Project planning of a sustainable process for PET waste recycling

Process flow sheet and Equipment selection

Members of PSE (Group 1)

Aagam Atulkumar Shah Joydeep Bagchi Prachi Nilesh Shah
Esma Yeliz Aksungur Jyotimay Baishya Prakriti Gupta
Gayathri Venkatarathnam Nithya Simha Sunay Hesenov

Name, Vorname|
Dortmund Ort, Datum
, 17.11.2022
 Introduction

Name,
Sunay,Vorname|
Hasanov|Ort, Datum 17.11.2022
Dortmund, 2
 Introduction

Name,
Sunay,Vorname|
Hasanov|Ort, Datum 17.11.2022
Dortmund, 3
 Introduction
Recycling of
20kt/year PET

Mechanical Chemical Thermal

Recycling Recycling Conversion

Aminolysis Ammonolysis Glycolysis Hydrolysis Methanolysis Chemolysis

Cost Efficient Expensive

Name,
Sunay,Vorname|
Hasanov|Ort, Datum 17.11.2022
Dortmund, 4
 Today's recipe
 Process Description(PFD)
 Melt Glycolysis
 Reactor Design
 Filters
 Crystallizer
 Evaporator
 Condenser
 Dryer
 Material and Energy Balance

Name,
Sunay,Vorname|
Hasanov|Ort, Datum 17.11.2022
Dortmund, 5
 185°C

200-205°C,1atm

185°C,1atm 100°C,1atm 40°C,1atm

Rotary dryer

80-90°C

Name,
Sunay,Vorname|
Hasanov|Ort, Datum 17.11.2022
Dortmund, 6
 MELT GLYCOLYSIS

Bagchi,Vorname|
Name, Joydeep|Dortmund,
Ort, Datum 17.11.2022 7
 Introduction
 Continuous and steady state process

 High L/D ratio

 Behaviour similar to plug flow

 Channel depth decreases from conveying to

devolatilization zone

 Reaction and mixing takes place in the kneading

zone
Fig 1. Schematic diagram of Twin Screw Extruder(TSE)

Bagchi, Joydeep|Dortmund,
Name, Vorname| Ort, Datum 17.11.2022 1. R.R. Rao et. al(2021) 2. J.D.Patterson(2007) 3. Yousef Haik et.al (2017 ) 8
 Advantages Disadvantages
Low residence time(10-15 minutes) Only BHET oligomers are obtained
Better mixing High operating conditions
required is low Re-polymerization of BHET oligomer to get
monomer

Bagchi, Joydeep|Dortmund,
Name, Vorname| Ort, Datum 17.11.2022 1. J.D.Patterson(2007) 2. Yousef Haik et.al (2017) 9
 REACTOR DESIGN

Bagchi,
Name, Joydeep|Dortmund,
Vorname| Ort, Datum 17.11.2022 10
 Introduction K1

PET + EG Na2CO3 BHET(monomer) + BHET(oligomer)

 Slow reaction kinetics(first order)
K2

 Operating conditions: 185 °C and 1 atm pressure

 Raw Materials: PET flakes, Ethylene Glycol(solvent in excess)

 Catalyst: Sodium Carbonate(Na2CO3)

 Reaction type: Endothermal( change in enthalpy value = +10-

12 kJ/mol)

 Solid-Liquid reaction and the shrinking core kinetic model is

applied

Bagchi, Joydeep|Dortmund,
Name, Vorname| Ort, Datum 17.11.2022 1. Lopez et. al(2021) 2. Van-Pham et.al(2020) 3. A. Fijacko et.al (2013) 11
 Why cascade of continuous stirred tank reactors(CSTRs)?

 Continuous operation is required.

 Reaction is slow and uniform mixing and composition is required.

 Cascade of CSTRs resembles the behavior of plug flow(overall high conversion).

 High pressure drop and maximum conversion of the reactant is not suitable in the de-polymerization.

