Progress Lab

20/12/2021 TOPTAP
Last week
• Aj nick
• Over Dope TiO2 QDs in 0.2 M KCl : 0.1 M Citirc acid (0% 5% 20% 40%)
• Review paper
ETL
• TTIP 200ul in 2 ml ethanol (1:10)
• Pre spin 2000 rpm 3s spin 5000 rpm 30 s
• Annealing 500⁰C 1 hour
• TiO2 QDs 0.2 M KCl Dope in TTIP
• Pre spin 2000 rpm 3s spin 5000 rpm 30 s
• Annealing 500 ⁰C 1 hour
Perovskite
• PbI2 : MAI (1:1)
• PbI2 461 mg
• MAI 159 mg
• DMF:DMSO (4:1) 1ml
• DMF 800 ul
• DMSO 200 ul
• Stirring at 70 ⁰C Over night
• Spin 5000 rpm 30 s (anti-solvent after 15 s)
• Annealing 100 ⁰C 1 hour
Spiro-OMeTAD
• Spiro-OMeTAD 0.050 g in 700 uL CB
• Stir at room temperature over night
• Dope tBp 20.16 uL and Li-TFSI 12.25 uL
• Spin 4500 rpm 30 s
Complete Cells
1st TTIP
2nd 5% dope (100uL)
3rd 20% dope (400uL)
4th 40% dope (800uL)
Next
• 1:10
• 2%
• 5%
• 10 %