PSG COLLEGE OF ARTS AND

SCIENCE(AUTONOMOUS)
Affiliated to Bharathiar University
Coimbatore-641014.
SYNTHESIS AND CHARACTERISATION OF
MANGANESE DOPED TITANIUM DIOXIDE
NANOPARTICLES

Candidate Guide PRIYADHARSHINI.R

Dr.M.ELANGO M.Sc.,M.Phil.,Ph.D.,
(18MPH019) Assistant Professor of Physics
Department of Physics
 TABLE OF CONTENTS
0 0
02
1
INTRODUCTI
ON&
MATERIAL
INTRODUCTI 3
CHARACTERISA
TION
MATERIAL ON TECHNIQUES &
PREFERNCE EXPERIMENTAL
PROCEDURE

04 05
RESULT & CONCLUSI
DISCUSSIO ON
N
EXPERIMENTAL PROCEDURE-Mn DOPED
TiO2
3.6 ml of Titanium
isopropoxide
Transparent Calcinated at
Ti{OCH(CH3)2}4 in
solution was 300°C for 3 hrs
100 ml distilled water
formed

02 04 06

01 03 05
5 ml of ammonia Centrifuge at Grained for 30
was added to 2000 rpm for 10 mins Mn doped
maintain pH- minutes TiO2
6,8,10 and stirred nanoparticles
for 3 hours
formed
CHARACTERIZATION
TECHNIQUES

UV VISIBLE
SPECTROSCO
XRD PY FTIR

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image on the screen image on the screen
with your own with your own
XRD
• ● X-Ray
  diffraction experiment is performed by the Shimadzu diffractometer
using CuKα line.
• The obtained peaks in the xrd graph is well matched to the JCPDS card no.
894921, and shows the Tetragonal phase of TiO2
• Average grain size of the molybdenum trioxide nanoparticle corresponding to
the highest intensity peak was found to be 6.2040 nm using Scherrer’s formula
D = (nm)
SNEAK PEEK
ANTIFUNGAL
ACTIVITY
The results of antifungal activity against Aspergillus shows a good
variation with variation in pH of Mn doped TiO2 nanoparticles, of pH 6,
pH 8 and pH 10.

 
 
CONCLUSIO
N
● The Mn doped TiO2 (10%) nanoparticles was synthesized with different
pH=6,8,10 by Co-precipitation method.The prepared Mn doped TiO 2 nano
particles were subjected to analytical techniques for material confirmation.

● The XRD pattern revealed the tetragonal structure of the sample, and the
crystalline size for the Mn doped TiO2 of pH=6 is about 6.18 nm whereas the size
increases to 6.20 nm and 6.50 nm for pH=8,10 respectively.

● The optical absorption spectra showed red shift in the Mn doped TiO 2
nanoparticles when comparing it with the pure TiO2 nanoparticles. The band
gap of Mn doped TiO2 (10%) nanoparticles of pH=6,8,10 was about
4.05 eV, 4.06eV and 4.03eV respectively.

● The antimicrobial activity shows that the increase in pH of TiO₂ increases the
antifungal activity.