 Viscous reaction mixtures are better handled in this case.

Bagchi, Joydeep|Dortmund,
Name, Vorname| Ort, Datum 17.11.2022 1. Woods(2017) 2. Levenspiel(1998) 3. G.Schembecker(2022) 12
 Reaction Kinetics and Mass Balance
Rate law with respect to polyethylene terephthalate and excess of ethylene glycol

where, K1 is the forward reaction rate constant and K2 is the backward reaction rate constant
S.No. Stream Amount(kg/hr)
1. PET flakes 2500
2. EG inlet 8073
3. Unreacted PET 500
4. BHET monomer 3094
5. EG at outlet 5553
6. BHET dimer 1426

Name,
Bagchi,Vorname| Ort, Datum 11.17.2022
Joydeep|Dortmund, 1. Lopez et. al(2021) 2. Van-Pham et.al(2020) 3. Leo-Wang et.al (1999) 13
 Filter-1

Name,
Shah, Vorname| Ort,|Datum
Prachi Nilesh Dortmund, 17.11.2022 14
 Filter: Filtration of unreacted PET and oligomers
The reactant (PET) size fed in
reactor is 1 mm

The reactant size decreases as

reaction proceeds

Dead-zones and bypassing

PET above 72 °C acts as a rubbery

elastic
Figure 1 Schematic illustration of CSTR

Name,
Shah, Vorname|
Prachi Ort,
Nilesh, TUDatum
Dortmund, 17.11.2022 1. Levenspiel, O. (1998) 2. Holdich, R.G. (2008) 15
 Filter: Filtration of unreacted PET and oligomers
Table 1 Classification of filtration apparatus based on different parameter
Unit operation Particle size (mm) Type of Feed solid
process content (%w/w)
Vertical pressure 0.001- 0.12 Batch 0.08–0.5
filter leaf
vacuum leaf filter 0.001- 0.5 Batch 0.07–2
deep bed filtration 0.00001- 0.05 Batch 0.002–0.02
Rotary vacuum 0.001 – 0.7 or 0.01 - 1 Continuous 5–60
PET : 0.001 – 1 mm
drum filter
Solid content - 18 wt%
gravity drum filter 0.04- 0.5 Continuous 0.08-0.8
pressure drum 0.005- 0.2 Continuous 0.75–5
filter

Name, Vorname|
Shah, Prachi Ort, TU
Nilesh, Datum
Dortmund, 17.11.2022 1. Woods (2007) 2. Holdich, R.G. (2008) 16
 Filter: Rotary vacuum drum filtration unit
ⅆ𝑣 𝐴 𝛥𝑝
=
ⅆ𝑡 𝜇 ( 𝑅𝑓 + 𝛼 𝐶 ( 𝑣 / 𝐴 ))

– wt. of solids/ vol. of liquid (kg/m3)

(N/ Sec m2 )
– Pressure difference (N/ m2 )
(m2)
(m3)

Figure 2 Schematic of a rotary vacuum drum filter with

knife discharge

Shah,
Name,Prachi Nilesh,Ort,
Vorname| TUDatum
Dortmund, 17.11.2022 1. Tarleton, S. (2006) 2. Couper, J.R. (2005) 17
 Filter: Rotary vacuum drum filtration unit
Important parameter during the designing of the Rotary
Table 2 Information about filter cloth vacuum drum filter
Cloth T (°C) Resistance
towards Area
Ethylene Glycol
Polyester 130 Fair
Polypropylene 110 Good Wash flow rate

Total filter Area, Wash time

1. Standard filter corporation, Filter chart 2. Kobe, K.A. (1957)

Shah,
Name,Prachi Nilesh,Ort,
Vorname| TUDatum
Dortmund, 17.11.2022 18
https://www.standardfilter.com/products/filter-media-chemical-resistance-chart /
 Crystallizer

