.2
3 32 18 34.5
4 32 19 34.75
2nd adjustment to
5 32 heating mantle 60 20 35
degrees
6 32 21 35.2
7 32 22 36
8 32 23 36.5
9 32 24 36.8
3rd adjustment to heating
10 32 mantle 80 degrees 25 41
Ethyl alcohol’s temp.
11 33 increases 26 65
12 33.2 27 74 1st drop of the distillate

13 33.5 28 75.2
14 33.75 29 76
15 34 30 76.2 Boiling pt. of ethyl alcohol
Final temp recorded.
SIMPLE DISTILLATION (ETHYL ALCOHOL)

LINE GRAPH OF SIMPLE DISTILLATION (ETHYL ALCOHOL)

90

80

70

60

50

40

30

20

10

0
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30
LINE GRAPH
SIMPLE DISTILLATION
(Isopropyl alcohol)
Time (min) Temperature Time (min) Temperature
1 33 Initial temp (50 degrees)
24 35
2 33 25 35
3 33 26 35
4 33
27 35
5 33
28 35.5
6 33
29 35.5 adjustment to heating
7 33 mantle 80 degrees
8 33.5
30 35.5
9 33.5 31 35.5
10 33.9 32 35.5
11 34 33 36
12 34 34 75
13 34 35 77 1st drop of the distillate

14 34 36 78
15 34 37 78.5
16 34.5 38 79
17 34.5 39 79
18 34.5 40 79
19 34.5 41 79.5
20 35 42 79.5
21 35
43 79.5
22 35
44 79.5
23 35
45 79.5
SIMPLE DISTILLATION (ETHYL ALCOHOL)

LINE GRAPH OF SIMPLE DISTILLATION (ISOPROPYL ALCOHOL)

90

80

70

60

50

40

30

20

10

0
1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 40 41 42 43 44 45
LINE GRAPH
 FRACTIONAL
DISTILLATION
(Ethyl alcohol)
Time (min) Temperature

1 32 INITIAL

2 32
3 72
1ST DROP
4 75
5 75
6 75
7 76
SIMPLE DISTILLATION (ETHYL ALCOHOL)

LINE GRAPH OF FRACTIONAL DISTILLATION (ETHYL ALCOHOL)

80

70

60

50

40

30

20

10

0
1 2 3 4 5 6 7
LINE GRAPH