DESIGN AND CONSTRUCTION OF

POLYANILINE POLYMERIATION REACTION

MONITORING SYSTEM AT 0-4
TEMPERATURE BASED ON IOT
Nova Indah Safitri
19101020
Advisor : Examiner :

Dr. Eng. Anjar Taufik Hidayat, S.Pd.,M.Sc. Sevia Indah Purnama, S.ST., M.T.
Prasetyo Yuliantoro, S.T.,M.T.
 Chapter 1:
RESEARCH BACKGROUND
Among the various conducting polymers made from organic materials,
polyaniline is a type of conducting polymer with high stability, low cost of
synthesis, and high electrical conductivity. The most common and easy
polymerization method to do is chemical oxidative polymerization. In this
method, most researchers use freezing temperatures or ice to obtain a more
conductive polymer.
Therefore a method is needed to control the temperature of the solution to be
constant at 0-4 ℃. In this study a tool was designed to monitor pH and
temperature in the polymerization reaction process using the pH-4502C sensor
and the DS18B20 sensor which is integrated with nodeMCU and can be accessed
via the internet using the Blynk app. This tool is equipped with a Styrofoam box
and ice cubes as a cooling material to keep the temperature within the range of 0-
4 ℃. The system measures pH and temperature, and sends the data to blynk and
monitors it via smartphone.
 PROBLEM
IDENTIFICATION
How to make a polymerization reaction
monitoring system at 0-4 ℃ based on IoT?
How are the test results and accuracy of the
DS18B20 sensor and the ph-4502C sensor?

How is the performance of the polymerization reaction

monitoring system at a temperature of 0-4 ℃ based on
IoT in remote monitoring?
 RESEARCH
PURPOSE
Measuring the
performance of a
polymerization
Create a reaction
Measuring the
polymerization monitoring system
accuracy of the
reaction at 0-4 ℃
DS18B20 sensor
monitoring temperature
and the pH- based on IoT in
system at 0-4 ℃
4502C sensor. remote
based on IoT.
monitoring.
 2016
Palash Chandra Maity dan Mudrika
Khandelwel
Research on the effect of polymeriation
process time and temperature of polyaniline
on conductivity and morphology.
The results show that polyaniline polymerized
at low temperatures produces higher
conductivity values than polyaniline
polymerized at room temperature. With the
data obtained at room temperature or room
temperature obtained a conductivity of 5.7
S/cm, and at low temperatures (0 - 4 ° C) can
obtain a conductivity of 7.11 S/cm - 11.1 S/cm
2021
Risma Alfia
This research is about monitoring four water
quality parameters in an aquaponic system,
namely temperature, pH, (TDS), and water
turbidity which the results are displayed on a
web server and telegram. This research uses
several sensors such as DS18B20, PH-4502C,
SEN0244, SEN0189, and arduino pro mini.
Based on the research results, it was found
that the developed prototype has an accuracy
rate of 98.63% for the water temperature
sensor and 98.36% for the water pH sensor.
 Chapter 3:
Research
Flowchart
Block diagram
Ilustration
Design
System Work
Flowchart
 System
Design
Results

Display of temperature and

pH monitoring on the blynk
Chapter 4: Table of DS18B20 temperature sensor
calibration results
Average
No pH measurement percentage
accuracy
1 4 99,690 %

2 6,67 99,813 %

3 9,2 99,845 %

Average accuracy % 99,783 %

 Table of ph-4502c sensor
calibration results
Average
No Water type percentage
accuracy
1 Hot water 99,479 %

2 Plain water 99,273 %

3 Ice water 97,485 %

Average accuracy % 98,745 %

 Notification, if the
temperature is not
in the range of 0-4 ᵒC
 Monitoring Using A Smartphone on
the blynk app

Graph of temperature and pH monitoring

in the polyaniline polymerization process
for 3 hours
 Chapter: 4

Results PaNi Powder

PaNi powder
filtration PaNi powder research
process results reference
 Conclusion
An IoT-based monitoring system for polyaniline polymerization reactions at 0-4 ℃, was
1 created by starting with designing the end device, setting up the nodeMCU program using
the Arduino IDE, and connecting it to the blynk application using an internet connection.

The test results that have been carried out by the DS18B20 sensor and pH-4502C sensor
2 have a good accuracy of 98.745% for the DS18B20 temperature sensor and an accuracy
of 99.783% for the pH-4502C sensor.

An IoT-based polymerization reaction monitoring system at 0-4 ℃ has been

successfully created and implemented well in remote monitoring and is capable of
3 transmitting data in real-time via an internet connection. The system is able to provide
notifications via the blynk application when unwanted changes or conditions occur, in
this research if the temperature is not in the range of 0-4 ℃.
Thank
you!