Name, Vorname|
Aksungur, Esma Ort,
YelizDatum
| Dortmund, 17.11.2022 19
 CRYSTALLIZER

Aksungur,
Name, Esma Ort,
Vorname| YelizDatum
| Dortmund, 17.11.2022 20
 CRYSTALLIZER

 Recovering of BHET BHET is dissolved in EG

 Continuous Crystallizer

BHET : 0.7 mm
Crystallizer type Crystal size (mm)
FC 0.2 – 0.8
DTB 0.8 – 2.5
Oslo 1.5 – 5

Aksungur,
Name, Esma Ort,
Vorname| YelizDatum
| Dortmund, 17.11.2022 1.Beckmann (2013) 2.Van-Pham et al. (2020) 21
 CRYSTALLIZER
1.6 40 - 90 ℃ 4
 Solubility
1.4 curve 3.5
1.2 3

g Na2CO3 / g EG
1 2.5
g BHET / g EG

0.8 2
0.6 1.5
0.4 1
10 - 55 ℃
0.2 0.5
0 0
0 10 20 30 40 50 60 70 80 90 100 110 120
Temperature (℃)

Aksungur,
Name, Esma Ort,
Vorname| YelizDatum
| Dortmund, 17.11.2022 1.Yao et al. (2022) 2.Oosterhof et al. (1999) 22
 CRYSTALLIZER
1.6 4

 Solubility curve
1.2 3

g Na2CO3 / g EG
 Solubility highly depends on temperature

g BHET / g EG
0.8 2

0.4 1
Cooling Crystallizer

0 0
0 20 40 60 80 100 120

Temperature (℃)

Aksungur,
Name, Esma Ort,
Vorname| YelizDatum
| Dortmund, 17.11.2022 1.Yao et al. (2022) 2.Oosterhof et al. (1999) 3. Kramer et al. (1999) 23
 CRYSTALLIZER
1.6 4
1.4 3.5
1.2 3

g Na2CO3 / g EG
1 2.5
g BHET / g EG

0.8 2
0.6 1 bar 1.5
0.4 1
0.2 0.5
0 0
0 10 20 30 40 50 60 70 80 90 100 110 120
Temperature (℃)

Aksungur,
Name, Esma Ort,
Vorname| YelizDatum
| Dortmund, 17.11.2022 1.Yao et al. (2022) 2.Oosterhof et al. (1999) 24
 CRYSTALLIZER

 Forced Circulation Cooling Crystallizer

 Vacuum

Low vapor pressure of EG

5.3 Pa @20 ℃

Aksungur,
Name, Esma Ort,
Vorname| YelizDatum
| Dortmund, 17.11.2022 1.Beckmann (2013) 2.Lewis et al. (2015) 25
 EVAPORATOR

Aksungur,
Name, Esma Ort,
Vorname| YelizDatum
| Dortmund, 17.11.2022 26
 EVAPORATOR
 Purifying of EG

 Further separation of BHET

 Selection of Proper Evaporator

 Viscosity of feed 20 cp @ 40

 Fouling EG is not aggressive towards most metals and plastics

Na2CO3 is noncorrosive
 Foaming EG

Aksungur,
Name, Esma Ort,
Vorname| YelizDatum
| Dortmund, 17.11.2022 1. Gallant (1967) 2. Ullmanns (2005) 3. Haque (2013) 27
 Vapor
EVAPORATOR

 External short tube vertical exchanger

natural circulation
 Boiling temperature of EG = 197.60
Feed
 Boiling point elevation : 1.5 – 5.5 Steam

200-205
1 bar Thick
liquor

Aksungur,
Name, Esma Ort,
Vorname| YelizDatum
| Dortmund, 17.11.2022 1. Ullmanns (2005) 2.Woods(2017) 3. Couper et al (2012) 28
 Condenser design

Shah,
Name,Aagam |Dortmund,
Vorname| 17.17.2022
Ort, Datum 29
 Introduction
 Industrial application

 Cost effective – plate type

 Efficient for low viscosity – double pipe

 Condensing hydraulic fluids, chemicals,

oils.

 Goal:- condense EG vapors from 203°C to Fig 1. Schematic diagram of water cooled condenser (Reference)
180°C

Shah,
Name,Aagam |Dortmund,
Vorname| 17.17.2022
Ort, Datum 1. Woods (2007) 30
 Design
 Allocating shell side and tube side

Table 1 Inlet and outlet temperature profile

Inlet (°C) Outlet (°C)

Shell Side (EG) 203.1 180

Tube Side (Water) 20 80

 Calculation of Log mean temperature difference(LMTD)

Shah,
Name,Aagam |Dortmund,
Vorname| 17.17.2022
Ort, Datum 1. Woods (2007) 31
  estimating flow pattern

Fig-1 Counter-current flow graph and equation(Reference)

 LMTD = 17.77°C using counter-current flow

 Calculating heat flow rate using Q = m*(Cp(EG)* ΔT + Δλ)

Δλ:- latent heat of condensation

Shah
Name,Aagam |Dortmund,
Vorname| 17.17.2022
Ort, Datum 1. Woods (2007) 32
  considering, heat loss by vapour = heat gain by water

 Calculating, mass of water required.

 Assuming heat transfer co-effcient(U);

U = 100 to 300 W/ m2°C for solvent-water system[1]

 Using Q= U*A*(LMTD), Area is estimated.

 Tube material:-
 Stainless steel, if water is used as cold fluid.
 Fluid is non-corrosive and if temp< 450 °C, carbon steel is cheaper option.

 EG is accumulated in storage tank and further used.

Shah
Name,Aagam |Dortmund,
Vorname| 17.17.2022
Ort, Datum 1. Woods (2007) 33
 Filter-2

Name, Vorname|
Baishya, Ort,
Jyotimay Datum
| Dortmund, 17.11.2022 34
 Further processing?
• Obtained BHET crystals and mother liquor from Crystalliser
• Recovery of BHET crystals
• Recirculation of mother liquor

What type of filtration

unit is more feasible?

Baishya,
Name, Jyotimay|
Vorname| Ort,Dortmund,
Datum 17.11.2022 35
 Different operating ranges of filters

Filter type Particle diameter Type Solid concentration

(mm) (% w/w)
Drum, gravity 0.04 – 5 Continuous 0.08 – 0.8

Drum, rotary vacuum 0.001 – 0.7 Continuous 5 – 60

BHET : 0.7 mm
Pressure, filter press 0.002 – 0.1 Batch 0.003 – 25 Conc. : 28.43 %
Drum, pre-coat rotary 0.0005 – 0.08 Continuous 0.02 – 0.1
vacuum

Baishya,
Name, Jyotimay|
Vorname| Ort,Dortmund,
Datum 17.11.2022 1.Woods(2017) 2.McCabe 36
 Key aspects of Rotary Drum Filter
• Low operating cost (+)
• Variability of drum speed (+)
• Higher purity (+)
• High moisture content (-)
• High energy consumption (-)

Baishya,
Name, Jyotimay|
Vorname| Ort,Dortmund,
Datum 17.11.2022 1.Hicks 2.McCabe 3. Sivakumar 37
 Key aspects of Rotary Drum Filter
• Low operating cost (+)
• Variability of drum speed (+)
• Higher purity (+)
• High moisture content (-)
• High energy consumption (-)

Baishya,
Name, Jyotimay|
Vorname| Ort,Dortmund,
Datum 17.11.2022 38
 Cake Discharge Method
Type Cake thickness (mm)
Belt discharge 3–5
Scraper discharge >6
Roll discharge >1
String discharge >6

Discharge of
thin and fragile
end products

Baishya,
Name, Jyotimay|
Vorname| Ort,Dortmund,
Datum 17.11.2022 1.Woods(2017) 39
 Dryer

Name,
Simha,Vorname|
Nithya | Ort, Datum 17.11.2022
Dortmund, 40
 Construction

Fig 3. Flights

• The length of the cyclinderical tube

is between 4-10 times of it’s
diameter and cyclindrical volume
will be 12-15%.
Fig 2. Construction of Rotary Dryer
• The flights are usually offset every
0.6-2m and shape depends.
Name,
Simha,Vorname|
Nithya | Ort, Datum 17.11.2022
Dortmund, 41
 Working Principle of Roatary Dryer

f m oist ure content

Lowering o
Wet material feed

Hot stream of
unsaturated air

Counter Current
Fig 4.Front View of Rotary Dryer

Name,
Simha,Vorname|
Nithya | Ort, Datum 17.11.2022
Dortmund, 1.Woods(2017)
 Operating Conditions

Capacity Large particle size

Drying Temperature 80°C
Moisture Reduction Up to 70%
Gas velocity 1 to 1.5 m/s
Heat Insulation thickness 30 – 40 mm
Residence Time 0.1 V/volumetric feed rate

Name,
Simha,Vorname|
Nithya | Ort, Datum 17.11.2022
Dortmund, 1. Woods, Donald R. et al. (2007) 43
 • Less sensitive to • Excess
particle size entrainment loss.
• Inexpensive • High velocity and
• Larger capacity gas volumes
• Also efficient at required
low temperatures

Name,
Simha,Vorname|
Nithya | Ort, Datum 17.11.2022
Dortmund, 44
 BASIC MATERIAL AND ENERGY BALANCE

Venkatarathnam, Gayathri
Name, Vorname| Ort, Datum | Dortmund, 17.11.2022 45
 Reactor: Kinetics
PET, EG BHET, Dimers
REACTOR

; [ 𝐷 ] [𝐸𝐺 ] 𝑚 𝐸𝐺
𝐾= ; 𝐾 =𝑎 (1+2 𝑎)
[𝐵] 2 𝑀 𝐸𝐺 ×𝑛 𝑃𝐸𝑇

80%
Conversion of PET, X 𝑊 0− 𝑊1 1
¿ × 100 % 𝑛 𝐵= 𝑛 0,262
𝑊0 1+2 𝑎 𝑃𝐸𝑇
0,656
1
= 𝑛 𝐷= 𝑛
1+2 𝑎 𝑃𝐸𝑇 0,172

Venkatarathnam,
Name, Gayathri
Vorname| Ort, Datum| Dortmund, 17.11.2022 1. S.Baliga et al 46
 Reactor: Kinetics Hydroxyl number:
Determination of the
extent of reaction or
number of hydroxyl
groups available for
further reaction.

Hydroxyl numbers
Molecular weights
(kg/kmol) (mg KOH/g)

PET 192
BHET 441,5
31,22%
Dimer 251,3
BHET 254
EG 1809,7 • Hydroxyl number: Number of milligrams of potassium hydroxide (KOH) required to neutralize the acetic acid
Dimer 446 taken up on acetylation of one gram of a chemical substance that contains free hydroxyl groups.
• : Number of moles of PET repeating units.
(H0) 959,22 • Total mass of the reacting system.
EG 62 • : Mass of free EG when glycolysis reaches equilibrium.
• H0 = measured hydroxyl number before glycol removal when the reaction reaches equilibrium.
(H1) 381,49 • H1 = measured hydroxyl number of glycolyzed products when reaction reaches equilibrium.

Venkatarathnam,
Name, Gayathri
Vorname| Ort, Datum| Dortmund, 17.11.2022 1. S.Baliga et al 47
 REACTOR

Unreacted PET, EG
PET, EG BHET, Dimers
REACTOR

Inlet streams(kg/hr) Outlet streams(kg/hr)

Unreacted PET 500,000

PET 2500,000
EG 5552,813
EG 8072,917
BHET 3093,966
Total 10572,92
Dimers 1426,138

Total 10572,92

Venkatarathnam,
Name, Gayathri
Vorname| Ort, Datum| Dortmund, 17.11.2022 48
 Jacketed cooling

𝑄𝑐𝑜𝑜𝑙𝑖𝑛𝑔 =( 𝑚×
˙ 𝐶 𝑝 × ∆ 𝑇 ) 𝑐𝑜 𝑜𝑙𝑖𝑛𝑔 𝑤𝑎𝑡𝑒𝑟 =( 𝑚
˙ × 𝐶 𝑝 ×∆ 𝑇 )𝑟𝑒𝑎𝑐𝑡𝑖𝑜𝑛 𝑚𝑖𝑥𝑡𝑢𝑟
/

185 °C

34,052kg/hr 100 °C

Venkatarathnam,
Name, Gayathri
Vorname| Ort, Datum| Dortmund, 17.11.2022 49
 Filtration
𝑐𝐹
𝑐= Density (kg/m3)
1− [ ( 𝑚 𝐹 / 𝑚𝐶 ) − 1 ] 𝑐 𝑠 / 𝜌
PET 1400

Dimers 1737,8

BHET 1216,3

EG 1110

Assumption:
Moisture content in slurry,
mF = 100%

1655,91kg/hr
Residual moisture content in
cake, mC= 16% = Rate of solids production
= Slurry flowrate (
= Solids concentration in feed)
= Density of solids )

Venkatarathnam,
Name, Gayathri
Vorname| Ort, Datum| Dortmund, 17.11.2022 1. McCabe and Smith(1993) 50
 Filtration
EG, BHET

Unreacted PET, EG
BHET, Dimers
FILTRATION

Unreacted PET, Dimers

Inlet streams (kg/hr) Outlet streams (kg/hr)

Unreacted PET 500,000 Solids in cake 1655,905
Dimers 1426,138 Solids in filtrate 270,233
BHET 3093,966
BHET 3093,966
EG 5552,813
EG 5552,813
Total 10572,92
Total 10572,92

Venkatarathnam,
Name, Gayathri
Vorname| Ort, Datum| Dortmund, 17.11.2022 51
 CRYSTALLIZATION

Name,Prakriti
Gupta, Vorname|| TUOrt, Datum 17.11.2022
Dortmund. 52
 CRYSTALLIZATION
BHET EG

Gupta,
Name, Prakriti
Prakriti || Ort,
Vorname|
Gupta, Dortmund,
TU Datum 16.11.22
Dortmund. 17.11.2022 53
 Current operating
point at X= 0.6632 g
BHET/g EG at 100°C

Gupta, Vorname|
Name, Prakriti | TU Dortmund.
Ort, Datum 17.11.2022 Yao, Haoyu et al (2022) 54
 Slope of mass ratio > 0.005 / °C ? Slope ≈ 0.01 > defining
value

Name,Prakriti
Gupta, Vorname|| TUOrt, Datum 17.11.2022
Dortmund. Lewis, Alison (2015) ISBN 13: 9781107052154 55
 V%(BHET) ? V%(incoming fluid) = 37%

Gupta,Vorname|
Name, Prakriti | TU
Ort,Dortmund.
Datum 17.11.2022 Lewis, Alison (2015) ISBN 13: 9781107052154 56
 One valuable product of Yes, only BHET

high capacity?

Name,Prakriti
Gupta, Vorname|| TUOrt, Datum 17.11.2022
Dortmund. Lewis, Alison (2015) ISBN 13: 9781107052154 57
 40°C
Mother liquor [kg/hr]
110-100°C
Solid residue 34.371
Inlet stream [kg/hr] BHET 4664.36
Residual solids 270.233 4698.734
Total flow rate
BHET 3093.966
Crystallization
EG 4664.363
   
Wet crystals [kg/hr]
Total flow rate 8028.562
PET residue 270.233
BHET 3059.595
Total flow rate 3329.828

Gupta,Vorname|
Name, Prakriti | TU
Ort,Dortmund.
Datum 17.11.2022 58
 EVAPORATION

Name,Prakriti
Gupta, Vorname|| TUOrt, Datum 17.11.2022
Dortmund. 59
 EVAPORATION
Assumptions

 Specific heat of feed ≈ specific heat of pure EG

 Thick solution is at boiling point of pure EG with BPE

 Heating utility : Medium pressure steam

 𝐻𝑒𝑎𝑡 𝑖𝑛𝑝𝑢𝑡 𝑟𝑒𝑞𝑢𝑖𝑟𝑒𝑚𝑒𝑛𝑡 𝑄̇𝐻 [𝑘𝑊] =𝐸𝑡ℎ𝑎𝑙𝑝𝑦 𝑐ℎ𝑎𝑛𝑔𝑒 𝑜𝑓 𝑓𝑒𝑒𝑑 𝑠𝑡𝑟𝑒𝑎𝑚+𝐸𝑛𝑒𝑟𝑔𝑦 𝑟𝑒𝑞𝑢𝑖𝑟𝑒𝑑 𝑡𝑜 𝑣𝑎𝑝𝑜𝑟𝑖𝑧𝑒 𝒇

𝑓𝑟𝑎𝑐𝑡𝑖𝑜𝑛 𝑜𝑓 𝑡ℎ𝑒 𝑓𝑒𝑒𝑑 = 𝐸𝑛𝑡ℎ𝑎𝑙𝑝𝑦 𝑜𝑓 medium 𝑝𝑟𝑒𝑠𝑠𝑢𝑟𝑒 𝑠𝑡𝑒𝑎𝑚 𝑢𝑡𝑙𝑖𝑡𝑦.

Name,Prakriti
Gupta, Vorname|| TUOrt, Datum 17.11.2022
Dortmund. 60
 Evaporated EG [kg/hr]
3265.05
 EG

Total flow rate 3265.05

Inlet streams [kg/hr]

Solids in mother liquor 34.371 Evaporation

EG 4664.363
Thick liquid [kg/hr]
   
Residual solids 34.371
Total flow rate 4698.734
EG present in thick liquid 1399.309

Total flow rate 1433.68

Name,Prakriti
Gupta,
Gupta, Vorname|
Prakriti TUOrt,
|| TU Datum 17.11.2022
Dortmund.
Dortmund. 17.11.2022 61
 CONCLUSION

Name,Prakriti
Gupta, Vorname|| TUOrt, Datum 17.11.2022
Dortmund. 62
 Proposed Process flow diagram

Name,Prakriti
Gupta, Vorname|| TUOrt, Datum 17.11.2022
Dortmund. 63
 Proposed Process flow diagram

Equipment selection

Name,Prakriti
Gupta, Vorname|| TUOrt, Datum 17.11.2022
Dortmund. 64
 Proposed Process flow diagram

Equipment selection

Property estimation

Name,Prakriti
Gupta, Vorname|| TUOrt, Datum 17.11.2022
Dortmund. 65
 Proposed Process flow diagram

Equipment selection

Property estimation

Identification of plant decision variables

Name, Prakriti
Gupta, Vorname|| TUOrt, Datum 17.11.2022
Dortmund. 66
 Objectives for the next fortnight …

 Extensive equipment design and dimensioning

 Calculations of plant utilities and design

 Optimization of plant decision variables

Name,Prakriti
Gupta, Vorname|| TUOrt, Datum 17.11.2022
Dortmund. 67
 Thank you for your
time and attention.

www.tu-dortmund.de
Name,
Gupta,Vorname| Ort,Dortmund.
Prakriti | TU Datum 17.11.2022
 www.tu-dortmund.de
Name, Vorname| Ort, Datum